Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates

Gao, Pu-Xian; Lu, Xingxu; Hoang, Son

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Title: Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates

Abstract

A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.

Inventors:: Gao, Pu-Xian; Lu, Xingxu; Hoang, Son

Issue Date:: Tue Oct 11 00:00:00 EDT 2022

Research Org.:: Univ. of Connecticut, Storrs, CT (United States)

Sponsoring Org.:: USDOE; National Science Foundation (NSF)

OSTI Identifier:: 1986672

Patent Number(s):: 11465129

Application Number:: 16/465,969

Assignee:: The University of Connecticut (Farmington, CT)

DOE Contract Number:: EE0006854; CBET-1344792

Resource Type:: Patent

Resource Relation:: Patent File Date: 06/01/2018

Country of Publication:: United States

Language:: English

Citation Formats


                    Gao, Pu-Xian, Lu, Xingxu, and Hoang, Son. Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates.  United States: N. p., 2022. 
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                    Gao, Pu-Xian, Lu, Xingxu, & Hoang, Son. Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates.  United States.

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                    Gao, Pu-Xian, Lu, Xingxu, and Hoang, Son. Tue .  
        "Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates".  United States.  https://www.osti.gov/servlets/purl/1986672.

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@article{osti_1986672,

  title        = {Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates},

  author       = {Gao, Pu-Xian and Lu, Xingxu and Hoang, Son},

  abstractNote = {A method of making a titanium dioxide nanowire array includes contacting a substrate with a solvent comprising a titanium (III) precursor, an acid, and an oxidant while microwave heating the solvent, thereby forming a hydrogen titanate H2Ti2O5.H2O nanowire array. The hydrogen titanate nanowire array is annealed to form a titanium dioxide nanowire array. The substrate is seeded with titanium dioxide before starting the hydrothermal synthesis of the hydrogen titanate nanowire array. The titanium dioxide nanowire array is loaded with a platinum group metal to form an exhaust gas catalyst. The titanium dioxide nanowire array can be used to catalyze oxidation of combustion exhaust.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Oct 11 00:00:00 EDT 2022},

  month        = {Tue Oct 11 00:00:00 EDT 2022}

}

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Jian, Dunliang; Gao, Pu-Xian; Cai, Wenjie
Journal of Materials Chemistry, Vol. 19, Issue 7, p. 970-975
https://doi.org/10.1039/b817235h

Nonhydrolytic Synthesis of High-Quality Anisotropically Shaped Brookite TiO₂ Nanocrystals
journal, August 2008

Buonsanti, Raffaella; Grillo, Vincenzo; Carlino, Elvio
Journal of the American Chemical Society, Vol. 130, Issue 33, p. 11223-11233
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Zinc magnesium oxide nanofibers on glass substrate by solution growth technique
journal, August 2008

Gayen, R. N.; Das, S. N.; Dalui, S.
Journal of Crystal Growth, Vol. 310, Issue 18, p. 4073-4080
https://doi.org/10.1016/j.jcrysgro.2008.06.049

High-Quality Brookite TiO₂ Flowers: Synthesis, Characterization, and Dielectric Performance
journal, August 2009

Hu, Wanbiao; Li, Liping; Li, Guangshe
Crystal Growth & Design, Vol. 9, Issue 8, p. 3676-3682
https://doi.org/10.1021/cg9004032

Annealing induced nanostructure and photoluminescence property evolution in solution-processed Mg-alloyed ZnO nanowires
journal, September 2010

Shimpi, Paresh; Ding, Yong; Suarez, Ernesto
Applied Physics Letters, Vol. 97, Issue 10, Article No. 103104
https://doi.org/10.1063/1.3483614

Manganese-Cobalt Spinel Oxide Nanowire Arrays
patent-application, February 2020

Gao, Pu-Xian; Tang, Wenxiang
US Patent Application 16/465948; 20200061591
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20200061591

Sacrificial template method of fabricating a nanotube
patent-application, September 2004

Yang, Peidong; He, Rongrui; Goldberger, Joshua
US Patent Application 10/731745; 20040175844
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20040175844

Metal Oxide Nanorod Arrays on Monolithic Substrates
patent-application, September 2014

Gao, Pu-Xian; Guo, Yanbing; Zhang, Zhonghua
US Patent Application 14/347850; 20140256534
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140256534

Catalyst-free two-step growth of quasialigned ZnMgO nanorods and their properties
journal, March 2006

Zhu, Liping; Zhi, Mingjia; Ye, Zhizhen
Applied Physics Letters, Vol. 88, Issue 11, Article No. 113106
https://doi.org/10.1063/1.2185609

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Title: Microwave assisted and low-temperature fabrication of nanowire arrays on scalable 2D and 3D substrates

Abstract

Citation Formats

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One-dimensional metal oxide nanostructures for heterogeneous catalysis journal, January 2013

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Low-Temperature Diesel Oxidation Catalysts Using TiO₂ Nanowire Arrays Integrated on a Monolithic Substrate patent-application, January 2020

Growth and characterization of well-aligned densely-packed rutile TiO2 nanocrystals on sapphire substrates via metal–organic chemical vapor deposition journal, January 2008

Anodized aluminum oxide nanoporous template and associated method of fabrication patent-application, November 2006

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Zinc magnesium oxide nanofibers on glass substrate by solution growth technique journal, August 2008

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Annealing induced nanostructure and photoluminescence property evolution in solution-processed Mg-alloyed ZnO nanowires journal, September 2010

Manganese-Cobalt Spinel Oxide Nanowire Arrays patent-application, February 2020

Sacrificial template method of fabricating a nanotube patent-application, September 2004

Metal Oxide Nanorod Arrays on Monolithic Substrates patent-application, September 2014

Catalyst-free two-step growth of quasialigned ZnMgO nanorods and their properties journal, March 2006

Perovskite oxide nanotubes: synthesis, structural characterization, properties and applications
journal, January 2010

Boundary-Modulated Nanoparticle Junctions and a Method for Manufacture Thereof
patent-application, July 2013

Au Decorated Zinc Oxide Nanowires for CO Sensing
journal, August 2009

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journal, July 2004

One-dimension MnCo2O4 nanowire arrays for electrochemical energy storage
journal, January 2014

ZnO nanowires grown along the non-polar direction
journal, March 2008

The deposition and annealing study of MOCVD ZnMgO
journal, April 2005

Compacted nanoscale sensors by merging ZnO nanorods with interdigitated electrodes
conference, May 2011

Single crystalline brookite titanium dioxide nanorod arrays rooted on ceramic monoliths: a hybrid nanocatalyst support with ultra-high surface area and thermal stability
journal, January 2013

Low temperature synthesis and characterization of MgO/ZnO composite nanowire arrays
journal, March 2009

Method Of Preparing Patterned Carbon Nanotube Array And Patterned Carbon Nanotube Array Prepared Thereby
patent-application, November 2007

Growth and properties of ZnO/hexagonal ZnMgO/cubic ZnMgO nanopagoda heterostructures
journal, August 2007

Formation of Core/Shell-Type ZnO/CeO₂ Nanorods and CeO₂ Nanotube Arrays by Aqueous Synthesis and Wet-Etching
journal, June 2008

Fabrication and characterization of vertically aligned ZnMgO/ZnO nanowire arrays
journal, January 2008

Structure and optical properties of ZnO/Mg_0.2Zn_0.8O superlattices
journal, August 1999

Calculation of Formation Energy of Oxygen Vacancy in ZnO Based on Photoluminescence Measurements
journal, June 2010

Fine-Tuning the Dispersion and the Mobility of BaO Domains on NO_x Storage Materials via TiO₂ Anchoring Sites
journal, July 2010

A Study of Anomalous Temperature-Programmed Reduction Profiles of Cu2O, CuO, and CuO-ZnO Catalysts
journal, August 1994

Low-Temperature Surface Doping/Alloying/Coating Of Large Scale Semiconductor Nanowire Arrays
patent-application, July 2010

Methods to fabricate vertically oriented anatase nanowire arrays on transparent conductive substrates and applications thereof
patent, September 2014

Transition-Metal Doped Zinc Oxide Nanowires
journal, January 2006

Nonostructure arrays and methods of making same
patent-application, November 2007

Metal oxide nanorod arrays on monolithic substrates
patent, January 2018

A Simple Route to Porous ZnO and ZnCdO Nanowires
journal, June 2006

Nanowire Piezoelectric Nanogenerators on Plastic Substrates as Flexible Power Sources for Nanodevices
journal, January 2007

Facile preparation of ordered mesoporous MnCo₂O₄ for low-temperature selective catalytic reduction of NO with NH₃
journal, January 2015

Catalytic converter monolithic substrate retention
patent, January 1989

Effects of deposition temperature on the properties of Zn_1−xMg_xO thin films
journal, March 2004

One-dimensional metal oxide nanostructures for heterogeneous catalysis
journal, January 2013

Monolith structures, materials, properties and uses
journal, September 2001

Low-Temperature Diesel Oxidation Catalysts Using TiO₂ Nanowire Arrays Integrated on a Monolithic Substrate
patent-application, January 2020

Growth and characterization of well-aligned densely-packed rutile TiO₂ nanocrystals on sapphire substrates via metal–organic chemical vapor deposition
journal, January 2008

Anodized aluminum oxide nanoporous template and associated method of fabrication
patent-application, November 2006

Cu-Decorated ZnO Nanorod Array Integrated Structured Catalysts for Low-Pressure CO 2 Hydrogenation to Methanol
journal, December 2017

Thermally Stable Pt/CeO₂ Hetero-Nanocomposites with High Catalytic Activity
journal, April 2010

Robust 3-D configurated metal oxide nano-array based monolithic catalysts with ultrahigh materials usage efficiency and catalytic performance tunability
journal, September 2013

Method of producing regular arrays of nano-scale objects using nano-structured block-copolymeric materials
patent, October 2006

High-performance binder-free supercapacitor electrode by direct growth of cobalt-manganese composite oxide nansostructures on nickel foam
journal, September 2014

Hydrothermal synthesis and automotive exhaust catalytic performance of CeO₂ nanotube arrays
journal, January 2011

Mg_xZn_1−xO(0⩽x<0.2) nanowire arrays on sapphire grown by high-pressure pulsed-laser deposition
journal, April 2005

Oriented single crystalline titanium dioxide nanowires
journal, November 2008

Analysis of ZnO and ZnMgO nanopillars grown by self-organization
journal, June 2004

In situ TPR removal: a generic method for fabricating tubular array devices with mechanical and structural soundness, and functional robustness on various substrates
journal, January 2012

Preparation of Tractable Platinum, Rhodium, and Ruthenium Nanoclusters with Small Particle Size in Organic Media
journal, June 2000

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journal, August 2014

Nanowire sensor, sensor array, and method for making the same
patent-application, October 2009

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journal, April 2008

Growth of Submicrometer-Scale Rectangular Parallelepiped Rutile TiO₂ Films in Aqueous TiCl₃ Solutions under Hydrothermal Conditions
journal, June 2004

Band gap engineering and stimulated emission of ZnMgO nanowires
journal, July 2006

A simple low temperature synthesis route for ZnO–MgO core–shell nanowires
journal, October 2008

Reduction kinetics of porous zinc oxide pellet with CO–N₂gas mixture
journal, December 2008

Anomalous growth of multi-phased and multi-dimensional Manganese oxide–Metal (Fe, Co and Ni) oxide nanostructures: Synthesis and optical limiting properties
journal, October 2014

Storage of NO₂ on BaO/TiO₂ and the influence of NO
journal, July 2003

Low-temperature oxidation of CO catalysed by Co₃O₄ nanorods
journal, April 2009

Boundary-modulated nanoparticle junctions and a method for manufacture thereof
patent, April 2014

Thermal conductivity of an aligned carbon nanotube array
journal, November 2007

Scalable Integration of Highly Uniform Mn _x Co _{3− x} O ₄ Nanosheet Array onto Ceramic Monolithic Substrates for Low-Temperature Propane Oxidation
journal, October 2017

Method of Making a Nanotube Array Structure
patent-application, September 2015

Controlled synthesis of hierarchical Co _x Mn _3−x O ₄ array micro-/nanostructures with tunable morphology and composition as integrated electrodes for lithium-ion batteries
journal, January 2013

Strontium-Doped Perovskites Rival Platinum Catalysts for Treating NO_x in Simulated Diesel Exhaust
journal, March 2010

Optical biosensor
patent-application, January 2005

Vertically Aligned Single Crystal TiO₂ Nanowire Arrays Grown Directly on Transparent Conducting Oxide Coated Glass: Synthesis Details and Applications
journal, November 2008

Catalytic Converters, Insert Materials for Catalytic Converters, and Methods of Making
patent-application, February 2013

Substrate having a zinc oxide nanowire array normal to its surface and fabrication method thereof
patent-application, October 2005

Film Having Cobalt Selenide Nanowires and Method of Forming Same
patent-application, September 2010

Effect of Calcination Temperature on the Structure of a Pt/TiO₂ (B) Nanofiber and Its Photocatalytic Activity in Generating H₂
journal, August 2008

Synthesis, characterization, and photocatalytic properties of ZnO/(La,Sr)CoO₃ composite nanorod arrays
journal, January 2009

Nonhydrolytic Synthesis of High-Quality Anisotropically Shaped Brookite TiO₂ Nanocrystals
journal, August 2008

Zinc magnesium oxide nanofibers on glass substrate by solution growth technique
journal, August 2008

High-Quality Brookite TiO₂ Flowers: Synthesis, Characterization, and Dielectric Performance
journal, August 2009

Annealing induced nanostructure and photoluminescence property evolution in solution-processed Mg-alloyed ZnO nanowires
journal, September 2010

Manganese-Cobalt Spinel Oxide Nanowire Arrays
patent-application, February 2020

Sacrificial template method of fabricating a nanotube
patent-application, September 2004

Metal Oxide Nanorod Arrays on Monolithic Substrates
patent-application, September 2014

Catalyst-free two-step growth of quasialigned ZnMgO nanorods and their properties
journal, March 2006