Determining carbazole in anthracene
Journal Article
·
· Coke Chem. USSR (Engl. Transl.); (United States)
OSTI ID:6227933
At the present time the coking industry is the main supplier of the anthracene which is used for synthesis of dyes, phosphors, plastics, etc. One of the undesirable and difficulty-removable impurities in the anthracene obtained from coking feedstocks is carbazole. Determination by the Kjel'dahl method does not permit one to find the true value of the carbazole concentration in anthracene due to the presence of other nitrogen-containing compounds in the anthracene. In the present article we describe a method of analyzing the carbazole concentration in crude and enriched anthracene by means of thin layer chromatography and subsequent spectrophotometric determination of the carbazole concentration.
- OSTI ID:
- 6227933
- Journal Information:
- Coke Chem. USSR (Engl. Transl.); (United States), Journal Name: Coke Chem. USSR (Engl. Transl.); (United States) Vol. 2; ISSN COKCA
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
01 COAL, LIGNITE, AND PEAT
010401* -- Coal & Coal Products-- Carbonization-- (-1987)
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400100 -- Analytical & Separations Chemistry
ANTHRACENE
AROMATICS
AZOLES
CARBAZOLES
CARBONIZATION
CHEMICAL ANALYSIS
CHEMICAL REACTIONS
CHROMATOGRAPHY
COKE
COKING
COKING PLANTS
CONDENSED AROMATICS
DECOMPOSITION
HETEROCYCLIC COMPOUNDS
HYDROCARBONS
INDUSTRIAL PLANTS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
SEPARATION PROCESSES
SPECTROPHOTOMETRY
THIN-LAYER CHROMATOGRAPHY
010401* -- Coal & Coal Products-- Carbonization-- (-1987)
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400100 -- Analytical & Separations Chemistry
ANTHRACENE
AROMATICS
AZOLES
CARBAZOLES
CARBONIZATION
CHEMICAL ANALYSIS
CHEMICAL REACTIONS
CHROMATOGRAPHY
COKE
COKING
COKING PLANTS
CONDENSED AROMATICS
DECOMPOSITION
HETEROCYCLIC COMPOUNDS
HYDROCARBONS
INDUSTRIAL PLANTS
ORGANIC COMPOUNDS
ORGANIC NITROGEN COMPOUNDS
SEPARATION PROCESSES
SPECTROPHOTOMETRY
THIN-LAYER CHROMATOGRAPHY