Quantitative texture analysis at the WAND2 and HIDRA diffractometers
Abstract
Data collection and analysis strategies have been developed for efficient and reliable crystallographic texture measurements at two recently upgraded neutron diffractometers: the Wide Angle Neutron Diffractometer Squared (WAND2) and the High Intensity Diffractometer for Residual Stress Analysis (HIDRA) at the High Flux Isotope Reactor located at Oak Ridge National Laboratory. These methods are demonstrated using measurements on a variety of textured samples, including multi-phase steel composites and polycrystalline calcite (CaCO3). Reference measurements were also made at VULCAN, the engineering diffractometer located at the Spallation Neutron Source. The texture data obtained on the different instruments are in agreement, and WAND2 is more time efficient than HIDRA. Two analysis methods were investigated, single-peak fitting to obtain individual pole figures for inversion and Rietveld texture analysis using MAUD. Here, the impact of the differences between the various textures obtained was evaluated through the calculation of diffraction elastic constants, which is one application of the texture data collected. Both instruments were found to provide texture data that are suitable for complementing other analyses, such as residual stress mapping.
- Authors:
-
[2];
[2];
[2];
[2];
[2];
- Univ. of Virginia, Charlottesville, VA (United States)
- Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
- Publication Date:
- Research Org.:
- Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1897000
- Grant/Contract Number:
- AC05-00OR22725
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Applied Crystallography (Online)
- Additional Journal Information:
- Journal Name: Journal of Applied Crystallography (Online); Journal Volume: 55; Journal Issue: 6; Journal ID: ISSN 1600-5767
- Publisher:
- International Union of Crystallography
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 47 OTHER INSTRUMENTATION; crystallographic texture; neutron diffraction; Rietveld texture analysis
Citation Formats
Peterson, Nathan E., Fancher, Christopher M., Frontzek, Matthias D., Bunn, Jeffrey R., Payzant, Andrew, An, Ke, and Agnew, Sean R. Quantitative texture analysis at the WAND2 and HIDRA diffractometers. United States: N. p., 2022.
Web. doi:10.1107/s1600576722009013.
Peterson, Nathan E., Fancher, Christopher M., Frontzek, Matthias D., Bunn, Jeffrey R., Payzant, Andrew, An, Ke, & Agnew, Sean R. Quantitative texture analysis at the WAND2 and HIDRA diffractometers. United States. https://doi.org/10.1107/s1600576722009013
Peterson, Nathan E., Fancher, Christopher M., Frontzek, Matthias D., Bunn, Jeffrey R., Payzant, Andrew, An, Ke, and Agnew, Sean R. Thu .
"Quantitative texture analysis at the WAND2 and HIDRA diffractometers". United States. https://doi.org/10.1107/s1600576722009013. https://www.osti.gov/servlets/purl/1897000.
@article{osti_1897000,
title = {Quantitative texture analysis at the WAND2 and HIDRA diffractometers},
author = {Peterson, Nathan E. and Fancher, Christopher M. and Frontzek, Matthias D. and Bunn, Jeffrey R. and Payzant, Andrew and An, Ke and Agnew, Sean R.},
abstractNote = {Data collection and analysis strategies have been developed for efficient and reliable crystallographic texture measurements at two recently upgraded neutron diffractometers: the Wide Angle Neutron Diffractometer Squared (WAND2) and the High Intensity Diffractometer for Residual Stress Analysis (HIDRA) at the High Flux Isotope Reactor located at Oak Ridge National Laboratory. These methods are demonstrated using measurements on a variety of textured samples, including multi-phase steel composites and polycrystalline calcite (CaCO3). Reference measurements were also made at VULCAN, the engineering diffractometer located at the Spallation Neutron Source. The texture data obtained on the different instruments are in agreement, and WAND2 is more time efficient than HIDRA. Two analysis methods were investigated, single-peak fitting to obtain individual pole figures for inversion and Rietveld texture analysis using MAUD. Here, the impact of the differences between the various textures obtained was evaluated through the calculation of diffraction elastic constants, which is one application of the texture data collected. Both instruments were found to provide texture data that are suitable for complementing other analyses, such as residual stress mapping.},
doi = {10.1107/s1600576722009013},
journal = {Journal of Applied Crystallography (Online)},
number = 6,
volume = 55,
place = {United States},
year = {Thu Oct 27 00:00:00 EDT 2022},
month = {Thu Oct 27 00:00:00 EDT 2022}
}
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