Review of Recent Development of in situ/operando Characterization Techniques for Lithium Battery Research
Abstract
The increasing demands on energy storage requires significant improvement of current Li-ion battery electrode materials and development of advanced electrode materials. This necessitates in-depth understanding of the reaction processes, degradation mechanism, and thermal decomposition mechanisms of electrode materials under realistic operation conditions. This can be achieved by in situ/operando characterization techniques that provide information of the structure evolution, redox mechanism, solid-electrolyte interphase (SEI) formation, side reactions and Li-ion transport properties under operating conditions. In this review, recent progress of in situ/operando techniques employed for the investigation of the structural stability, dynamic properties, chemical environment changes and morphological evolution during electrochemical processes are described and summarized in detail. The experimental approaches reviewed in this paper include X-ray, Electron, Neutron, Optical, and Scanning probes. Each advanced technique has unique capabilities to study specific properties of electrode materials within specific limitations. The experimental methods and operating principles, and especially the in situ cell designs are described in detail. To illustrate the possibilities of each technique representative studies making use of these in situ/operando techniques are discussed and summarized. Finally, the major current challenges and future opportunities of the in situ/operando techniques are outlined. Several important battery challenges are anticipated to profit from thesemore »
- Authors:
-
- Tsinghua Univ., Shenzhen (China). Engineering Lab. for the Next Generation Power and Energy Storage Batteries, Graduate School at Shenzhen
- Tsinghua Univ., Shenzhen (China). Engineering Lab. for the Next Generation Power and Energy Storage Batteries, Graduate School at Shenzhen; Tsinghua Univ., Shenzhen (China). Nano Energy Materials Lab. (NEM), Tsinghua-Berkeley Shenzhen Inst. (TBSI)
- Brookhaven National Lab. (BNL), Upton, NY (United States). Chemistry Dept.
- Tsinghua Univ., Shenzhen (China). Nano Energy Materials Lab. (NEM), Tsinghua-Berkeley Shenzhen Inst. (TBSI)
- Delft Univ. of Technology (Netherlands). Dept. of Radiation Science and Technology
- Hong Kong Polytechnic Univ. (Hong Kong)
- Publication Date:
- Research Org.:
- Brookhaven National Laboratory (BNL), Upton, NY (United States)
- Sponsoring Org.:
- USDOE Office of Energy Efficiency and Renewable Energy (EERE), Vehicle Technologies Office (EE-3V); National Nature Science Foundation of China (NNSFC); USDOE
- OSTI Identifier:
- 1507700
- Alternate Identifier(s):
- OSTI ID: 1513307
- Report Number(s):
- BNL-211557-2019-JAAM
Journal ID: ISSN 0935-9648
- Grant/Contract Number:
- SC0012704; DE‐SC0012704
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Advanced Materials
- Additional Journal Information:
- Journal Volume: 31; Journal Issue: 28; Journal ID: ISSN 0935-9648
- Publisher:
- Wiley
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 25 ENERGY STORAGE; characterization techniques; in situ-operando; lithium battery
Citation Formats
Liu, Dongqing, Qian, K., Li, H., Wang, S.W., Yu, Q. P., Qin, X.Y., Yang, Q.-H., Kang, F.Y., Li, B. H., Shadike, Zulipiya, Lin, R. Q., Yang, X.-Q., Qian, K., Liu, M., Ganapathy, S., Wagemaker, M., and Li, K. K. Review of Recent Development of in situ/operando Characterization Techniques for Lithium Battery Research. United States: N. p., 2019.
Web. doi:10.1002/adma.201806620.
Liu, Dongqing, Qian, K., Li, H., Wang, S.W., Yu, Q. P., Qin, X.Y., Yang, Q.-H., Kang, F.Y., Li, B. H., Shadike, Zulipiya, Lin, R. Q., Yang, X.-Q., Qian, K., Liu, M., Ganapathy, S., Wagemaker, M., & Li, K. K. Review of Recent Development of in situ/operando Characterization Techniques for Lithium Battery Research. United States. https://doi.org/10.1002/adma.201806620
Liu, Dongqing, Qian, K., Li, H., Wang, S.W., Yu, Q. P., Qin, X.Y., Yang, Q.-H., Kang, F.Y., Li, B. H., Shadike, Zulipiya, Lin, R. Q., Yang, X.-Q., Qian, K., Liu, M., Ganapathy, S., Wagemaker, M., and Li, K. K. Tue .
"Review of Recent Development of in situ/operando Characterization Techniques for Lithium Battery Research". United States. https://doi.org/10.1002/adma.201806620. https://www.osti.gov/servlets/purl/1507700.
@article{osti_1507700,
title = {Review of Recent Development of in situ/operando Characterization Techniques for Lithium Battery Research},
author = {Liu, Dongqing and Qian, K. and Li, H. and Wang, S.W. and Yu, Q. P. and Qin, X.Y. and Yang, Q.-H. and Kang, F.Y. and Li, B. H. and Shadike, Zulipiya and Lin, R. Q. and Yang, X.-Q. and Qian, K. and Liu, M. and Ganapathy, S. and Wagemaker, M. and Li, K. K.},
abstractNote = {The increasing demands on energy storage requires significant improvement of current Li-ion battery electrode materials and development of advanced electrode materials. This necessitates in-depth understanding of the reaction processes, degradation mechanism, and thermal decomposition mechanisms of electrode materials under realistic operation conditions. This can be achieved by in situ/operando characterization techniques that provide information of the structure evolution, redox mechanism, solid-electrolyte interphase (SEI) formation, side reactions and Li-ion transport properties under operating conditions. In this review, recent progress of in situ/operando techniques employed for the investigation of the structural stability, dynamic properties, chemical environment changes and morphological evolution during electrochemical processes are described and summarized in detail. The experimental approaches reviewed in this paper include X-ray, Electron, Neutron, Optical, and Scanning probes. Each advanced technique has unique capabilities to study specific properties of electrode materials within specific limitations. The experimental methods and operating principles, and especially the in situ cell designs are described in detail. To illustrate the possibilities of each technique representative studies making use of these in situ/operando techniques are discussed and summarized. Finally, the major current challenges and future opportunities of the in situ/operando techniques are outlined. Several important battery challenges are anticipated to profit from these in situ/operando techniques, including the inhomogeneous reactions of high energy density cathodes, the development of safe and reversible Li metal plating and the development of stable SEI on electrodes.},
doi = {10.1002/adma.201806620},
journal = {Advanced Materials},
number = 28,
volume = 31,
place = {United States},
year = {Tue Apr 30 00:00:00 EDT 2019},
month = {Tue Apr 30 00:00:00 EDT 2019}
}
Web of Science
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