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CONTROLLED-POTENTIAL COULOMETRIC TITRATION OF URANIUM(VI) IN THE PRESENCE OF NITRATE

Technical Report ·
DOI:https://doi.org/10.2172/4817799· OSTI ID:4817799
A study into the use of sulfamic acld as a nitritedestroying reagent in the controlled-potentlal coulometrlc tltratlon method for uranlum(VI) was made. When nltrites are thus destroyed, the tltration ls much less subject to error from HNO/sub 3/. The results of titratlons of known amounts of uranlum(VI) in the presence of varlous amounts of HNO/sub 3/, Th(NO/sub 3/)/sub 4/, Al(NO/sub 3/ )/sub 4/, and LiNO/sub 3/ are given. (auth)
Research Organization:
Oak Ridge National Lab., Tenn.
DOE Contract Number:
W-7405-ENG-26
NSA Number:
NSA-16-008678
OSTI ID:
4817799
Report Number(s):
ORNL-TM-113
Country of Publication:
United States
Language:
English