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Title: New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team

Abstract

An overview of the in situ laser heating system at the High Pressure Collaborative Access Team, with emphasis on newly developed capabilities, is presented. Since its establishment at the beamline 16-ID-B a decade ago, laser-heated diamond anvil cell coupled with in situ synchrotron x-ray diffraction has been widely used for studying the structural properties of materials under simultaneous high pressure and high temperature conditions. Recent developments in both continuous-wave and modulated heating techniques have been focusing on resolving technical issues of the most challenging research areas. Furthermore, the new capabilities have demonstrated clear benefits and provide new opportunities in research areas including high-pressure melting, pressure-temperature-volume equations of state, chemical reaction, and time resolved studies.

Authors:
 [1];  [1];  [1];  [2];  [1]
  1. Carnegie Institution of Washington, Argonne, IL (United States)
  2. Carnegie Institution of Washington, Washington, D.C. (United States)
Publication Date:
Research Org.:
Carnegie Institution of Washington, Washington, D.C. (United States); Carnegie Inst. of Science, Argonne, IL (United States)
Sponsoring Org.:
USDOE National Nuclear Security Administration (NNSA)
OSTI Identifier:
1335884
Alternate Identifier(s):
OSTI ID: 1228679
Grant/Contract Number:  
NA0002006; AC02-06CH11357; FG02-99ER45775; NA0001974
Resource Type:
Accepted Manuscript
Journal Name:
Review of Scientific Instruments
Additional Journal Information:
Journal Volume: 86; Journal Issue: 7; Journal ID: ISSN 0034-6748
Publisher:
American Institute of Physics (AIP)
Country of Publication:
United States
Language:
English
Subject:
43 PARTICLE ACCELERATORS; 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats

Meng, Yue, Hrubiak, Rostislav, Rod, Eric, Boehler, Reinhard, and Shen, Guoyin. New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team. United States: N. p., 2015. Web. doi:10.1063/1.4926895.
Meng, Yue, Hrubiak, Rostislav, Rod, Eric, Boehler, Reinhard, & Shen, Guoyin. New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team. United States. doi:10.1063/1.4926895.
Meng, Yue, Hrubiak, Rostislav, Rod, Eric, Boehler, Reinhard, and Shen, Guoyin. Fri . "New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team". United States. doi:10.1063/1.4926895. https://www.osti.gov/servlets/purl/1335884.
@article{osti_1335884,
title = {New developments in laser-heated diamond anvil cell with in situ synchrotron x-ray diffraction at High Pressure Collaborative Access Team},
author = {Meng, Yue and Hrubiak, Rostislav and Rod, Eric and Boehler, Reinhard and Shen, Guoyin},
abstractNote = {An overview of the in situ laser heating system at the High Pressure Collaborative Access Team, with emphasis on newly developed capabilities, is presented. Since its establishment at the beamline 16-ID-B a decade ago, laser-heated diamond anvil cell coupled with in situ synchrotron x-ray diffraction has been widely used for studying the structural properties of materials under simultaneous high pressure and high temperature conditions. Recent developments in both continuous-wave and modulated heating techniques have been focusing on resolving technical issues of the most challenging research areas. Furthermore, the new capabilities have demonstrated clear benefits and provide new opportunities in research areas including high-pressure melting, pressure-temperature-volume equations of state, chemical reaction, and time resolved studies.},
doi = {10.1063/1.4926895},
journal = {Review of Scientific Instruments},
number = 7,
volume = 86,
place = {United States},
year = {2015},
month = {7}
}

Journal Article:
Free Publicly Available Full Text
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Cited by: 21 works
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Works referenced in this record:

The birth and development of laser heating in diamond anvil cells
journal, January 2001

  • Bassett, William A.
  • Review of Scientific Instruments, Vol. 72, Issue 2
  • DOI: 10.1063/1.1343861

Silicate perovskite from phase transformations of pyrope-garnet at high pressure and temperature
journal, October 1974


Structure of Liquid Iron at Pressures up to 58 GPa
journal, May 2004


Stability and crystal structure of MgSiO 3 perovskite to the core-mantle boundary : STABILITY OF MgSiO
journal, May 2004

  • Shim, S. -H.; Duffy, T. S.; Jeanloz, R.
  • Geophysical Research Letters, Vol. 31, Issue 10
  • DOI: 10.1029/2004GL019639

Discovery of the recoverable high-pressure iron oxide Fe4O5
journal, October 2011

  • Lavina, B.; Dera, P.; Kim, E.
  • Proceedings of the National Academy of Sciences, Vol. 108, Issue 42
  • DOI: 10.1073/pnas.1107573108

Disproportionation of (Mg,Fe)SiO3 perovskite in Earth's deep lower mantle
journal, May 2014


Iron-rich silicates in the Earth's D'' layer
journal, June 2005

  • Mao, W. L.; Meng, Y.; Shen, G.
  • Proceedings of the National Academy of Sciences, Vol. 102, Issue 28
  • DOI: 10.1073/pnas.0503737102

Advanced flat top laser heating system for high pressure research at GSECARS: application to the melting behavior of germanium
journal, September 2008


Measurement of temperature distributions across laser heated samples by multispectral imaging radiometry
journal, January 2008

  • Campbell, Andrew J.
  • Review of Scientific Instruments, Vol. 79, Issue 1
  • DOI: 10.1063/1.2827513

Metastable high-pressure transformations of orthoferrosilite Fs82
journal, August 2013

  • Dera, Przemyslaw; Finkelstein, Gregory J.; Duffy, Thomas S.
  • Physics of the Earth and Planetary Interiors, Vol. 221
  • DOI: 10.1016/j.pepi.2013.06.006

Effects of Fe-enrichment on the equation of state and stability of (Mg,Fe)SiO3 perovskite
journal, January 2013

  • Dorfman, Susannah M.; Meng, Yue; Prakapenka, Vitali B.
  • Earth and Planetary Science Letters, Vol. 361
  • DOI: 10.1016/j.epsl.2012.10.033

Laser heated diamond cell system at the Advanced Photon Source for in situ x-ray measurements at high pressure and temperature
journal, January 2001

  • Shen, Guoyin; Rivers, Mark L.; Wang, Yanbin
  • Review of Scientific Instruments, Vol. 72, Issue 2
  • DOI: 10.1063/1.1343867

Double-sided laser heating system at HPCAT for in situ x-ray diffraction at high pressures and high temperatures
journal, June 2006


Portable laser-heating stand for synchrotron applications
journal, April 2009

  • Boehler, R.; Musshoff, H. G.; Ditz, R.
  • Review of Scientific Instruments, Vol. 80, Issue 4
  • DOI: 10.1063/1.3115183

    Works referencing / citing this record:

    Postaragonite phases of CaCO 3 at lower mantle pressures
    journal, January 2018


    Thermal equation of state of Molybdenum determined from in situ synchrotron X-ray diffraction with laser-heated diamond anvil cells
    journal, February 2016

    • Huang, Xiaoli; Li, Fangfei; Zhou, Qiang
    • Scientific Reports, Vol. 6, Issue 1
    • DOI: 10.1038/srep19923