Wide-angle diamond cell for neutron scattering

Haberl, Bianca; Dissanayake, Sachith E.; Ye, Feng; Daemen, Luke L.; Cheng, Yongqiang; Li, Chen W.; Ramirez-Cuesta, Anibal -J.  (Timmy); Matsuda, Masaaki; Molaison, Jamie J.; Boehler, Reinhard

doi:10.1080/08957959.2017.1390571

Title: Wide-angle diamond cell for neutron scattering

Abstract

Here, a new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the Oak Ridge National Laboratory. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax^®) pressure anvils are used. We predict a routine pressure regime up to 20 GPa with sample volumes of ~0.5 mm3. Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.

Authors:

^[1];

^[1]; Daemen, Luke L. ^[1];

^[1]; Li, Chen W. ^[2];

^[3];

^[1];

^[1]; Boehler, Reinhard ^[4]

Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of California-Riverside, Riverside, CA (United States)
(Timmy) [Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Carnegie Inst. for Sciences, Washington, D.C. (United States)

Publication Date:: Thu Oct 19 00:00:00 EDT 2017

Research Org.:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Energy Frontier Research Centers (EFRC) (United States). Energy Frontier Research in Extreme Environments (EFree)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES)

OSTI Identifier:: 1465058

Grant/Contract Number:: AC05-00OR22725

Resource Type:: Accepted Manuscript

Journal Name:: High Pressure Research

Additional Journal Information:: Journal Volume: 37; Journal Issue: 4; Journal ID: ISSN 0895-7959

Publisher:: Taylor & Francis

Country of Publication:: United States

Language:: English

Subject:: 42 ENGINEERING; high pressure neutron scattering; diamond anvil cell; inelastic neutron scattering

Citation Formats


                    Haberl, Bianca, Dissanayake, Sachith E., Ye, Feng, Daemen, Luke L., Cheng, Yongqiang, Li, Chen W., Ramirez-Cuesta, Anibal -J., Matsuda, Masaaki, Molaison, Jamie J., and Boehler, Reinhard. Wide-angle diamond cell for neutron scattering.  United States: N. p., 2017. 
Web.  doi:10.1080/08957959.2017.1390571.

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                    Haberl, Bianca, Dissanayake, Sachith E., Ye, Feng, Daemen, Luke L., Cheng, Yongqiang, Li, Chen W., Ramirez-Cuesta, Anibal -J., Matsuda, Masaaki, Molaison, Jamie J., & Boehler, Reinhard. Wide-angle diamond cell for neutron scattering.  United States.  https://doi.org/10.1080/08957959.2017.1390571

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                    Haberl, Bianca, Dissanayake, Sachith E., Ye, Feng, Daemen, Luke L., Cheng, Yongqiang, Li, Chen W., Ramirez-Cuesta, Anibal -J., Matsuda, Masaaki, Molaison, Jamie J., and Boehler, Reinhard. Thu .  
"Wide-angle diamond cell for neutron scattering".  United States.  https://doi.org/10.1080/08957959.2017.1390571.  https://www.osti.gov/servlets/purl/1465058.

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@article{osti_1465058,

  title        = {Wide-angle diamond cell for neutron scattering},

  author       = {Haberl, Bianca and Dissanayake, Sachith E. and Ye, Feng and Daemen, Luke L. and Cheng, Yongqiang and Li, Chen W. and Ramirez-Cuesta, Anibal -J. and Matsuda, Masaaki and Molaison, Jamie J. and Boehler, Reinhard},

  abstractNote = {Here, a new diamond cell with extreme apertures is described. It is tailored for a large variety of neutron scattering techniques such as inelastic neutron scattering and single-crystal diffraction both at the Spallation Neutron Source (SNS) and the High Flux Isotope Reactor at the Oak Ridge National Laboratory. Simple springs enable forces of over 10 metric tons to be clamped in for low-temperature measurements. At present, low-cost polycrystalline diamond (Versimax®) pressure anvils are used. We predict a routine pressure regime up to 20 GPa with sample volumes of ~0.5 mm3. Future use of large CVD single-crystal diamond anvils will significantly expand this pressure range. We show examples for measurements at the SNAP, VISION and CORELLI beamlines of the SNS.},

  doi          = {10.1080/08957959.2017.1390571},

  journal      = {High Pressure Research},

  number       = 4,

  volume       = 37,

  place        = {United States},

  year         = {Thu Oct 19 00:00:00 EDT 2017},

  month        = {Thu Oct 19 00:00:00 EDT 2017}

}

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Works referenced in this record:

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journal, June 2005

Goncharenko, Igor; Loubeyre, Paul
Nature, Vol. 435, Issue 7046
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Novel diamond cells for neutron diffraction using multi-carat CVD anvils
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Boehler, R.; Molaison, J. J.; Haberl, B.
Review of Scientific Instruments, Vol. 88, Issue 8
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Pressure dependence of the magnetic ground states in MnP
journal, March 2016

Matsuda, M.; Ye, F.; Dissanayake, S. E.
Physical Review B, Vol. 93, Issue 10
DOI: 10.1103/PhysRevB.93.100405

Emergence of long-range order in sheets of magnetic dimers
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Haravifard, S.; Banerjee, A.; van Wezel, J.
Proceedings of the National Academy of Sciences, Vol. 111, Issue 40
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Neutron diffraction experiments in diamond and sapphire anvil cells
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Goncharenko, I. N.
High Pressure Research, Vol. 24, Issue 1
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Integrated-fin gasket for palm cubic-anvil high pressure apparatus
journal, September 2014

Cheng, J. -G.; Matsubayashi, K.; Nagasaki, S.
Review of Scientific Instruments, Vol. 85, Issue 9
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High pressure neutron diffraction using the paris-edinburgh cell: Experimental possibilities and future prospects
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Klotz, S.; Besson, J. M.; Hamel, G.
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Single crystal neutron experiments under pressures up to 38 GPa
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Goncharenko, I.; Gukasov, A.; Loubeyre, P.
Acta Crystallographica Section A Foundations of Crystallography, Vol. 61, Issue a1
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Phonon dispersion in graphite under hydrostatic pressure up to 60 kbar using a sapphire-anvil technique
journal, August 1995

Ivanov, A. S.; Goncharenko, I. N.; Somenkov, V. A.
Physica B: Condensed Matter, Vol. 213-214
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Benzene-derived carbon nanothreads
journal, September 2014

Fitzgibbons, Thomas C.; Guthrie, Malcolm; Xu, En-shi
Nature Materials, Vol. 14, Issue 1
DOI: 10.1038/nmat4088

Transverse Acoustic Phonons of Germanium up to 9.7 GPa by Neutron Inelastic Scattering
journal, November 1996

Klotz, S.; Besson, J. M.; Braden, M.
physica status solidi (b), Vol. 198, Issue 1
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Pressure-induced crystallization of a spin liquid
journal, November 2002

Mirebeau, I.; Goncharenko, I. N.; Cadavez-Peres, P.
Nature, Vol. 420, Issue 6911
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Toroidal anvils for single-crystal neutron studies
journal, December 2005

Bull, Craig L.; Guthrie, Malcolm; Klotz, Stefan
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Equation of state of sodium chloride up to 32 kbar and 500°C†
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Boehler, Reinhard; Kennedy, George C.
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Works referencing / citing this record:

A suite-level review of the neutron single-crystal diffraction instruments at Oak Ridge National Laboratory
journal, September 2018

Coates, L.; Cao, H. B.; Chakoumakos, B. C.
Review of Scientific Instruments, Vol. 89, Issue 9
DOI: 10.1063/1.5030896

Next-generation diamond cell and applications to single-crystal neutron diffraction
journal, September 2018

Haberl, Bianca; Dissanayake, Sachith; Wu, Yan
Review of Scientific Instruments, Vol. 89, Issue 9
DOI: 10.1063/1.5031454

A suite-level review of the neutron powder diffraction instruments at Oak Ridge National Laboratory
journal, September 2018

Calder, S.; An, K.; Boehler, R.
Review of Scientific Instruments, Vol. 89, Issue 9
DOI: 10.1063/1.5033906

On intensities in high pressure neutron powder diffraction using single and polycrystalline diamond anvils: small versus large sample volumes
journal, January 2019

Klotz, Stefan; Bull, Craig L.; Ridley, Christopher J.
High Pressure Research, Vol. 39, Issue 1
DOI: 10.1080/08957959.2019.1579806

A nano-polycrystalline diamond anvil cell with bulk metallic glass cylinder for single-crystal neutron diffraction
journal, December 2019

Yamashita, Keishiro; Komatsu, Kazuki; Klotz, Stefan
High Pressure Research, Vol. 40, Issue 1
DOI: 10.1080/08957959.2019.1700980

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Title: Wide-angle diamond cell for neutron scattering

Abstract

Citation Formats

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Novel diamond cells for neutron diffraction using multi-carat CVD anvils journal, August 2017

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High pressure neutron diffraction using the paris-edinburgh cell: Experimental possibilities and future prospects journal, January 1996

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Transverse Acoustic Phonons of Germanium up to 9.7 GPa by Neutron Inelastic Scattering journal, November 1996

Pressure-induced crystallization of a spin liquid journal, November 2002

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Equation of state of sodium chloride up to 32 kbar and 500°C† journal, January 1980

A suite-level review of the neutron single-crystal diffraction instruments at Oak Ridge National Laboratory journal, September 2018

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Neutron and X-ray diffraction study of the broken symmetry phase transition in solid deuterium
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Novel diamond cells for neutron diffraction using multi-carat CVD anvils
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Pressure dependence of the magnetic ground states in MnP
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Emergence of long-range order in sheets of magnetic dimers
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Neutron diffraction experiments in diamond and sapphire anvil cells
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Integrated-fin gasket for palm cubic-anvil high pressure apparatus
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High pressure neutron diffraction using the paris-edinburgh cell: Experimental possibilities and future prospects
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Experimental study of the vibrational spectrum and structure variations in NH ₄ Cl under high pressure
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Single crystal neutron experiments under pressures up to 38 GPa
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Benzene-derived carbon nanothreads
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Transverse Acoustic Phonons of Germanium up to 9.7 GPa by Neutron Inelastic Scattering
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Pressure-induced crystallization of a spin liquid
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Toroidal anvils for single-crystal neutron studies
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Equation of state of sodium chloride up to 32 kbar and 500°C†
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A suite-level review of the neutron single-crystal diffraction instruments at Oak Ridge National Laboratory
journal, September 2018

Next-generation diamond cell and applications to single-crystal neutron diffraction
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