Graphite resistive heated diamond anvil cell for simultaneous high-pressure and high-temperature diffraction experiments

Hwang, Huijeong; Bang, Yoonah; Choi, Jinhyuk; Cynn, Hyunchae; Jenei, Zsolt; Evans, William J.; Ehnes, Anita; Schwark, Iris; Glazyrin, Konstantin; Gatta, Giacomo Diego; Lotti, Paolo; Sanloup, Chrystèle; Lee, Yongjae; Liermann, Hanns-Peter

doi:10.1063/5.0132981

Title: Graphite resistive heated diamond anvil cell for simultaneous high-pressure and high-temperature diffraction experiments

Journal Article · Fri Aug 04 00:00:00 EDT 2023 · Review of Scientific Instruments

DOI:https://doi.org/10.1063/5.0132981· OSTI ID:2205713

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Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany); Gwangju Inst. of Science and Technology (Korea, Republic of)
Yonsei Univ., Seoul (Korea, Republic of)
Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)
Deutsches Elektronen-Synchrotron (DESY), Hamburg (Germany)
Univ. degli Studi di Milano (Italy)
Sorbonne Univ., Paris (France); Centre National de la Recherche Scientifique-Mixed Organizations (CNRS-UMR), Paris (France)

High-pressure and high-temperature experiments using a resistively heated diamond anvil cell have the advantage of heating samples homogeneously with precise temperature control. Here, we present the design and performance of a graphite resistive heated diamond anvil cell (GRHDAC) setup for powder and single-crystal x-ray diffraction experiments developed at the Extreme Conditions Beamline (P02.2) at PETRA III, Hamburg, Germany. In the GRHDAC, temperatures up to 2000 K can be generated at high pressures by placing it in a water-cooled vacuum chamber. Temperature estimates from thermocouple measurements are within +/–35 K at the sample position up to 800 K and within +90 K between 800 and 1400 K when using a standard seat combination of cBN and WC. Isothermal compression at high temperatures can be achieved by employing a remote membrane control system. Importantly, the advantage of the GRHDAC is demonstrated through the study of geophysical processes in the Earth’s crust and upper mantle region.

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Research Organization:: Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Organization:: USDOE National Nuclear Security Administration (NNSA)

Grant/Contract Number:: AC52-07NA27344

OSTI ID:: 2205713

Report Number(s):: LLNL-JRNL-855232; 1083570

Journal Information:: Review of Scientific Instruments, Vol. 94, Issue 8; ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: English

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