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Title: Process of forming compounds using reverse micelle or reverse microemulsion systems

Patent ·
OSTI ID:871644

The present invention is directed to a process for producing a nanometer-sized metal compound. The process comprises forming a reverse micelle or reverse microemulsion system comprising a polar fluid in a non-polar or low-polarity fluid. A first reactant comprising a multi-component, water-soluble metal compound is introduced into the polar fluid in a non-polar or low-polarity fluid. This first reactant can be introduced into the reverse micelle or reverse microemulsion system during formation thereof or subsequent to the formation of the reverse micelle or microemulsion system. The water-soluble metal compound is then reacted in the reverse micelle or reverse microemulsion system to form the nanometer-sized metal compound. The nanometer-sized metal compound is then precipitated from the reverse micelle or reverse microemulsion system.

Research Organization:
Battelle Memorial Institute, Columbus, OH (United States)
DOE Contract Number:
AC06-76RL01830
Assignee:
Battelle Memorial Institute (Richland, WA)
Patent Number(s):
US 5770172
OSTI ID:
871644
Country of Publication:
United States
Language:
English

References (10)

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Nucleation and Growth of CdSe on ZnS Quantum Crystallite Seeds, and Vice Versa, in Inverse Micelle Media journal February 1990
The statistics of surface atoms and surface sites on metal crystals journal June 1969
Surface derivatization and isolation of semiconductor cluster molecules journal May 1988
Coal Dissolution Promoted by Ultrafine Iron-Based Catalysts book January 1991
Liquefaction of Subbituminous Coal in the Presence of Dispersed Iron and Molybdenum Catalysts book January 1991
Highly Active Catalysts of Coal Liquefaction book January 1991
Kinetics and mechanism of formation of quantum-sized cadmium sulphide particles in water–aerosol-OT–oil microemulsions journal January 1990