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Title: On the efficacy of post-build thermomechanical treatments to improve properties of Zirconium fabricated using ultrasonic additive manufacturing

Abstract

Here, hot-isostatic pressing has been applied to Zirconium plate fabricated using the ultrasonic additive manufacturing (UAM) technique to enhance interfacial bond quality. Specimens heated to 800 C for 1 h at 100 MPa pressure showed grain growth across many prior foil-to-foil interfaces, thereby increasing foil adhesion. In addition to the material softening induced by a loss of Hall-Petch strengthening, premature failure of specimens loaded parallel to the build direction was observed. Premature specimen failure was attributed to the local delamination at prior foil-to-foil boundaries where grain growth was pinned by Ti impurities introduced during the UAM process via the interaction between a Ti-alloy buffer foil and the welded Zr-foils underneath. In addition, the presence of Ti along select foil interfaces resulted in the nucleation and growth of secondary (Zr,Ti)(Fe,Cr) laves phases during higher-temperature thermomechanical processing. Using a combination of micro-scale X-ray computed tomography, fractography, and in-situ digital image correlation, the effect of defects along prior foil-to-foil boundaries was revealed as delamination-assisted plasticity accelerated specimen failure in preferred tensile orientations. These findings underscore the importance of impurity control when optimizing weld quality of higher-strength material systems using ultrasonic welding.

Authors:
 [1]; ORCiD logo [1]; ORCiD logo [1];  [1]; ORCiD logo [1]; ORCiD logo [1]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Publication Date:
Research Org.:
Oak Ridge National Laboratory (ORNL), Oak Ridge, TN (United States)
Sponsoring Org.:
USDOE National Nuclear Security Administration (NNSA), Office of Defense Nuclear Nonproliferation
OSTI Identifier:
1890328
Grant/Contract Number:  
AC05-00OR22725
Resource Type:
Accepted Manuscript
Journal Name:
Additive Manufacturing
Additional Journal Information:
Journal Volume: 59; Journal Issue: A; Journal ID: ISSN 2214-8604
Publisher:
Elsevier
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Ultrasonic additive manufacturing; Zirconium; Grain growth; Tensile test; Electron backscatter diffraction (EBSD); X-ray tomography; Hot isostatic pressing

Citation Formats

Massey, Caleb P., Gussev, Maxim N., Havrilak, Cody J., Seibert, Rachel L., Cakmak, Ercan, and Nelson, Andrew T. On the efficacy of post-build thermomechanical treatments to improve properties of Zirconium fabricated using ultrasonic additive manufacturing. United States: N. p., 2022. Web. doi:10.1016/j.addma.2022.103110.
Massey, Caleb P., Gussev, Maxim N., Havrilak, Cody J., Seibert, Rachel L., Cakmak, Ercan, & Nelson, Andrew T. On the efficacy of post-build thermomechanical treatments to improve properties of Zirconium fabricated using ultrasonic additive manufacturing. United States. https://doi.org/10.1016/j.addma.2022.103110
Massey, Caleb P., Gussev, Maxim N., Havrilak, Cody J., Seibert, Rachel L., Cakmak, Ercan, and Nelson, Andrew T. Wed . "On the efficacy of post-build thermomechanical treatments to improve properties of Zirconium fabricated using ultrasonic additive manufacturing". United States. https://doi.org/10.1016/j.addma.2022.103110. https://www.osti.gov/servlets/purl/1890328.
@article{osti_1890328,
title = {On the efficacy of post-build thermomechanical treatments to improve properties of Zirconium fabricated using ultrasonic additive manufacturing},
author = {Massey, Caleb P. and Gussev, Maxim N. and Havrilak, Cody J. and Seibert, Rachel L. and Cakmak, Ercan and Nelson, Andrew T.},
abstractNote = {Here, hot-isostatic pressing has been applied to Zirconium plate fabricated using the ultrasonic additive manufacturing (UAM) technique to enhance interfacial bond quality. Specimens heated to 800 C for 1 h at 100 MPa pressure showed grain growth across many prior foil-to-foil interfaces, thereby increasing foil adhesion. In addition to the material softening induced by a loss of Hall-Petch strengthening, premature failure of specimens loaded parallel to the build direction was observed. Premature specimen failure was attributed to the local delamination at prior foil-to-foil boundaries where grain growth was pinned by Ti impurities introduced during the UAM process via the interaction between a Ti-alloy buffer foil and the welded Zr-foils underneath. In addition, the presence of Ti along select foil interfaces resulted in the nucleation and growth of secondary (Zr,Ti)(Fe,Cr) laves phases during higher-temperature thermomechanical processing. Using a combination of micro-scale X-ray computed tomography, fractography, and in-situ digital image correlation, the effect of defects along prior foil-to-foil boundaries was revealed as delamination-assisted plasticity accelerated specimen failure in preferred tensile orientations. These findings underscore the importance of impurity control when optimizing weld quality of higher-strength material systems using ultrasonic welding.},
doi = {10.1016/j.addma.2022.103110},
journal = {Additive Manufacturing},
number = A,
volume = 59,
place = {United States},
year = {Wed Aug 24 00:00:00 EDT 2022},
month = {Wed Aug 24 00:00:00 EDT 2022}
}

Works referenced in this record:

Ultrasonic additive manufacturing of 4130 steel using Ni interlayers
journal, May 2019

  • Kuo, Chih-Hsiang; Sridharan, Niyanth; Han, Tianyang
  • Science and Technology of Welding and Joining, Vol. 24, Issue 5
  • DOI: 10.1080/13621718.2019.1607486

Effect of post weld heat treatment on the 6061 aluminum alloy produced by ultrasonic additive manufacturing
journal, January 2017


Neutron diffraction study of atomic bonding properties in the hydrogen-absorbing Zr(AlxFe1−x)2 system
journal, May 1997


Power consumption and friction coefficient in the ultrasonic consolidation of aluminium alloys
journal, November 2016


Dissimilar metals deposition by directed energy based on powder-fed laser additive manufacturing
journal, July 2019


High-temperature strain monitoring of stainless steel using fiber optics embedded in ultrasonically consolidated nickel layers
journal, July 2019

  • Petrie, Christian M.; Sridharan, Niyanth; Hehr, Adam
  • Smart Materials and Structures, Vol. 28, Issue 8
  • DOI: 10.1088/1361-665X/ab2a27

Rationalization of anisotropic mechanical properties of Al-6061 fabricated using ultrasonic additive manufacturing
journal, September 2016


Transmission electron microscopy of an ultrasonically consolidated copper–aluminum interface
journal, July 2014

  • Sietins, Jennifer M.; Gillespie, John W.; Advani, Suresh G.
  • Journal of Materials Research, Vol. 29, Issue 17
  • DOI: 10.1557/jmr.2014.176

Phase stability and neutron diffraction studies of Laves phases Zr(Cr1−M )2 with M = Mn, Fe, Co, Ni, Cu and 0 < x < 0.2 and their hydrides
journal, March 1995


Ultrasonic additive manufacturing of zirconium: Pilot results
journal, November 2021


Specimen size effects on the tensile properties of JPCA and JFMS
journal, December 2000


Laser-Based Additive Manufacturing of Zirconium
journal, March 2018

  • Sahasrabudhe, Himanshu; Bandyopadhyay, Amit
  • Applied Sciences, Vol. 8, Issue 3
  • DOI: 10.3390/app8030393

Deformation and fracture characteristics of zirconium plate produced via ultrasonic additive manufacturing
journal, October 2021

  • Massey, Caleb P.; Bibhanshu, Nitish; Gussev, Maxim N.
  • Journal of Materials Research, Vol. 37, Issue 1
  • DOI: 10.1557/s43578-021-00380-6

Embedded metallized optical fibers for high temperature applications
journal, April 2019

  • Petrie, Christian M.; Sridharan, Niyanth; Subramanian, Mohan
  • Smart Materials and Structures, Vol. 28, Issue 5
  • DOI: 10.1088/1361-665X/ab0b4e