In situ investigation of stress-induced martensitic transformation in granular shape memory ceramic packings
Abstract
Stress-induced martensitic transformation can occur in granular shape memory materials when individual particles experience high stresses and transform from a high-symmetry austenite phase to a low-symmetry martensite phase. This involves a highly heterogeneous distribution of the driving force and very low mechanical constraint for martensite nucleation, so the transformation behavior can be dramatically different from the well-documented case of monolithic solids. In this work, we investigate the stress-induced martensitic transformation in granular shape memory ceramic packings, which consist of single-crystal micro-particles of ZrO2-12 at%CeO2 and ZrO2-15 at%CeO2. Using in situ neutron diffraction, we study how the phase fraction, lattice strain, and integral peak broadness evolve during external loading, unloading, and subsequent heating. Several peculiar features are discovered, including (i) a continuous mode of transformation with a wide range of transformation loads, (ii) co-evolution of the packing structure, contact deformation, and martensitic transformation, and (iii) a strong correlation between the peak broadening and the transformed phase fraction. In addition, we show the first direct evidence of reversible stress-induced martensitic transformation in granular materials. We additionally discuss the mechanism for martensite nucleation and growth in granular packings and show how that leads to the observed transformation characteristics.
- Authors:
-
[2];
[2];
[1]
- Virginia Polytechnic Inst. and State Univ. (Virginia Tech), Blacksburg, VA (United States)
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Publication Date:
- Research Org.:
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division
- OSTI Identifier:
- 1503993
- Alternate Identifier(s):
- OSTI ID: 1637028
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Acta Materialia
- Additional Journal Information:
- Journal Volume: 168; Journal Issue: C; Journal ID: ISSN 1359-6454
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Shape memory; Zirconia; Granular materials; Martensitic transformation; Neutron diffraction
Citation Formats
Rauch, Hunter A., Chen, Yan, An, Ke, and Yu, Hang Z. In situ investigation of stress-induced martensitic transformation in granular shape memory ceramic packings. United States: N. p., 2019.
Web. doi:10.1016/j.actamat.2019.02.028.
Rauch, Hunter A., Chen, Yan, An, Ke, & Yu, Hang Z. In situ investigation of stress-induced martensitic transformation in granular shape memory ceramic packings. United States. https://doi.org/10.1016/j.actamat.2019.02.028
Rauch, Hunter A., Chen, Yan, An, Ke, and Yu, Hang Z. Fri .
"In situ investigation of stress-induced martensitic transformation in granular shape memory ceramic packings". United States. https://doi.org/10.1016/j.actamat.2019.02.028. https://www.osti.gov/servlets/purl/1503993.
@article{osti_1503993,
title = {In situ investigation of stress-induced martensitic transformation in granular shape memory ceramic packings},
author = {Rauch, Hunter A. and Chen, Yan and An, Ke and Yu, Hang Z.},
abstractNote = {Stress-induced martensitic transformation can occur in granular shape memory materials when individual particles experience high stresses and transform from a high-symmetry austenite phase to a low-symmetry martensite phase. This involves a highly heterogeneous distribution of the driving force and very low mechanical constraint for martensite nucleation, so the transformation behavior can be dramatically different from the well-documented case of monolithic solids. In this work, we investigate the stress-induced martensitic transformation in granular shape memory ceramic packings, which consist of single-crystal micro-particles of ZrO2-12 at%CeO2 and ZrO2-15 at%CeO2. Using in situ neutron diffraction, we study how the phase fraction, lattice strain, and integral peak broadness evolve during external loading, unloading, and subsequent heating. Several peculiar features are discovered, including (i) a continuous mode of transformation with a wide range of transformation loads, (ii) co-evolution of the packing structure, contact deformation, and martensitic transformation, and (iii) a strong correlation between the peak broadening and the transformed phase fraction. In addition, we show the first direct evidence of reversible stress-induced martensitic transformation in granular materials. We additionally discuss the mechanism for martensite nucleation and growth in granular packings and show how that leads to the observed transformation characteristics.},
doi = {10.1016/j.actamat.2019.02.028},
journal = {Acta Materialia},
number = C,
volume = 168,
place = {United States},
year = {Fri Feb 22 00:00:00 EST 2019},
month = {Fri Feb 22 00:00:00 EST 2019}
}
Free Publicly Available Full Text
Publisher's Version of Record
Other availability
Search WorldCat to find libraries that may hold this journal
Cited by: 16 works
Citation information provided by
Web of Science
Web of Science
Save to My Library
You must Sign In or Create an Account in order to save documents to your library.
Works referenced in this record:
A Perspective on Martensitic Nucleation
journal, August 1981
- Olson, G. B.; Cohen, M.
- Annual Review of Materials Science, Vol. 11, Issue 1
Size Effects on Magnetic Actuation in Ni-Mn-Ga Shape-Memory Alloys
journal, October 2010
- Dunand, David C.; Müllner, Peter
- Advanced Materials, Vol. 23, Issue 2, p. 216-232
Giant magnetic-field-induced strains in polycrystalline Ni–Mn–Ga foams
journal, September 2009
- Chmielus, M.; Zhang, X. X.; Witherspoon, C.
- Nature Materials, Vol. 8, Issue 11
Martensitic toughening of ceramics
journal, August 1990
- Kriven, Waltraud M.
- Materials Science and Engineering: A, Vol. 127, Issue 2
REVIEW-Transformation Toughening in Ceramics: Martensitic Transformations in Crack-Tip Stress Fields
journal, May 1980
- Evans, A. G.; Heuer, A. H.
- Journal of the American Ceramic Society, Vol. 63, Issue 5-6
Transformation Plasticity of CeO2-Stabilized Tetragonal Zirconia Polycrystals: II, Pseudoelasticity and Shape Memory Effect
journal, August 1988
- Reyes-Morel, Patricio E.; Cherng, Jyh-Shiarn; Chen, I-Wei
- Journal of the American Ceramic Society, Vol. 71, Issue 8
Ultralow-fatigue shape memory alloy films
journal, May 2015
- Chluba, C.; Ge, W.; Lima de Miranda, R.
- Science, Vol. 348, Issue 6238
Superelasticity in micro-scale shape memory ceramic particles
journal, January 2017
- Du, Zehui; Zeng, Xiao Mei; Liu, Qing
- Acta Materialia, Vol. 123
Superelasticity and fatigue in oligocrystalline shape memory alloy microwires
journal, January 2012
- Ueland, Stian M.; Schuh, Christopher A.
- Acta Materialia, Vol. 60, Issue 1
Shape Memory and Superelastic Ceramics at Small Scales
journal, September 2013
- Lai, A.; Du, Z.; Gan, C. L.
- Science, Vol. 341, Issue 6153
The martensitic transformation in ceramics — its role in transformation toughening
journal, January 2002
- Kelly, Patrick M.; Francis Rose, L. R.
- Progress in Materials Science, Vol. 47, Issue 5
Implications of Transformation Plasticity in ZrO2-Containing Ceramics: II, Elastic-Plastic Indentation
journal, March 1986
- Chen, I-Wei
- Journal of the American Ceramic Society, Vol. 69, Issue 3
Evolution of Percolating Force Chains in Compressed Granular Media
journal, October 2002
- Hidalgo, Raúl Cruz; Grosse, Christian U.; Kun, Ferenc
- Physical Review Letters, Vol. 89, Issue 20
Force Distributions in Dense Two-Dimensional Granular Systems
journal, July 1996
- Radjai, Farhang; Jean, Michel; Moreau, Jean-Jacques
- Physical Review Letters, Vol. 77, Issue 2
Contact force measurements and stress-induced anisotropy in granular materials
journal, June 2005
- Majmudar, T. S.; Behringer, R. P.
- Nature, Vol. 435, Issue 7045
Enhanced shape memory and superelasticity in small-volume ceramics: a perspective on the controlling factors
journal, October 2017
- Zeng, Xiaomei; Du, Zehui; Schuh, Christopher A.
- MRS Communications, Vol. 7, Issue 4
Synthesis of monodisperse CeO 2 -ZrO 2 particles exhibiting cyclic superelasticity over hundreds of cycles
journal, May 2017
- Du, Zehui; Ye, Pengcheng; Zeng, Xiao Mei
- Journal of the American Ceramic Society, Vol. 100, Issue 9
In-situ studies on martensitic transformation and high-temperature shape memory in small volume zirconia
journal, August 2017
- Zeng, Xiao Mei; Du, Zehui; Tamura, Nobumichi
- Acta Materialia, Vol. 134
Development of Superplastic Structural Ceramics
journal, September 1990
- Chen, I-Wei; Xue, Liang An
- Journal of the American Ceramic Society, Vol. 73, Issue 9
Granular shape memory ceramic packings
journal, June 2017
- Yu, Hang Z.; Hassani-Gangaraj, Mostafa; Du, Zehui
- Acta Materialia, Vol. 132
Neutron diffraction studies and multivariant simulations of shape memory alloys: Empirical texture development–mechanical response relations of martensitic nickel–titanium
journal, April 2011
- Stebner, Aaron; Gao, Xiujie; Brown, Donald W.
- Acta Materialia, Vol. 59, Issue 7
In Situ Neutron Diffraction Studies of Large Monotonic Deformations of Superelastic Nitinol
journal, May 2015
- Stebner, Aaron P.; Paranjape, Harshad M.; Clausen, Bjørn
- Shape Memory and Superelasticity, Vol. 1, Issue 2
Neutron Diffraction Study of Ferroelasticity in a 3 mol% Y2O3-ZrO2
journal, February 2001
- Ma, Yuxiang; Kisi, Erich H.; Kennedy, Shane J.
- Journal of the American Ceramic Society, Vol. 84, Issue 2
Stress-induced charge-ordering process in LiMn 2 O 4
journal, July 2016
- Chen, Yan; Yu, Dunji; An, Ke
- Materials Research Letters, Vol. 5, Issue 2
In situ, 3D characterization of the deformation mechanics of a superelastic NiTi shape memory alloy single crystal under multiscale constraint
journal, February 2018
- Paranjape, Harshad M.; Paul, Partha P.; Amin-Ahmadi, Behnam
- Acta Materialia, Vol. 144
First In Situ Lattice Strains Measurements Under Load at VULCAN
journal, October 2010
- An, Ke; Skorpenske, Harley D.; Stoica, Alexandru D.
- Metallurgical and Materials Transactions A, Vol. 42, Issue 1
Constitutive Model Calibration for Powder Compaction Using Instrumented Die Testing
journal, October 2011
- Shang, C.; Sinka, I. C.; Pan, J.
- Experimental Mechanics, Vol. 52, Issue 7
A profile refinement method for nuclear and magnetic structures
journal, June 1969
- Rietveld, H. M.
- Journal of Applied Crystallography, Vol. 2, Issue 2, p. 65-71
EXPGUI , a graphical user interface for GSAS
journal, April 2001
- Toby, Brian H.
- Journal of Applied Crystallography, Vol. 34, Issue 2
Transformation Plasticity of CeO2-Stabilized Tetragonal Zirconia Polycrystals: I, Stress Assistance and Autocatalysis
journal, May 1988
- Reyes-Morel, Patricio E.; Chen, I-Wei
- Journal of the American Ceramic Society, Vol. 71, Issue 5
Constitutive relations for the isotropic deformation of frictionless packings of polydisperse spheres
journal, October 2010
- Göncü, Fatih; Durán, Orencio; Luding, Stefan
- Comptes Rendus Mécanique, Vol. 338, Issue 10-11
Micro-macro correlations and anisotropy in granular assemblies under uniaxial loading and unloading
journal, April 2014
- Imole, Olukayode I.; Wojtkowski, Mateusz; Magnanimo, Vanessa
- Physical Review E, Vol. 89, Issue 4
Tetragonal-Monoclinic Phase Transition Enthalpy and Temperature of ZrO2-CeO2 Solid Solutions
journal, August 1995
- Yashima, Masatomo; Mitsuhashi, Takefumi; Takashina, Hiroyuki
- Journal of the American Ceramic Society, Vol. 78, Issue 8
Densification of Powders by Particle Deformation
journal, January 1983
- Fischmeister, H. F.; Arzt, E.
- Powder Metallurgy, Vol. 26, Issue 2
Hot-isostatic pressing diagrams: New developments
journal, December 1985
- Helle, A. S.; Easterling, K. E.; Ashby, M. F.
- Acta Metallurgica, Vol. 33, Issue 12
Creep, Ageing and Microstructural Change in Dense Granular Materials
journal, August 2003
- Bowman, Elisabetht; Soga, Kenichi
- Soils and Foundations, Vol. 43, Issue 4
Thermal Expansion Anisotropy of Ceria-Stabilized Tetragonal Zirconia
journal, October 1992
- Scardi, Paolo; Maggio, Rosa Di; Lutterotti, Luca
- Journal of the American Ceramic Society, Vol. 75, Issue 10
Ferroelastic domain switching in lead zirconate titanate measured by in situ neutron diffraction
journal, April 2007
- Jones, Jacob L.; Hoffman, Mark; Vogel, Sven C.
- Mechanics of Materials, Vol. 39, Issue 4
Direct observation of ferroelastic domain switching in polycrystalline BaTiO3 using in situ neutron diffraction
journal, April 2005
- Forrester, J. S.; Kisi, E. H.; Studer, A. J.
- Journal of the European Ceramic Society, Vol. 25, Issue 4
HREM investigation of interface between tetragonal and monoclinic phases in a ZrO2(3mol %Y2O3) ceramic
journal, January 1996
- Zhu, W. Z.; Lei, T. C.; Zhou, Y.
- Journal of Materials Science Letters, Vol. 15, Issue 1
A Localized Soft Mode Theory for Martensitic Transformations
journal, June 1973
- Clapp, P. C.
- Physica Status Solidi (b), Vol. 57, Issue 2
A localized soft mode model for the nucleation of thermoelastic martensitic transformation: Application to the β → 9r transformation
journal, July 1982
- GuÉnin, G.; Gobin, P. F.
- Metallurgical Transactions A, Vol. 13, Issue 7
Roles of dislocations and grain boundaries in martensite nucleation
journal, October 1986
- Kajiwara, S.
- Metallurgical Transactions A, Vol. 17, Issue 10
VESTA 3 for three-dimensional visualization of crystal, volumetric and morphology data
journal, October 2011
- Momma, Koichi; Izumi, Fujio
- Journal of Applied Crystallography, Vol. 44, Issue 6
Bimodal Character of Stress Transmission in Granular Packings
journal, January 1998
- Radjai, Farhang; Wolf, Dietrich E.; Jean, Michel
- Physical Review Letters, Vol. 80, Issue 1
On weak and strong contact force networks in granular materials
journal, August 2016
- Kruyt, N. P.
- International Journal of Solids and Structures, Vol. 92-93
Transition from many domain to single domain martensite morphology in small-scale shape memory alloys
journal, September 2013
- Ueland, Stian M.; Schuh, Christopher A.
- Acta Materialia, Vol. 61, Issue 15
Works referencing / citing this record:
Stress-induced phase transformation in shape memory ceramic nanoparticles
journal, December 2019
- Raut, V. S.; Glen, T. S.; Rauch, H. A.
- Journal of Applied Physics, Vol. 126, Issue 21