The Power of Non-Hydrolytic Sol-Gel Chemistry: A Review

Styskalik, Ales; Skoda, David; Barnes, Craig; Pinkas, Jiri

doi:10.3390/catal7060168

Title: The Power of Non-Hydrolytic Sol-Gel Chemistry: A Review

Journal Article · Thu May 25 00:00:00 EDT 2017 · Catalysts

DOI:https://doi.org/10.3390/catal7060168· OSTI ID:1429076

Styskalik, Ales ^[1]; Skoda, David ^[2]; Barnes, Craig ^[3];

^[4]

Masaryk Univ., Brno (Czech Republic). Dept. of Chemistry and Central European Inst. of Technology; Univ. of Tennessee, Knoxville, TN (United States). Dept. of Chemistry
Tomas Bata Univ., Zlin (Czech Republic). Centre of Polymer Systems
Univ. of Tennessee, Knoxville, TN (United States). Dept. of Chemistry
Masaryk Univ., Brno (Czech Republic). Dept. of Chemistry and Central European Inst. of Technology

This review is devoted to non-hydrolytic sol-gel chemistry. During the last 25 years, non-hydrolytic sol-gel (NHSG) techniques were found to be attractive and versatile methods for the preparation of oxide materials. Compared to conventional hydrolytic approaches, the NHSG route allows reaction control at the atomic scale resulting in homogeneous and well defined products. Due to these features and the ability to design specific materials, the products of NHSG reactions have been used in many fields of application. The aim of this review therefore is to present an overview of NHSG research in recent years with an emphasis on the syntheses of mixed oxides, silicates and phosphates. The first part of the review highlights well known condensation reactions with some deeper insights into their mechanism and also presents novel condensation reactions established in NHSG chemistry in recent years. In the second section we discuss porosity control and novel compositions of selected materials. In the last part, the applications of NHSG derived materials as heterogeneous catalysts and supports, luminescent materials and electrode materials in Li-ion batteries are described.

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Research Organization:: Univ. of Tennessee, Knoxville, TN (United States); Purdue Univ., West Lafayette, IN (United States)

Sponsoring Organization:: USDOE Office of Science (SC), Basic Energy Sciences (BES); Ministry of Education, Youth and Sports (MSMT) (Czech Republic)

Grant/Contract Number:: FG02-01ER15259; SC0000997

OSTI ID:: 1429076

Journal Information:: Catalysts, Vol. 7, Issue 6; ISSN 2073-4344

Publisher:: MDPICopyright Statement

Country of Publication:: United States

Language:: English

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Cited by: 70 works

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Hydrolysis of organometallic and metal-amide precursors: synthesis routes to oxo-bridged heterometallic complexes, metal-oxo clusters and metal oxide nanoparticles. Garden, Ja; Pike, Sebastian Apollo - University of Cambridge Repository https://doi.org/10.17863/cam.22967	text	January 2018
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