Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Development of boron and phosphorus liquid metal ion sources for the focused ion beam system

Thesis/Dissertation ·
OSTI ID:6708715
The approach taken here was to develop and build dual carbon filament liquid metal ion sources along with the test bed system. Pd/sub 73/B/sub 27/ and Pt/sub 58/B/sub 42/ binary alloys were selected as p-type dopant sources, and Cu/sub 3/P binary alloy was used as n-type dopant source. Three emitters with different tip radii were used in the present investigation. The results indicate that Pd/sub 73/B/sub 27/ alloy is a good candidate for a boron liquid metal ion source. This conclusion was derived in this investigation from a lifetime test result with 2.5 ..mu..m emitter of more than 120 hours. Pt/sub 58/B/sub 42/ alloy is not a suitable alloy source for a boron liquid metal ion source despite the higher mole fraction of boron to be used as a source of ionizing species. Cu/sub 3/P alloy is a good candidate for a phosphorus liquid metal ion source. Any apparent chemical interactions were found by metallographic technique, although AES result shows emitter element in the spectrum of collected beam current. A combination of rhenium and graphite ribbon as liquid metal ion source emitter and heater used in this investigation is the only possible approach to produce a long lifetime boron and phosphorus liquid metal ion source.
Research Organization:
Rensselaer Polytechnic Inst., Troy, NY (USA)
OSTI ID:
6708715
Country of Publication:
United States
Language:
English