Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations

Burch, Matthew J.; Fancher, Chris M.; Patala, Srikanth; De Graef, Marc; Dickey, Elizabeth C.

doi:10.1016/j.ultramic.2016.11.013

Title: Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations

Abstract

A novel technique, which directly and nondestructively maps polar domains using electron backscatter diffraction (EBSD) is described and demonstrated. Through dynamical diffraction simulations and quantitative comparison to experimental EBSD patterns, the absolute orientation of a non-centrosymmetric crystal can be determined. With this information, the polar domains of a material can be mapped. The technique is demonstrated by mapping the non-ferroelastic, or 180°, ferroelectric domains in periodically poled LiNbO₃ single crystals. Furthermore, the authors demonstrate the possibility of mapping polarity using this technique in other polar materials system.

Authors:

Burch, Matthew J. ^[1]; Fancher, Chris M. ^[1]; Patala, Srikanth ^[1]; De Graef, Marc ^[2]; Dickey, Elizabeth C. ^[1]

North Carolina State Univ., Raleigh, NC (United States)
Carnegie Mellon Univ., Pittsburgh, PA (United States)

Publication Date:: Fri Nov 18 00:00:00 EST 2016

Research Org.:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)

Sponsoring Org.:: USDOE Office of Science (SC)

OSTI Identifier:: 1342702

Grant/Contract Number:: AC05-00OR22725

Resource Type:: Accepted Manuscript

Journal Name:: Ultramicroscopy

Additional Journal Information:: Journal Volume: 173; Journal Issue: C; Journal ID: ISSN 0304-3991

Publisher:: Elsevier

Country of Publication:: United States

Language:: English

Subject:: 36 MATERIALS SCIENCE; EBSD; ferroelectric; ferroelectric domain; electron backscatter diffraction

Citation Formats


                    Burch, Matthew J., Fancher, Chris M., Patala, Srikanth, De Graef, Marc, and Dickey, Elizabeth C. Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations.  United States: N. p., 2016. 
Web.  doi:10.1016/j.ultramic.2016.11.013.

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                    Burch, Matthew J., Fancher, Chris M., Patala, Srikanth, De Graef, Marc, & Dickey, Elizabeth C. Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations.  United States.  https://doi.org/10.1016/j.ultramic.2016.11.013

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                    Burch, Matthew J., Fancher, Chris M., Patala, Srikanth, De Graef, Marc, and Dickey, Elizabeth C. Fri .  
"Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations".  United States.  https://doi.org/10.1016/j.ultramic.2016.11.013.  https://www.osti.gov/servlets/purl/1342702.

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@article{osti_1342702,

  title        = {Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations},

  author       = {Burch, Matthew J. and Fancher, Chris M. and Patala, Srikanth and De Graef, Marc and Dickey, Elizabeth C.},

  abstractNote = {A novel technique, which directly and nondestructively maps polar domains using electron backscatter diffraction (EBSD) is described and demonstrated. Through dynamical diffraction simulations and quantitative comparison to experimental EBSD patterns, the absolute orientation of a non-centrosymmetric crystal can be determined. With this information, the polar domains of a material can be mapped. The technique is demonstrated by mapping the non-ferroelastic, or 180°, ferroelectric domains in periodically poled LiNbO3 single crystals. Furthermore, the authors demonstrate the possibility of mapping polarity using this technique in other polar materials system.},

  doi          = {10.1016/j.ultramic.2016.11.013},

  journal      = {Ultramicroscopy},

  number       = C,

  volume       = 173,

  place        = {United States},

  year         = {Fri Nov 18 00:00:00 EST 2016},

  month        = {Fri Nov 18 00:00:00 EST 2016}

}

Copy to clipboard

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https://doi.org/10.1016/j.ultramic.2016.11.013

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Absolute Structure from Scanning Electron Microscopy
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Title: Mapping 180° polar domains using electron backscatter diffraction and dynamical scattering simulations

Abstract

Citation Formats

Domain wall contributions to the properties of piezoelectric thin films journal, March 2007

Domain wall motion and its contribution to the dielectric and piezoelectric properties of lead zirconate titanate films journal, January 2001

Bichiral structure of ferroelectric domain walls driven by flexoelectricity journal, October 2012

Domain Structures and Phase Transitions in Barium Titanate journal, October 1949

Ferroelectricity, Domain Structure, and Phase Transitions of Barium Titanate journal, July 1950

Scanning Electron Microscopy and Transmission Electron Microscopy Study of Ferroelectric Domains in Doped BaTiO3 journal, August 1986

Domain Structure in the Tetragonal Phase of BaTiO 3 – from Bulk to Nanoparticles journal, January 2012

Friedel's Law in Electron Diffraction as Applied to the Study of Domain Structures in Non-Centrosymmetrical Crystals journal, July 1973

An exception to Friedel's law in electron diffraction journal, July 1950

Polarity characterization by anomalous x-ray dispersion of ZnO films and GaN lateral polar structures journal, January 2014

Simultaneous resonant x-ray diffraction measurement of polarization inversion and lattice strain in polycrystalline ferroelectrics journal, February 2016

Domain Wall Displacement is the Origin of Superior Permittivity and Piezoelectricity in BaTiO 3 at Intermediate Grain Sizes journal, September 2013

Applications of piezoresponse force microscopy in materials research: from inorganic ferroelectrics to biopiezoelectrics and beyond journal, January 2016

Raman and AFM piezoresponse study of dense BaTiO3 nanocrystalline ceramics journal, January 2005

Correlation of electron backscatter diffraction and piezoresponse force microscopy for the nanoscale characterization of ferroelectric domains in polycrystalline lead zirconate titanate journal, August 2010

A Review of Domain Modelling and Domain Imaging Techniques in Ferroelectric Crystals journal, February 2011

Imaging mechanism of piezoresponse force microscopy of ferroelectric surfaces journal, March 2002

Piezoresponse force microscopy (PFM) journal, November 2011

Exploring Local Electrostatic Effects with Scanning Probe Microscopy: Implications for Piezoresponse Force Microscopy and Triboelectricity journal, October 2014

Origin of internal field and visualization of 180° domains in congruent LiTaO 3 crystals journal, December 1996

Direct Observation of Antiparallel Domains During Polarization Reversal in Single-Crystal Barium Titanate journal, April 1959

Origin of the Visibility of the Antiparallel 180° Domains in Barium Titanate journal, November 1963

Chirality determination of quartz crystals using Electron Backscatter Diffraction journal, February 2015

Dynamical Electron Backscatter Diffraction Patterns. Part I: Pattern Simulations journal, June 2013

EBSD geometry in the SEM: simulation and representation journal, January 2005

A Dictionary Approach to Electron Backscatter Diffraction Indexing journal, June 2015

Domain configuration and equilibrium size of domains in BaTiO 3 ceramics journal, September 1980

Dielectric properties of fine‐grained barium titanate ceramics journal, August 1985

Dependence of GaN polarity on the parameters of the buffer layer grown by molecular beam epitaxy journal, June 2001

Polarity determination of GaN films by ion channeling and convergent beam electron diffraction journal, October 1996

Orientation mapping of nanostructured materials using transmission Kikuchi diffraction in the scanning electron microscope journal, September 2012

Transmission Kikuchi diffraction and transmission electron forescatter imaging of electropolished and FIB manufactured TEM specimens journal, June 2015

Transmission EBSD from 10 nm domains in a scanning electron microscope: TRANSMISSION EBSD IN THE SEM journal, November 2011

Absolute Structure from Scanning Electron Microscopy journal, March 2020

Unambiguous Determination of Local Orientations of Polycrystalline CuInSe 2 Thin Films via Dictionary‐Based Indexing journal, March 2019

Dictionary Indexing of Electron Back-Scatter Diffraction Patterns: a Hands-On Tutorial journal, May 2019

Absolute Structure from Scanning Electron Microscopy journal, March 2020

Domain wall contributions to the properties of piezoelectric thin films
journal, March 2007

Domain wall motion and its contribution to the dielectric and piezoelectric properties of lead zirconate titanate films
journal, January 2001

Bichiral structure of ferroelectric domain walls driven by flexoelectricity
journal, October 2012

Domain Structures and Phase Transitions in Barium Titanate
journal, October 1949

Ferroelectricity, Domain Structure, and Phase Transitions of Barium Titanate
journal, July 1950

Scanning Electron Microscopy and Transmission Electron Microscopy Study of Ferroelectric Domains in Doped BaTiO3
journal, August 1986

Domain Structure in the Tetragonal Phase of BaTiO ₃ – from Bulk to Nanoparticles
journal, January 2012

Friedel's Law in Electron Diffraction as Applied to the Study of Domain Structures in Non-Centrosymmetrical Crystals
journal, July 1973

An exception to Friedel's law in electron diffraction
journal, July 1950

Polarity characterization by anomalous x-ray dispersion of ZnO films and GaN lateral polar structures
journal, January 2014

Simultaneous resonant x-ray diffraction measurement of polarization inversion and lattice strain in polycrystalline ferroelectrics
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Domain Wall Displacement is the Origin of Superior Permittivity and Piezoelectricity in BaTiO ₃ at Intermediate Grain Sizes
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Applications of piezoresponse force microscopy in materials research: from inorganic ferroelectrics to biopiezoelectrics and beyond
journal, January 2016

Raman and AFM piezoresponse study of dense BaTiO3 nanocrystalline ceramics
journal, January 2005

Correlation of electron backscatter diffraction and piezoresponse force microscopy for the nanoscale characterization of ferroelectric domains in polycrystalline lead zirconate titanate
journal, August 2010

A Review of Domain Modelling and Domain Imaging Techniques in Ferroelectric Crystals
journal, February 2011

Imaging mechanism of piezoresponse force microscopy of ferroelectric surfaces
journal, March 2002

Piezoresponse force microscopy (PFM)
journal, November 2011

Exploring Local Electrostatic Effects with Scanning Probe Microscopy: Implications for Piezoresponse Force Microscopy and Triboelectricity
journal, October 2014

Origin of internal field and visualization of 180° domains in congruent LiTaO ₃ crystals
journal, December 1996

Direct Observation of Antiparallel Domains During Polarization Reversal in Single-Crystal Barium Titanate
journal, April 1959

Origin of the Visibility of the Antiparallel 180° Domains in Barium Titanate
journal, November 1963

Chirality determination of quartz crystals using Electron Backscatter Diffraction
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Dynamical Electron Backscatter Diffraction Patterns. Part I: Pattern Simulations
journal, June 2013

EBSD geometry in the SEM: simulation and representation
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A Dictionary Approach to Electron Backscatter Diffraction Indexing
journal, June 2015

Domain configuration and equilibrium size of domains in BaTiO ₃ ceramics
journal, September 1980

Dielectric properties of fine‐grained barium titanate ceramics
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Dependence of GaN polarity on the parameters of the buffer layer grown by molecular beam epitaxy
journal, June 2001

Polarity determination of GaN films by ion channeling and convergent beam electron diffraction
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Transmission Kikuchi diffraction and transmission electron forescatter imaging of electropolished and FIB manufactured TEM specimens
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journal, May 2019

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