The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team

Hrubiak, Rostislav; Sinogeikin, Stanislav; Rod, Eric; Shen, Guoyin

doi:10.1063/1.4926889

Title: The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team

Abstract

We report we have designed and constructed a new system for micro-machining parts and sample assemblies used for diamond anvil cells and general user operations at the High Pressure Collaborative Access Team, sector 16 of the Advanced Photon Source. The new micro-machining system uses a pulsed laser of 400 ps pulse duration, ablating various materials without thermal melting, thus leaving a clean edge. With optics designed for a tight focus, the system can machine holes any size larger than 3 μm in diameter. Unlike a standard electrical discharge machining drill, the new laser system allows micro-machining of non-conductive materials such as: amorphous boron and silicon carbide gaskets, diamond, oxides, and other materials including organic materials such as polyimide films (i.e., Kapton). An important feature of the new system is the use of gas-tight or gas-flow environmental chambers which allow the laser micro-machining to be done in a controlled (e.g., inert gas) atmosphere to prevent oxidation and other chemical reactions in air sensitive materials. The gas-tight workpiece enclosure is also useful for machining materials with known health risks (e.g., beryllium). Specialized control software with a graphical interface enables micro-machining of custom 2D and 3D shapes. The laser-machining system was designed inmore »« less

Authors:

Hrubiak, Rostislav ^[1]; Sinogeikin, Stanislav ^[1]; Rod, Eric ^[1]; Shen, Guoyin ^[1]

Carnegie Inst. of Washington, Argonne, IL (United States). High Pressure Collaborative Access Team (HPCAT)

Publication Date:: Mon Jul 20 00:00:00 EDT 2015

Research Org.:: Argonne National Laboratory (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF)

OSTI Identifier:: 1203737

Alternate Identifier(s):: OSTI ID: 1228680

Grant/Contract Number:: NA0001974; FG02-99ER45775; AC02-06CH11357

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 86; Journal Issue: 7; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: ENGLISH

Subject:: 47 OTHER INSTRUMENTATION; Oxides; Mechanical instruments; Physics of gases; Lasers; Chemical elements; Organic materials; Diamond anvil cells; Carbides; Polymers; Machining

Citation Formats


                    Hrubiak, Rostislav, Sinogeikin, Stanislav, Rod, Eric, and Shen, Guoyin. The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team.  United States: N. p., 2015. 
Web.  doi:10.1063/1.4926889.

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                    Hrubiak, Rostislav, Sinogeikin, Stanislav, Rod, Eric, & Shen, Guoyin. The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team.  United States.  https://doi.org/10.1063/1.4926889

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                    Hrubiak, Rostislav, Sinogeikin, Stanislav, Rod, Eric, and Shen, Guoyin. Mon .  
"The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team".  United States.  https://doi.org/10.1063/1.4926889.  https://www.osti.gov/servlets/purl/1203737.

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@article{osti_1203737,

  title        = {The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team},

  author       = {Hrubiak, Rostislav and Sinogeikin, Stanislav and Rod, Eric and Shen, Guoyin},

  abstractNote = {We report we have designed and constructed a new system for micro-machining parts and sample assemblies used for diamond anvil cells and general user operations at the High Pressure Collaborative Access Team, sector 16 of the Advanced Photon Source. The new micro-machining system uses a pulsed laser of 400 ps pulse duration, ablating various materials without thermal melting, thus leaving a clean edge. With optics designed for a tight focus, the system can machine holes any size larger than 3 μm in diameter. Unlike a standard electrical discharge machining drill, the new laser system allows micro-machining of non-conductive materials such as: amorphous boron and silicon carbide gaskets, diamond, oxides, and other materials including organic materials such as polyimide films (i.e., Kapton). An important feature of the new system is the use of gas-tight or gas-flow environmental chambers which allow the laser micro-machining to be done in a controlled (e.g., inert gas) atmosphere to prevent oxidation and other chemical reactions in air sensitive materials. The gas-tight workpiece enclosure is also useful for machining materials with known health risks (e.g., beryllium). Specialized control software with a graphical interface enables micro-machining of custom 2D and 3D shapes. The laser-machining system was designed in a Class 1 laser enclosure, i.e., it includes laser safety interlocks and computer controls and allows for routine operation. Though initially designed mainly for machining of the diamond anvil cell gaskets, the laser-machining system has since found many other micro-machining applications, several of which are presented here.},

  doi          = {10.1063/1.4926889},

  journal      = {Review of Scientific Instruments},

  number       = 7,

  volume       = 86,

  place        = {United States},

  year         = {Mon Jul 20 00:00:00 EDT 2015},

  month        = {Mon Jul 20 00:00:00 EDT 2015}

}

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Works referencing / citing this record:

Pressure-Induced Bandgap Optimization in Lead-Based Perovskites with Prolonged Carrier Lifetime and Ambient Retainability
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Ultrahigh-pressure isostructural electronic transitions in hydrogen
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Room-temperature compression and equation of state of body-centered cubic zirconium
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Pigott, Jeffrey S.; Velisavljevic, Nenad; Moss, Eric K.
Journal of Physics: Condensed Matter, Vol. 32, Issue 12
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Venture into Water’s No Man’s Land: Structural Transformations of Solid $H_{2} O$ under Rapid Compression and Decompression
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In situ quantitative study of plastic strain-induced phase transformations under high pressure: Example for ultra-pure Zr
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Title: The laser micro-machining system for diamond anvil cell experiments and general precision machining applications at the High Pressure Collaborative Access Team

Abstract

Citation Formats

Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures journal, June 2006

Modeling and simulation on long pulse laser drilling processing journal, June 2014

Melt ejection during laser drilling of metals journal, September 2003

High-pressure x-ray diffraction studies on the structure of liquid silicate using a Paris–Edinburgh type large volume press journal, January 2011

Laser drilling velocity in metals journal, December 1976

Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature journal, January 2001

Miniature diamond anvil pressure cell for single crystal x‐ray diffraction studies journal, February 1974

A portable laser heating microscope for high pressure research journal, March 2010

High-pressure powder X-ray diffraction at the turn of the century journal, December 2002

Laser drilling mechanics journal, October 1974

Molecular dynamics simulation study of deep hole drilling in iron by ultrashort laser pulses journal, April 2006

Overview of polycapillary X-ray optics journal, June 2002

Focusing Polycapillary Optics and Their Applications journal, January 2010

Pressure-Induced Bandgap Optimization in Lead-Based Perovskites with Prolonged Carrier Lifetime and Ambient Retainability journal, December 2016

Discovery of Cu 3 Pb journal, September 2018

Microstructures define melting of molybdenum at high pressures journal, March 2017

Ultrahigh-pressure isostructural electronic transitions in hydrogen journal, September 2019

A CO 2 laser heating system for in situ high pressure-temperature experiments at HPCAT journal, August 2018

In situ x-ray diffraction study of polyamorphism in H 2 O under isothermal compression and decompression journal, June 2019

High pressure-induced distortion in face-centered cubic phase of thallium journal, September 2016

Experimental evidence of low-density liquid water upon rapid decompression journal, February 2018

Room-temperature compression and equation of state of body-centered cubic zirconium journal, December 2019

High-pressure studies with x-rays using diamond anvil cells journal, November 2016

Venture into Water’s No Man’s Land: Structural Transformations of Solid H 2 O under Rapid Compression and Decompression journal, November 2018

Postaragonite phases of CaCO 3 at lower mantle pressures journal, January 2018

Probing disorder in high-pressure cubic tin (IV) oxide: a combined X-ray diffraction and absorption study journal, May 2019

Discovery of Cu 3 Pb journal, September 2018

Postaragonite phases of CaCO3 at lower mantle pressures text, January 2018

In situ quantitative study of plastic strain-induced phase transformations under high pressure: Example for ultra-pure Zr journal, September 2020

Experimental evidence of low-density liquid water upon rapid decompression journal, February 2018

Spin Quenching Assisted by a Strongly Anisotropic Compression Behavior in MnP text, January 2017

Bond strengthening in dense H2O and implications to planetary composition preprint, January 2019

In situ quantitative study of plastic strain-induced phase transformations under high pressure: Example for ultra-pure Zr preprint, January 2019

Evidence for a pressure-induced antiferromagnetic quantum critical point in intermediate valence UTe2 text, January 2020

Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures
journal, June 2006

Modeling and simulation on long pulse laser drilling processing
journal, June 2014

Melt ejection during laser drilling of metals
journal, September 2003

High-pressure x-ray diffraction studies on the structure of liquid silicate using a Paris–Edinburgh type large volume press
journal, January 2011

Laser drilling velocity in metals
journal, December 1976

Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature
journal, January 2001

Miniature diamond anvil pressure cell for single crystal x‐ray diffraction studies
journal, February 1974

A portable laser heating microscope for high pressure research
journal, March 2010

High-pressure powder X-ray diffraction at the turn of the century
journal, December 2002

Laser drilling mechanics
journal, October 1974

Molecular dynamics simulation study of deep hole drilling in iron by ultrashort laser pulses
journal, April 2006

Overview of polycapillary X-ray optics
journal, June 2002

Focusing Polycapillary Optics and Their Applications
journal, January 2010

Pressure-Induced Bandgap Optimization in Lead-Based Perovskites with Prolonged Carrier Lifetime and Ambient Retainability
journal, December 2016

Discovery of Cu ₃ Pb
journal, September 2018

Microstructures define melting of molybdenum at high pressures
journal, March 2017

Ultrahigh-pressure isostructural electronic transitions in hydrogen
journal, September 2019

A CO ₂ laser heating system for in situ high pressure-temperature experiments at HPCAT
journal, August 2018

In situ x-ray diffraction study of polyamorphism in H ₂ O under isothermal compression and decompression
journal, June 2019

High pressure-induced distortion in face-centered cubic phase of thallium
journal, September 2016

Experimental evidence of low-density liquid water upon rapid decompression
journal, February 2018

Room-temperature compression and equation of state of body-centered cubic zirconium
journal, December 2019

High-pressure studies with x-rays using diamond anvil cells
journal, November 2016

Venture into Water’s No Man’s Land: Structural Transformations of Solid $H_{2} O$ under Rapid Compression and Decompression
journal, November 2018

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journal, January 2018

Probing disorder in high-pressure cubic tin (IV) oxide: a combined X-ray diffraction and absorption study
journal, May 2019

Discovery of Cu ₃ Pb
journal, September 2018

Postaragonite phases of CaCO3 at lower mantle pressures
text, January 2018

In situ quantitative study of plastic strain-induced phase transformations under high pressure: Example for ultra-pure Zr
journal, September 2020

Experimental evidence of low-density liquid water upon rapid decompression
journal, February 2018

Spin Quenching Assisted by a Strongly Anisotropic Compression Behavior in MnP
text, January 2017

Bond strengthening in dense H2O and implications to planetary composition
preprint, January 2019

In situ quantitative study of plastic strain-induced phase transformations under high pressure: Example for ultra-pure Zr
preprint, January 2019

Evidence for a pressure-induced antiferromagnetic quantum critical point in intermediate valence UTe2
text, January 2020