High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization

Stemshorn, Andrew K.; Vohra, Yogesh K.; Smith, Spencer J.

doi:10.1063/1.5024941

Title: High pressure high temperature devitrification of Fe₇₈B₁₃Si₉ metallic glass with simultaneous x-ray structural characterization

Journal Article · Thu May 31 00:00:00 EDT 2018 · Journal of Applied Physics

DOI:https://doi.org/10.1063/1.5024941· OSTI ID:1440609

^[1]; Vohra, Yogesh K. ^[1]; Smith, Spencer J. ^[1]

Univ. of Alabama, Birmingham, AL (United States)

Changes in bulk crystallization behavior following devitrification at high pressure are investigated for a Fe₇₈B₁₃Si₉ composition metallic glass using in-situ energy dispersive x-ray powder diffraction. Crystallization with time was evaluated for a series of measurements to a maximum pressure of 5.63 ± 0.15 GPa for the Fe₇₈B₁₃Si₉ glass. Pressure was found to strongly affect onset bulk crystallization temperature T_x. Here, crystallization at each pressure was found to progress in two stages. In the first stage, α-Fe precipitates and in the second Fe₂B forms while α-Fe continues to crystallize. Complementary high pressure room temperature studies were conducted.

View Accepted Manuscript (DOE)

View Accepted Manuscript (Publisher)

Cite

Export

Save

Research Organization:: Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS)

Sponsoring Organization:: National Science Foundation (NSF); USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES). Scientific User Facilities Division

Grant/Contract Number:: DMR-1608682; NA0001974; AC02-06CH11357

OSTI ID:: 1440609

Alternate ID(s):: OSTI ID: 1439763

Journal Information:: Journal of Applied Physics, Vol. 123, Issue 21; ISSN 0021-8979

Publisher:: American Institute of Physics (AIP)Copyright Statement

Country of Publication:: United States

Language:: ENGLISH

References (49)

Crystallization of Zr41Ti14Cu12.5Ni10Be22.5 bulk metallic glass under high pressure examined by in situ synchrotron radiation x-ray diffraction Yang, C.; Wang, W. K.; Liu, R. P. Journal of Applied Physics, Vol. 99, Issue 2 https://doi.org/10.1063/1.2164541	journal	January 2006
The influence of efficient atomic packing on the constitution of metallic glasses Miracle, D. B.; Sanders, W. S.; Senkov, O. N. Philosophical Magazine, Vol. 83, Issue 20 https://doi.org/10.1080/1478643031000098828	journal	July 2003
Influence of microstructural inhomogeneity of individual sides of Fe81Si4B13C2 amorphous alloy ribbon on thermally induced structural transformations Minić, Dragica M.; Blagojević, Vladimir A.; Minić, Dušan M. Materials Chemistry and Physics, Vol. 130, Issue 3 https://doi.org/10.1016/j.matchemphys.2011.08.018	journal	November 2011
Rietveld refinements on laboratory energy dispersive X-ray diffraction (EDXD) data Ballirano, Paolo; Caminiti, Ruggero Journal of Applied Crystallography, Vol. 34, Issue 6 https://doi.org/10.1107/S0021889801014728	journal	November 2001
High-pressure x-ray diffraction studies on the structure of liquid silicate using a Paris–Edinburgh type large volume press Yamada, Akihiro; Wang, Yanbin; Inoue, Toru Review of Scientific Instruments, Vol. 82, Issue 1 https://doi.org/10.1063/1.3514087	journal	January 2011
Toughness of Bulk Metallic Glasses Madge, Shantanu Metals, Vol. 5, Issue 3 https://doi.org/10.3390/met5031279	journal	July 2015
Crystallization Process of Fe<SUB>80</SUB>P<SUB>20−<I>x</I></SUB>Si<I><SUB>x</SUB></I> Amorphous Alloys Ohnuma, Masato; Sasaki, Osamu; Kuwano, Hisashi Materials Transactions, JIM, Vol. 34, Issue 10 https://doi.org/10.2320/matertrans1989.34.874	journal	January 1993
Intercomparison of the gold, platinum, and MgO pressure scales up to 140 GPa and 2500 K: EQUATIONS OF STATE OF AU, PT, AND MGO Ye, Y.; Prakapenka, V.; Meng, Y. Journal of Geophysical Research: Solid Earth, Vol. 122, Issue 5 https://doi.org/10.1002/2016JB013811	journal	May 2017
Metallic glasses as structural materials Ashby, M.; Greer, A. Scripta Materialia, Vol. 54, Issue 3 https://doi.org/10.1016/j.scriptamat.2005.09.051	journal	February 2006
Amorphous and nanocrystalline materials for applications as soft magnets McHenry, Michael E.; Willard, Matthew A.; Laughlin, David E. Progress in Materials Science, Vol. 44, Issue 4 https://doi.org/10.1016/S0079-6425(99)00002-X	journal	October 1999
The influence of pressure on the phase stability of nanocomposite Fe ₈₉ Zr ₇ B ₄ during heating from energy dispersive x-ray diffraction Leary, A. M.; Lucas, M. S.; Ohodnicki, P. R. Journal of Applied Physics, Vol. 113, Issue 17 https://doi.org/10.1063/1.4795326	journal	May 2013
Pressure effects on Al89La6Ni5 amorphous alloy crystallization Zhuang, Y. X.; Jiang, J. Z.; Zhou, T. J. Applied Physics Letters, Vol. 77, Issue 25 https://doi.org/10.1063/1.1332409	journal	December 2000
Bulk Metallic Glasses and Their Composites: A Brief History of Diverging Fields Hofmann, Douglas C. Journal of Materials, Vol. 2013 https://doi.org/10.1155/2013/517904	journal	January 2013
High pressure die casting of Fe-based metallic glass Ramasamy, Parthiban; Szabo, Attila; Borzel, Stefan Scientific Reports, Vol. 6, Issue 1 https://doi.org/10.1038/srep35258	journal	October 2016
HPCAT: an integrated high-pressure synchrotron facility at the Advanced Photon Source Shen, Guoyin; Chow, Paul; Xiao, Yuming High Pressure Research, Vol. 28, Issue 3 https://doi.org/10.1080/08957950802208571	journal	September 2008
Iron bcc-hcp transition: Local structure from x-ray-absorption fine structure Wang, F. M.; Ingalls, R. Physical Review B, Vol. 57, Issue 10 https://doi.org/10.1103/PhysRevB.57.5647	journal	March 1998
Mechanical properties of bulk metallic glasses and composites Eckert, J.; Das, J.; Pauly, S. Journal of Materials Research, Vol. 22, Issue 2 https://doi.org/10.1557/jmr.2007.0050	journal	September 2006
Micro/nano ductile-phases reinforced Fe-based bulk metallic glass matrix composite with large plasticity Guo, Shengfeng; Su, Chen Materials Science and Engineering: A, Vol. 707 https://doi.org/10.1016/j.msea.2017.09.036	journal	November 2017
Matching Glass-Forming Ability with the Density of the Amorphous Phase Li, Y.; Guo, Q.; Kalb, J. A. Science, Vol. 322, Issue 5909 https://doi.org/10.1126/science.1163062	journal	December 2008
Kinetics and crystallization path of a Fe-based metallic glass alloy Duarte, M. J.; Kostka, A.; Crespo, D. Acta Materialia, Vol. 127 https://doi.org/10.1016/j.actamat.2017.01.031	journal	April 2017
Pressure effect on crystallization kinetics in Zr46.8Ti8.2Cu7.5Ni10Be27.5 bulk glass Jiang, J. Z.; Gerward, L.; Xu, Y. S. Applied Physics Letters, Vol. 81, Issue 23 https://doi.org/10.1063/1.1527227	journal	December 2002
Metallic glass matrix composites Qiao, Junwei; Jia, Haoling; Liaw, Peter K. Materials Science and Engineering: R: Reports, Vol. 100 https://doi.org/10.1016/j.mser.2015.12.001	journal	February 2016
Solid state dendrite formation in an amorphous magnetic Fe77.5Si13.5B9 alloy observed by in situ hot stage transmission electron microscopy Ramanujan, R. V.; Zhang, Y. R. Applied Physics Letters, Vol. 88, Issue 18 https://doi.org/10.1063/1.2201049	journal	May 2006
Toward comprehensive studies of liquids at high pressures and high temperatures: Combined structure, elastic wave velocity, and viscosity measurements in the Paris–Edinburgh cell Kono, Yoshio; Park, Changyong; Kenney-Benson, Curtis Physics of the Earth and Planetary Interiors, Vol. 228 https://doi.org/10.1016/j.pepi.2013.09.006	journal	March 2014
Distortion of alpha-uranium structure in praseodymium metal to 311 GPA Velisavljevic, Nenad; Vohra, Yogesh K. High Pressure Research, Vol. 24, Issue 2 https://doi.org/10.1080/08957950410001717150	journal	June 2004
Physics of ferromagnetic amorphous alloys O’Handley, R. C. Journal of Applied Physics, Vol. 62, Issue 10 https://doi.org/10.1063/1.339065	journal	November 1987
Cooling-rate dependence of the density of ${Pd}_{40} {Ni}_{10} {Cu}_{30} P_{20}$ bulk metallic glass Hu, X.; Ng, S. C.; Feng, Y. P. Physical Review B, Vol. 64, Issue 17 https://doi.org/10.1103/PhysRevB.64.172201	journal	October 2001
Evidence for effect of hydrostatic pressure during casting on glass-forming ability in Zr65Al7.5Ni10Cu17.5−xPdx (x=0–17.5) alloys Setyawan, A. D.; Kato, H.; Saida, J. Materials Science and Engineering: A, Vol. 449-451 https://doi.org/10.1016/j.msea.2006.02.386	journal	March 2007
Characteristic free volumes of bulk metallic glasses: Measurement and their correlation with glass-forming ability Hu, Qiang; Zeng, Xie-Rong; Fu, M. W. Journal of Applied Physics, Vol. 109, Issue 5 https://doi.org/10.1063/1.3549819	journal	March 2011
Finite strain isotherm and velocities for single-crystal and polycrystalline NaCl at high pressures and 300°K Birch, Francis Journal of Geophysical Research, Vol. 83, Issue B3, p. 1257-1268 https://doi.org/10.1029/JB083iB03p01257	journal	January 1978
Bulk Glass-Forming Metallic Alloys: Science and Technology Johnson, William L. MRS Bulletin, Vol. 24, Issue 10 https://doi.org/10.1557/S0883769400053252	journal	October 1999
Volume Effects in Bulk Metallic Glass Formation Yavari, A. R.; Inoue, A. MRS Proceedings, Vol. 554 https://doi.org/10.1557/PROC-554-21	journal	January 1998
POWDER CELL – a program for the representation and manipulation of crystal structures and calculation of the resulting X-ray powder patterns Kraus, W.; Nolze, G. Journal of Applied Crystallography, Vol. 29, Issue 3, p. 301-303 https://doi.org/10.1107/S0021889895014920	journal	June 1996
High-pressure suppression of crystallization in the metallic supercooled liquid ${Zr}_{41} {Ti}_{14} {Cu}_{12.5} {Ni}_{10} {Be}_{22.5}$ : Influence of viscosity Wang, W. H.; Wang, Z. X.; Zhao, D. Q. Physical Review B, Vol. 70, Issue 9 https://doi.org/10.1103/PhysRevB.70.092203	journal	September 2004
Determination of forming ability of high pressure die casting for Zr-based metallic glass Liu, L. H.; Ma, J.; Yu, C. Y. Journal of Materials Processing Technology, Vol. 244 https://doi.org/10.1016/j.jmatprotec.2017.01.015	journal	June 2017
P⿢V⿢T relation of MgO derived by simultaneous elastic wave velocity and in situ X-ray measurements: A new pressure scale for the mantle transition region Kono, Yoshio; Irifune, Tetsuo; Higo, Yuji Physics of the Earth and Planetary Interiors, Vol. 183, Issue 1-2 https://doi.org/10.1016/j.pepi.2010.03.010	journal	November 2010
Crystallization of the metallic glass Fe78B13Si9 Bang, J. Y.; Lee, R. Y. Journal of Materials Science, Vol. 26, Issue 18 https://doi.org/10.1007/BF00549877	journal	January 1991
Nanostructured transformation mechanism of amorphous Fe-B-Si alloys by the crystallization method Tong, H. Y.; Ding, B. Z.; Jiang, H. G. Journal of Physics D: Applied Physics, Vol. 27, Issue 2 https://doi.org/10.1088/0022-3727/27/2/033	journal	February 1994
New Challenges for the Pressure Evolution of the Glass Temperature Rzoska, Sylwester J. Frontiers in Materials, Vol. 4 https://doi.org/10.3389/fmats.2017.00033	journal	November 2017
Effect of high pressure on the crystallization of an amorphous Fe83 B17 alloy Wang, Wen -Kui; Iwasaki, Hiroshi; Fukamichi, Kazuaki Journal of Materials Science, Vol. 15, Issue 11 https://doi.org/10.1007/BF00550536	journal	November 1980
A comparative study on the isochronal and isothermal crystallization kinetics of Co46.45Fe25.55Ta8B20 soft magnetic metallic glass with high thermal stability Taghvaei, Amir Hossein; Eckert, Jürgen Journal of Alloys and Compounds, Vol. 675 https://doi.org/10.1016/j.jallcom.2016.03.053	journal	August 2016
CMPR – a powder diffraction toolkit Toby, Brian H. Journal of Applied Crystallography, Vol. 38, Issue 6 https://doi.org/10.1107/S0021889805030232	journal	November 2005
Two-dimensional detector software: From real detector to idealised image or two-theta scan Hammersley, A. P.; Svensson, S. O.; Hanfland, M. High Pressure Research, Vol. 14, Issue 4-6, p. 235-248 https://doi.org/10.1080/08957959608201408	journal	January 1996
Bulk metallic glasses Löffler, Jörg F. Intermetallics, Vol. 11, Issue 6 https://doi.org/10.1016/S0966-9795(03)00046-3	journal	June 2003
P–V–T equations of state of MgO and thermodynamics Dorogokupets, Peter I. Physics and Chemistry of Minerals, Vol. 37, Issue 9 https://doi.org/10.1007/s00269-010-0367-2	journal	April 2010
A quantitative model for describing crystal nucleation in pressurized solidification during squeeze casting Han, Zhiqiang; Huang, Xiaoran; Luo, Alan A. Scripta Materialia, Vol. 66, Issue 5 https://doi.org/10.1016/j.scriptamat.2011.10.041	journal	March 2012
Bulk metallic glasses Wang, W. H.; Dong, C.; Shek, C. H. Materials Science and Engineering: R: Reports, Vol. 44, Issue 2-3 https://doi.org/10.1016/j.mser.2004.03.001	journal	June 2004
Bulk metallic glasses Schneider, Susanne Journal of Physics: Condensed Matter, Vol. 13, Issue 34 https://doi.org/10.1088/0953-8984/13/34/316	journal	August 2001
New challenges for the pressure evolution of the glass temperature Rzoska, Sylwester J. arXiv https://doi.org/10.48550/arxiv.1707.04786	preprint	January 2017

Similar Records

Pressure-induced spin crossover in a Fe₇₈Si₉B₁₃ metallic glass

Journal Article · Thu Apr 22 00:00:00 EDT 2021 · Journal of Applied Physics · OSTI ID:1440609

Liang, Tao; Zhang, Fei; Zhang, Xin; +10 more

Multi-stage Devitrification Behavior of Mg₆₅Cu₂₅Tb₁₀ Bulk Metallic Glass

Journal Article · Tue Jan 01 00:00:00 EST 2008 · Metallurgical and Materials Transactions A · OSTI ID:1440609

Yang, Ling; Wang, Xun-Li; Stoica, Alexandru Dan; +3 more

Effect of hydriding on the electron structure of the metallic glasses Fe sub 78 Si sub 9 B sub 13 and Co sub 78 Si sub 9 B sub 13

Journal Article · Thu Mar 01 00:00:00 EST 1990 · Materials Characterization; (USA) · OSTI ID:1440609

Kolodziej, H B; Jakubczyk, E; Jakubczyk, M; +2 more

Related Subjects

36 MATERIALS SCIENCE
Crystallography
Metal oxides
Chemical elements
Glassy dynamics
Amorphous materials
Diffraction
Transition metals
Scanning electron microscopy
Alloys
X-rays

Title: High pressure high temperature devitrification of Fe78B13Si9 metallic glass with simultaneous x-ray structural characterization

Citation Formats

References (49)

Similar Records

Related Subjects

Title: High pressure high temperature devitrification of Fe₇₈B₁₃Si₉ metallic glass with simultaneous x-ray structural characterization