An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

Immoor, Julia; Marquardt, H.; Miyagi, L.; Speziale, S.; Merkel, S.; Schwark, I.; Ehnes, A.; Liermann, H. -P.

doi:10.1063/1.5143293

Title: An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

Journal Article · Tue Apr 28 00:00:00 EDT 2020 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/1.5143293· OSTI ID:1801157

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Univ. of Bayreuth (Germany)
Univ. of Oxford (United Kingdom)
Univ. of Utah, Salt Lake City, UT (United States)
German Research Center for Geosciences GFZ, Potsdam (Germany)
Univ. Lille (France)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)

We present an improved setup for the experimental study of deformation of solids at simultaneous high pressures and temperatures by radial x-ray diffraction. This technique employs a graphite resistive heated Mao–Bell type diamond anvil cell for radial x-ray diffraction in combination with a water-cooled vacuum chamber. The new chamber has been developed by the sample environment group at PETRA III and implemented at the Extreme Conditions Beamline P02.2 at PETRA III, DESY (Hamburg, Germany). Here, we discuss applications of the new setup to study deformation of a variety of materials, including ferropericlase, calcium perovskite, bridgmanite, and tantalum carbide, at high-pressure/temperature.

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Research Organization:: George Washington Univ., Washington, DC (United States); Univ. of Illinois, Chicago, IL (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA), Office of Defense Programs (DP); German Science Foundation; National Science Foundation (NSF); EU Framework Programme for Research and Innovation

Grant/Contract Number:: NA0003858; MA4534/3-1; MA4534/4-1; EAR-1344579; EAR-1654687; 730872; NA0003975

OSTI ID:: 1801157

Alternate ID(s):: OSTI ID: 1824202

Journal Information:: Review of Scientific Instruments, Vol. 91, Issue 4; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

References (43)

Evaluating post-perovskite as a cause of D′′ anisotropy in regions of palaeosubduction Nowacki, Andy; Walker, Andrew M.; Wookey, James Geophysical Journal International, Vol. 192, Issue 3 https://doi.org/10.1093/gji/ggs068	journal	December 2012
The role of recrystallization in the preferred orientation of olivine Karato, Shun-ichiro Physics of the Earth and Planetary Interiors, Vol. 51, Issue 1-3 https://doi.org/10.1016/0031-9201(88)90029-5	journal	June 1988
Ab initio study of the high-pressure behavior of CaSiO3 perovskite Jung, Daniel Y.; Oganov, Artem R. ETH Zurich https://doi.org/10.3929/ethz-b-000032624	text	January 2005
Deformation experiment at P–T conditions of the mantle transition zone using D-DIA apparatus Kawazoe, Takaaki; Nishiyama, Norimasa; Nishihara, Yu Physics of the Earth and Planetary Interiors, Vol. 183, Issue 1-2 https://doi.org/10.1016/j.pepi.2010.07.004	journal	November 2010
Ferropericlase Control of Lower Mantle Rheology : Impact of Phase Morphology Thielmann, Marcel; Golabek, Gregor J.; Marquardt, Hauke University of Bayreuth https://doi.org/10.15495/epub_ubt_00005078	text	January 2020
Anisotropy in the deep Earth Romanowicz, Barbara; Wenk, Hans-Rudolf Physics of the Earth and Planetary Interiors, Vol. 269 https://doi.org/10.1016/j.pepi.2017.05.005	journal	August 2017
Flow laws for rocks containing two non-linear viscous phases: A phenomenological approach Handy, Mark R. Journal of Structural Geology, Vol. 16, Issue 3 https://doi.org/10.1016/0191-8141(94)90035-3	journal	March 1994
Ab initio molecular dynamics study of $Ca Si O_{3}$ perovskite at $P − T$ conditions of Earth’s lower mantle Adams, Donat J.; Oganov, Artem R. Physical Review B, Vol. 73, Issue 18 https://doi.org/10.1103/physrevb.73.184106	journal	May 2006
Shear deformation of bridgmanite and magnesiowustite aggregates at lower mantle conditions Girard, J.; Amulele, G.; Farla, R. Science, Vol. 351, Issue 6269 https://doi.org/10.1126/science.aad3113	journal	December 2015
The deformation-DIA: A new apparatus for high temperature triaxial deformation to pressures up to 15 GPa Wang, Yanbin; Durham, William B.; Getting, Ivan C. Review of Scientific Instruments, Vol. 74, Issue 6 https://doi.org/10.1063/1.1570948	journal	June 2003
Diamond anvil cell deformation of CaSiO3 perovskite up to 49GPa Miyagi, Lowell; Merkel, Sébastien; Yagi, Takehiko Physics of the Earth and Planetary Interiors, Vol. 174, Issue 1-4 https://doi.org/10.1016/j.pepi.2008.05.018	journal	May 2009
Toward an internally consistent pressure scale Fei, Y.; Ricolleau, A.; Frank, M. Proceedings of the National Academy of Sciences, Vol. 104, Issue 22 https://doi.org/10.1073/pnas.0609013104	journal	May 2007
Ferropericlase Control of Lower Mantle Rheology: Impact of Phase Morphology Thielmann, M.; Golabek, G. J.; Marquardt, H. Geochemistry, Geophysics, Geosystems, Vol. 21, Issue 2 https://doi.org/10.1029/2019gc008688	journal	January 2020
Slab stagnation in the shallow lower mantle linked to an increase in mantle viscosity Marquardt, Hauke; Miyagi, Lowell Nature Geoscience, Vol. 8, Issue 4 https://doi.org/10.1038/ngeo2393	journal	March 2015
Phase transition in CaSiO3 perovskite Komabayashi, Tetsuya; Hirose, Kei; Sata, Nagayoshi Earth and Planetary Science Letters, Vol. 260, Issue 3-4 https://doi.org/10.1016/j.epsl.2007.06.015	journal	August 2007
Superplasticity in Earth's Lower Mantle: Evidence from Seismic Anisotropy and Rock Physics Karato, S. -i.; Zhang, S.; Wenk, H. -R. Science, Vol. 270, Issue 5235 https://doi.org/10.1126/science.270.5235.458	journal	October 1995
Non-cubic crystal symmetry of CaSiO3 perovskite up to 18 GPa and 1600 K Uchida, Takeyuki; Wang, Yanbin; Nishiyama, Norimasa Earth and Planetary Science Letters, Vol. 282, Issue 1-4 https://doi.org/10.1016/j.epsl.2009.03.027	journal	May 2009
Mantle Convection and Plate Tectonics: Toward an Integrated Physical and Chemical Theory Tackley, P. J. Science, Vol. 288, Issue 5473 https://doi.org/10.1126/science.288.5473.2002	journal	June 2000
The equation of state of TaC0.99 by X-ray diffraction in radial scattering geometry to 32 GPa and 1073 K Speziale, S.; Immoor, J.; Ermakov, A. Journal of Applied Physics, Vol. 126, Issue 10 https://doi.org/10.1063/1.5115350	journal	September 2019
Deformation of (Mg,Fe)SiO3 Post-Perovskite and D'' Anisotropy Merkel, S.; McNamara, A. K.; Kubo, A. Science, Vol. 316, Issue 5832 https://doi.org/10.1126/science.1140609	journal	June 2007
Two-phase deformation of lower mantle mineral analogs Kaercher, P.; Miyagi, L.; Kanitpanyacharoen, W. Earth and Planetary Science Letters, Vol. 456 https://doi.org/10.1016/j.epsl.2016.09.030	journal	December 2016
Deformation of polycrystalline MgO at pressures of the lower mantle: DEFORMATION OF MgO AT HIGH PRESSURE Merkel, Sébastien; Wenk, Hans Rudolf; Shu, Jinfu Journal of Geophysical Research: Solid Earth, Vol. 107, Issue B11 https://doi.org/10.1029/2001JB000920	journal	November 2002
In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K Merkel, S.; Liermann, H. -P.; Miyagi, L. Deutsches Elektronen-Synchrotron, DESY, Hamburg https://doi.org/10.3204/desy-2014-01884	text	January 2013
Combined resistive and laser heating technique for in situ radial X-ray diffraction in the diamond anvil cell at high pressure and temperature Miyagi, Lowell; Kanitpanyacharoen, Waruntorn; Raju, Selva Vennila Review of Scientific Instruments, Vol. 84, Issue 2 https://doi.org/10.1063/1.4793398	journal	February 2013
High-pressure rotational deformation apparatus to 15 GPa Yamazaki, D.; Karato, Shun-ichiro Review of Scientific Instruments, Vol. 72, Issue 11 https://doi.org/10.1063/1.1412858	journal	November 2001
Deformation of lower-mantle ferropericlase (Mg,Fe)O across the electronic spin transition Lin, Jung-Fu; Wenk, Hans-Rudolf; Voltolini, Marco Physics and Chemistry of Minerals, Vol. 36, Issue 10 https://doi.org/10.1007/s00269-009-0303-5	journal	April 2009
A cubic boron nitride gasket for diamond-anvil experiments Funamori, Nobumasa; Sato, Tomoko Review of Scientific Instruments, Vol. 79, Issue 5 https://doi.org/10.1063/1.2917409	journal	May 2008
Mantle dynamics inferred from the crystallographic preferred orientation of bridgmanite Tsujino, Noriyoshi; Nishihara, Yu; Yamazaki, Daisuke Nature, Vol. 539, Issue 7627 https://doi.org/10.1038/nature19777	journal	October 2016
X-ray transparent gasket for diamond anvil cell high pressure experiments Merkel, Sébastien; Yagi, Takehiko Review of Scientific Instruments, Vol. 76, Issue 4 https://doi.org/10.1063/1.1884195	journal	April 2005
Elastic Shear Anisotropy of Ferropericlase in Earth's Lower Mantle Marquardt, H.; Speziale, S.; Reichmann, H. J. Science, Vol. 324, Issue 5924 https://doi.org/10.1126/science.1169365	journal	April 2009
Experimental method for in situ determination of material textures at simultaneous high pressure and high temperature by means of radial diffraction in the diamond anvil cell Liermann, Hanns-Peter; Merkel, Sébastien; Miyagi, Lowell Review of Scientific Instruments, Vol. 80, Issue 10 https://doi.org/10.1063/1.3236365	journal	October 2009
Rheology of the Upper Mantle: A Synthesis Karato, S. -i.; Wu, P. Science, Vol. 260, Issue 5109 https://doi.org/10.1126/science.260.5109.771	journal	May 1993
A convection model to explain anisotropy of the inner core Wenk, H. -R.; Baumgardner, J. R.; Lebensohn, R. A. Journal of Geophysical Research: Solid Earth, Vol. 105, Issue B3 https://doi.org/10.1029/1999jb900346	journal	March 2000
Texture development and elastic stresses in magnesiowűstite at high pressure Tommaseo, Caterina E.; Devine, Jim; Merkel, Sébastien Physics and Chemistry of Minerals, Vol. 33, Issue 2 https://doi.org/10.1007/s00269-005-0054-x	journal	January 2006
Rheology of the lower mantle Karato, S. Physics of the Earth and Planetary Interiors, Vol. 24, Issue 1 https://doi.org/10.1016/0031-9201(81)90074-1	journal	January 1981
Some mineral physics constraints on the rheology and geothermal structure of Earth’s lower mantle Yamazaki, Daisuke; Karato, Shun-ichiro American Mineralogist, Vol. 86, Issue 4 https://doi.org/10.2138/am-2001-0401	journal	April 2001
Seismic anisotropy in the mantle transition zone induced by shear deformation of wadsleyite Kawazoe, Takaaki; Ohuchi, Tomohiro; Nishihara, Yu Physics of the Earth and Planetary Interiors, Vol. 216 https://doi.org/10.1016/j.pepi.2012.12.005	journal	March 2013
In situ radial X-ray diffraction study of texture and stress during phase transformations in bcc-, fcc- and hcp-iron up to 36GPa and 1000K Merkel, S.; Liermann, H. -P.; Miyagi, L. Acta Materialia, Vol. 61, Issue 14 https://doi.org/10.1016/j.actamat.2013.04.068	journal	August 2013
Ab initio study of the high-pressure behavior of CaSiO3 perovskite Jung, Daniel Y.; Oganov, Artem R. Physics and Chemistry of Minerals, Vol. 32, Issue 2 https://doi.org/10.1007/s00269-005-0453-z	journal	May 2005
Evidence for {100}<011> slip in ferropericlase in Earth's lower mantle from high-pressure/high-temperature experiments Immoor, J.; Marquardt, H.; Miyagi, L. Earth and Planetary Science Letters, Vol. 489 https://doi.org/10.1016/j.epsl.2018.02.045	journal	May 2018
In situ laser heating and radial synchrotron x-ray diffraction in a diamond anvil cell Kunz, Martin; Caldwell, Wendel A.; Miyagi, Lowell Review of Scientific Instruments, Vol. 78, Issue 6 https://doi.org/10.1063/1.2749443	journal	June 2007
Note: Modified anvil design for improved reliability in DT-Cup experiments Hunt, Simon A.; Dobson, David P. Review of Scientific Instruments, Vol. 88, Issue 12 https://doi.org/10.1063/1.5005885	journal	December 2017
High-pressure, high-temperature deformation of CaGeO ₃ (perovskite)±MgO aggregates: Implications for multiphase rheology of the lower mantle : DEFORMATION OF TWO-PHASE AGGREGATES Wang, Yanbin; Hilairet, Nadege; Nishiyama, Norimasa Geochemistry, Geophysics, Geosystems, Vol. 14, Issue 9 https://doi.org/10.1002/ggge.20200	journal	September 2013

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Title: An improved setup for radial diffraction experiments at high pressures and high temperatures in a resistive graphite-heated diamond anvil cell

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