Wide-angle diamond cell for neutron scattering

Haberl, Bianca; Dissanayake, Sachith E.; Ye, Feng; Daemen, Luke L.; Cheng, Yongqiang; Li, Chen W.; Ramirez-Cuesta, Anibal -J.  (Timmy); Matsuda, Masaaki; Molaison, Jamie J.; Boehler, Reinhard

doi:10.1080/08957959.2017.1390571

Title: Wide-angle diamond cell for neutron scattering

Journal Article · 19 October 2017 · High Pressure Research

DOI: https://doi.org/10.1080/08957959.2017.1390571 · OSTI ID:1465058

^[1];

^[1]; Daemen, Luke L. ^[1];

^[1]; Li, Chen W. ^[2];

^[1];

^[1]; Boehler, Reinhard ^[3]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of California-Riverside, Riverside, CA (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Carnegie Inst. for Sciences, Washington, D.C. (United States)

Here, a new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the Oak Ridge National Laboratory. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax^®) pressure anvils are used. We predict a routine pressure regime up to 20 GPa with sample volumes of ~0.5 mm3. Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.

View Accepted Manuscript (DOE)

Cite

Export

Save

Research Organization:: Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States); Energy Frontier Research Centers (EFRC) (United States). Energy Frontier Research in Extreme Environments (EFree)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

Grant/Contract Number:: AC05-00OR22725

OSTI ID:: 1465058

Journal Information:: High Pressure Research, Vol. 37, Issue 4; ISSN 0895-7959

Publisher:: Taylor & FrancisCopyright Statement

Country of Publication:: United States

Language:: English

Citation Metrics:

Cited by: 17 works

Citation information provided by
Web of Science

References (16)

Neutron and X-ray diffraction study of the broken symmetry phase transition in solid deuterium Goncharenko, Igor; Loubeyre, Paul Nature, Vol. 435, Issue 7046 https://doi.org/10.1038/nature03699	journal	June 2005
Novel diamond cells for neutron diffraction using multi-carat CVD anvils Boehler, R.; Molaison, J. J.; Haberl, B. Review of Scientific Instruments, Vol. 88, Issue 8 https://doi.org/10.1063/1.4997265	journal	August 2017
Pressure dependence of the magnetic ground states in MnP Matsuda, M.; Ye, F.; Dissanayake, S. E. Physical Review B, Vol. 93, Issue 10 https://doi.org/10.1103/PhysRevB.93.100405	journal	March 2016
Emergence of long-range order in sheets of magnetic dimers Haravifard, S.; Banerjee, A.; van Wezel, J. Proceedings of the National Academy of Sciences, Vol. 111, Issue 40 https://doi.org/10.1073/pnas.1413318111	journal	September 2014
Neutron diffraction experiments in diamond and sapphire anvil cells Goncharenko, I. N. High Pressure Research, Vol. 24, Issue 1 https://doi.org/10.1080/08957950410001661882	journal	January 2004
Integrated-fin gasket for palm cubic-anvil high pressure apparatus Cheng, J. -G.; Matsubayashi, K.; Nagasaki, S. Review of Scientific Instruments, Vol. 85, Issue 9 https://doi.org/10.1063/1.4896473	journal	September 2014
High pressure neutron diffraction using the paris-edinburgh cell: Experimental possibilities and future prospects Klotz, S.; Besson, J. M.; Hamel, G. High Pressure Research, Vol. 14, Issue 4-6 https://doi.org/10.1080/08957959608201409	journal	January 1996
Experimental study of the vibrational spectrum and structure variations in NH ₄ Cl under high pressure Balagurov, A. M.; Savenko, B. N.; Borman, A. V. High Pressure Research, Vol. 14, Issue 1-3 https://doi.org/10.1080/08957959508200902	journal	October 1995
Single crystal neutron experiments under pressures up to 38 GPa Goncharenko, I.; Gukasov, A.; Loubeyre, P. Acta Crystallographica Section A Foundations of Crystallography, Vol. 61, Issue a1 https://doi.org/10.1107/S0108767305094341	journal	August 2005
Phonon dispersion in graphite under hydrostatic pressure up to 60 kbar using a sapphire-anvil technique Ivanov, A. S.; Goncharenko, I. N.; Somenkov, V. A. Physica B: Condensed Matter, Vol. 213-214 https://doi.org/10.1016/0921-4526(95)00356-E	journal	August 1995
Benzene-derived carbon nanothreads Fitzgibbons, Thomas C.; Guthrie, Malcolm; Xu, En-shi Nature Materials, Vol. 14, Issue 1 https://doi.org/10.1038/nmat4088	journal	September 2014
Transverse Acoustic Phonons of Germanium up to 9.7 GPa by Neutron Inelastic Scattering Klotz, S.; Besson, J. M.; Braden, M. physica status solidi (b), Vol. 198, Issue 1 https://doi.org/10.1002/pssb.2221980115	journal	November 1996
Pressure-induced crystallization of a spin liquid Mirebeau, I.; Goncharenko, I. N.; Cadavez-Peres, P. Nature, Vol. 420, Issue 6911 https://doi.org/10.1038/nature01157	journal	November 2002
Toroidal anvils for single-crystal neutron studies Bull, Craig L.; Guthrie, Malcolm; Klotz, Stefan High Pressure Research, Vol. 25, Issue 4 https://doi.org/10.1080/08957950500452893	journal	December 2005
Techniques in High Pressure Neutron Scattering Klotz, Stefan CRC Press https://doi.org/10.1201/b13074	book	January 2012
Equation of state of sodium chloride up to 32 kbar and 500°C† Boehler, Reinhard; Kennedy, George C. Journal of Physics and Chemistry of Solids, Vol. 41, Issue 5 https://doi.org/10.1016/0022-3697(80)90183-3	journal	January 1980

Cited By (6)

A suite-level review of the neutron single-crystal diffraction instruments at Oak Ridge National Laboratory Coates, L.; Cao, H. B.; Chakoumakos, B. C. Review of Scientific Instruments, Vol. 89, Issue 9 https://doi.org/10.1063/1.5030896	journal	September 2018
Next-generation diamond cell and applications to single-crystal neutron diffraction Haberl, Bianca; Dissanayake, Sachith; Wu, Yan Review of Scientific Instruments, Vol. 89, Issue 9 https://doi.org/10.1063/1.5031454	journal	September 2018
A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory Calder, S.; An, K.; Boehler, R. Review of Scientific Instruments, Vol. 89, Issue 9 https://doi.org/10.1063/1.5033906	journal	September 2018
On intensities in high pressure neutron powder diffraction using single and polycrystalline diamond anvils: small versus large sample volumes Klotz, Stefan; Bull, Craig L.; Ridley, Christopher J. High Pressure Research, Vol. 39, Issue 1 https://doi.org/10.1080/08957959.2019.1579806	journal	January 2019
A nano-polycrystalline diamond anvil cell with bulk metallic glass cylinder for single-crystal neutron diffraction Yamashita, Keishiro; Komatsu, Kazuki; Klotz, Stefan High Pressure Research, Vol. 40, Issue 1 https://doi.org/10.1080/08957959.2019.1700980	journal	December 2019
Development of cubic anvil type high pressure apparatus for neutron diffraction Dissanayake, S. E.; Matsuda, M.; Munakata, K. Journal of Physics: Condensed Matter, Vol. 31, Issue 38 https://doi.org/10.1088/1361-648x/ab2688	journal	July 2019

Similar Records

Next-generation diamond cell and applications to single-crystal neutron diffraction

Journal Article · 2018 · Review of Scientific Instruments · OSTI ID:1474626

Haberl, Bianca; Dissanayake, Sachith E.; Wu, Yan; +14 more

Development of Large-Volume-Diamond Anvil Cell for Neutron Diffraction: The Neutron Diamond Anvil Cell Project at ORNL

Book · 2023 · OSTI ID:1960713

Boehler, Reinhard; Haberl, Bianca; Molaison, Jamie; +1 more

Large-volume diamond cells for neutron diffraction above 90GPa

Journal Article · 2013 · High Pressure Research · OSTI ID:1116499

Boehler, Reinhard; Guthrie, Malcolm; Molaison, Jamie J; +5 more

Related Subjects

42 ENGINEERING
high pressure neutron scattering
diamond anvil cell
inelastic neutron scattering

Title: Wide-angle diamond cell for neutron scattering

Citation Formats

References (16)

Cited By (6)

Similar Records

Related Subjects