Fly scan apparatus for high pressure research using diamond anvil cells

Smith, Jesse S.; Rod, Eric A.; Shen, Guoyin

doi:10.1063/1.5057445

Title: Fly scan apparatus for high pressure research using diamond anvil cells

Abstract

In this paper, the hardware and software used to execute fly scans at Sector 16 of the Advanced Photon Source is described. The system design and capabilities address dimensions and time scales relevant to samples in high pressure diamond anvil cells. The time required for routine sample positioning and centering is significantly reduced and, more importantly, the time savings associated with fly scanning makes it feasible for users to routinely generate two-dimensional x-ray transmission and x-ray diffraction maps. Consequently, this facilitates an important shift in high pressure research as experimentalists embrace the study of heterogeneous and minute sample volumes in the diamond anvil cell.

Authors:

^[1]; Rod, Eric A. ^[1]; Shen, Guoyin ^[1]

Argonne National Lab. (ANL), Argonne, IL (United States)

Publication Date:: Tue Jan 29 00:00:00 EST 2019

Research Org.:: Argonne National Lab. (ANL), Argonne, IL (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division; USDOE National Nuclear Security Administration (NNSA)

OSTI Identifier:: 1494058

Grant/Contract Number:: AC02-06CH11357; FG02-99ER45775

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 90; Journal Issue: 1; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 47 OTHER INSTRUMENTATION

Citation Formats


                    Smith, Jesse S., Rod, Eric A., and Shen, Guoyin. Fly scan apparatus for high pressure research using diamond anvil cells.  United States: N. p., 2019. 
Web.  doi:10.1063/1.5057445.

Copy to clipboard


                    Smith, Jesse S., Rod, Eric A., & Shen, Guoyin. Fly scan apparatus for high pressure research using diamond anvil cells.  United States.  https://doi.org/10.1063/1.5057445

Copy to clipboard


                    Smith, Jesse S., Rod, Eric A., and Shen, Guoyin. Tue .  
"Fly scan apparatus for high pressure research using diamond anvil cells".  United States.  https://doi.org/10.1063/1.5057445.  https://www.osti.gov/servlets/purl/1494058.

Copy to clipboard


                    
@article{osti_1494058,

  title        = {Fly scan apparatus for high pressure research using diamond anvil cells},

  author       = {Smith, Jesse S. and Rod, Eric A. and Shen, Guoyin},

  abstractNote = {In this paper, the hardware and software used to execute fly scans at Sector 16 of the Advanced Photon Source is described. The system design and capabilities address dimensions and time scales relevant to samples in high pressure diamond anvil cells. The time required for routine sample positioning and centering is significantly reduced and, more importantly, the time savings associated with fly scanning makes it feasible for users to routinely generate two-dimensional x-ray transmission and x-ray diffraction maps. Consequently, this facilitates an important shift in high pressure research as experimentalists embrace the study of heterogeneous and minute sample volumes in the diamond anvil cell.},

  doi          = {10.1063/1.5057445},

  journal      = {Review of Scientific Instruments},

  number       = 1,

  volume       = 90,

  place        = {United States},

  year         = {Tue Jan 29 00:00:00 EST 2019},

  month        = {Tue Jan 29 00:00:00 EST 2019}

}

Copy to clipboard

Journal Article:

Free Publicly Available Full Text

Accepted Manuscript (DOE)

Publisher's Version of Record

https://doi.org/10.1063/1.5057445

Other availability

Search WorldCat to find libraries that may hold this journal

Citation Metrics:

Cited by: 6 works

Citation information provided by
Web of Science

Save / Share:

Export Metadata

Save to My Library

Works referenced in this record:

Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar
journal, September 2018

Jenei, Zs.; O’Bannon, E. F.; Weir, S. T.
Nature Communications, Vol. 9, Issue 1
DOI: 10.1038/s41467-018-06071-x

Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression
journal, July 2015

Smith, Jesse S.; Sinogeikin, Stanislav V.; Lin, Chuanlong
Review of Scientific Instruments, Vol. 86, Issue 7
DOI: 10.1063/1.4926887

Preface: High-pressure studies with x-rays
journal, July 2015

Shen, Guoyin; Sinogeikin, Stanislav
Review of Scientific Instruments, Vol. 86, Issue 7
DOI: 10.1063/1.4926899

Diamond anvil cell behavior up to 4 Mbar
journal, February 2018

Li, Bing; Ji, Cheng; Yang, Wenge
Proceedings of the National Academy of Sciences, Vol. 115, Issue 8
DOI: 10.1073/pnas.1721425115

Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions
journal, January 2018

Moore, Samuel L.; Samudrala, Gopi K.; Catledge, Shane A.
Scientific Reports, Vol. 8, Issue 1
DOI: 10.1038/s41598-018-19915-9

Selected techniques in diamond anvil cell crystallography: centring samples using X-ray transmission and rocking powder samples to improve X-ray diffraction image quality
journal, November 2008

Smith, Jesse S.; Desgreniers, Serge
Journal of Synchrotron Radiation, Vol. 16, Issue 1
DOI: 10.1107/s0909049508030859

Covalency is Frustrating: La ₂ Sn ₂ O ₇ and the Nature of Bonding in Pyrochlores under High Pressure–Temperature Conditions
journal, July 2018

Childs, Christian; Lawler, Keith V.; Hector, Andrew L.
Inorganic Chemistry, Vol. 57, Issue 24
DOI: 10.1021/acs.inorgchem.8b01419

Toroidal diamond anvil cell for detailed measurements under extreme static pressures
journal, July 2018

Dewaele, Agnès; Loubeyre, Paul; Occelli, Florent
Nature Communications, Vol. 9, Issue 1
DOI: 10.1038/s41467-018-05294-2

Nanoprobe measurements of materials at megabar pressures
journal, March 2010

Wang, L.; Ding, Y.; Yang, W.
Proceedings of the National Academy of Sciences, Vol. 107, Issue 14
DOI: 10.1073/pnas.1001141107

Terapascal static pressure generation with ultrahigh yield strength nanodiamond
journal, July 2016

Dubrovinskaia, Natalia; Dubrovinsky, Leonid; Solopova, Natalia A.
Science Advances, Vol. 2, Issue 7
DOI: 10.1126/sciadv.1600341

High pressure studies using two-stage diamond micro-anvils grown by chemical vapor deposition
journal, May 2015

Vohra, Yogesh K.; Samudrala, Gopi K.; Moore, Samuel L.
High Pressure Research, Vol. 35, Issue 3
DOI: 10.1080/08957959.2015.1053881

Implementation of micro-ball nanodiamond anvils for high-pressure studies above 6 Mbar
journal, January 2012

Dubrovinsky, Leonid; Dubrovinskaia, Natalia; Prakapenka, Vitali B.
Nature Communications, Vol. 3, Issue 1
DOI: 10.1038/ncomms2160

Terapascal static pressure generation with ultrahigh yield strength nanodiamond
text, January 2016

Dubrovinskaia, Natalia; Dubrovinsky, Leonid; Solopova, Natalia A.
Karlsruhe
DOI: 10.5445/ir/1000059582

Works referencing / citing this record:

Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments
journal, February 2019

Hrubiak, Rostislav; Smith, Jesse S.; Shen, Guoyin
Review of Scientific Instruments, Vol. 90, Issue 2
DOI: 10.1063/1.5057518

Similar Records in DOE PAGES and OSTI.GOV collections:

Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments

Journal Article Hrubiak, Rostislav ; Smith, Jesse S. ; Shen, Guoyin - Review of Scientific Instruments

We have designed and implemented a new experimental system for fast mapping of crystal structures and other structural features of materials under high pressure at the High Pressure Collaborative Access Team, Sector 16 of the Advanced Photon Source. The system utilizes scanning X-ray diffraction microscopy (SXDM) and is optimized for use with diamond anvil cell devices. In SXDM, the X-ray diffraction (XRD) is collected in a forward scattering geometry from points on a two-dimensional grid by fly-scanning the sample with respect to a micro-focused X-ray beam. The recording of XRD is made during the continuous motion of the sample usingmore »« less
Cited by 13
https://doi.org/10.1063/1.5057518

Full Text Available
A scanning angle energy-dispersive X-ray diffraction technique for high-pressure structure studies in diamond anvil cells

Journal Article Yang, Wenge ; Shen, Guoyin ; Wang, Yanbin ; ... - High Pressure Res.

A scanning angle diffraction technique with an energy-dispersive solid-state detector (SSD) and white synchrotron radiation has been developed for high-pressure structure studies in diamond anvil cells (DACs). This technique is similar to the CAESAR technique [Y. Wang, T. Uchida, R. Von Dreele, M.L. Rivers, N. Nishiyama, K. Funakoshi, A. Nozawa, and H. Kaneko, A new technique for angle-dispersive powder diffraction using an energy-dispersive setup and synchrotron radiation, J. Appl. Cryst. 37 (2004), p. 947] developed for large-volume presses, but extended to DAC applications with high spatial resolution. The main feature of the technique is the well-defined collimation in the beammore »« less
https://doi.org/10.1080/08957950802246522
Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions

Journal Article Moore, Samuel L. ; Samudrala, Gopi K. ; Catledge, Shane A. ; ... - Scientific Reports

Early stage nucleation morphologies of spatially localized nanocrystalline diamond (NCD) micro-anvils grown on (100)-oriented single crystal diamond (SCD) anvil surfaces were analyzed and investigated for applications in high pressure studies on materials. NCD was grown on SCD using Microwave Plasma Chemical Vapor Deposition (MPCVD) for brief time intervals ranging from 1-15 minutes. Early stage film morphologies were characterized using scanning electron microscopy (SEM) and Raman spectroscopy and were compared to films grown for several hours. Rapid nucleation and growth of NCD on SCD is demonstrated without any pre-growth seeding of the substrate surface. As grown NCD diamond micro-anvils on SCDmore »« less
Cited by 10
https://doi.org/10.1038/s41598-018-19915-9

Full Text Available
The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team

Journal Article Hrubiak, Rostislav ; Sinogeikin, Stanislav ; Rod, Eric ; ... - Review of Scientific Instruments

We report we have designed and constructed a new system for micro-machining parts and sample assemblies used for diamond anvil cells and general user operations at the High Pressure Collaborative Access Team, sector 16 of the Advanced Photon Source. The new micro-machining system uses a pulsed laser of 400 ps pulse duration, ablating various materials without thermal melting, thus leaving a clean edge. With optics designed for a tight focus, the system can machine holes any size larger than 3 μm in diameter. Unlike a standard electrical discharge machining drill, the new laser system allows micro-machining of non-conductive materials suchmore »« less
Cited by 59
https://doi.org/10.1063/1.4926889

Full Text Available
Graphite resistive heated diamond anvil cell for simultaneous high-pressure and high-temperature diffraction experiments

Journal Article Hwang, Huijeong ; Bang, Yoonah ; Choi, Jinhyuk ; ... - Review of Scientific Instruments

High-pressure and high-temperature experiments using a resistively heated diamond anvil cell have the advantage of heating samples homogeneously with precise temperature control. Here, we present the design and performance of a graphite resistive heated diamond anvil cell (GRHDAC) setup for powder and single-crystal x-ray diffraction experiments developed at the Extreme Conditions Beamline (P02.2) at PETRA III, Hamburg, Germany. In the GRHDAC, temperatures up to 2000 K can be generated at high pressures by placing it in a water-cooled vacuum chamber. Temperature estimates from thermocouple measurements are within +/–35 K at the sample position up to 800 K and within +90more »« less
https://doi.org/10.1063/5.0132981

Similar Records

Title: Fly scan apparatus for high pressure research using diamond anvil cells

Abstract

Citation Formats

Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar journal, September 2018

Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression journal, July 2015

Preface: High-pressure studies with x-rays journal, July 2015

Diamond anvil cell behavior up to 4 Mbar journal, February 2018

Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions journal, January 2018

Selected techniques in diamond anvil cell crystallography: centring samples using X-ray transmission and rocking powder samples to improve X-ray diffraction image quality journal, November 2008

Covalency is Frustrating: La 2 Sn 2 O 7 and the Nature of Bonding in Pyrochlores under High Pressure–Temperature Conditions journal, July 2018

Toroidal diamond anvil cell for detailed measurements under extreme static pressures journal, July 2018

Nanoprobe measurements of materials at megabar pressures journal, March 2010

Terapascal static pressure generation with ultrahigh yield strength nanodiamond journal, July 2016

High pressure studies using two-stage diamond micro-anvils grown by chemical vapor deposition journal, May 2015

Implementation of micro-ball nanodiamond anvils for high-pressure studies above 6 Mbar journal, January 2012

Terapascal static pressure generation with ultrahigh yield strength nanodiamond text, January 2016

Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments journal, February 2019

Single crystal toroidal diamond anvils for high pressure experiments beyond 5 megabar
journal, September 2018

Developments in time-resolved high pressure x-ray diffraction using rapid compression and decompression
journal, July 2015

Preface: High-pressure studies with x-rays
journal, July 2015

Diamond anvil cell behavior up to 4 Mbar
journal, February 2018

Rapid Growth of Nanocrystalline Diamond on Single Crystal Diamond for Studies on Materials under Extreme Conditions
journal, January 2018

Selected techniques in diamond anvil cell crystallography: centring samples using X-ray transmission and rocking powder samples to improve X-ray diffraction image quality
journal, November 2008

Covalency is Frustrating: La ₂ Sn ₂ O ₇ and the Nature of Bonding in Pyrochlores under High Pressure–Temperature Conditions
journal, July 2018

Toroidal diamond anvil cell for detailed measurements under extreme static pressures
journal, July 2018

Nanoprobe measurements of materials at megabar pressures
journal, March 2010

Terapascal static pressure generation with ultrahigh yield strength nanodiamond
journal, July 2016

High pressure studies using two-stage diamond micro-anvils grown by chemical vapor deposition
journal, May 2015

Implementation of micro-ball nanodiamond anvils for high-pressure studies above 6 Mbar
journal, January 2012

Terapascal static pressure generation with ultrahigh yield strength nanodiamond
text, January 2016

Multimode scanning X-ray diffraction microscopy for diamond anvil cell experiments
journal, February 2019