Nanocellulose Dewatering and Drying: Current State and Future Perspectives

Sinquefield, Scott; Ciesielski, Peter N.; Li, Kai; Gardner, Douglas J.; Ozcan, Soydan

doi:10.1021/acssuschemeng.0c01797

Title: Nanocellulose Dewatering and Drying: Current State and Future Perspectives

Abstract

The knowledge base for nanocellulose (NC) has grown exponentially over the past two decades and continues to expand with the increasing number of potential applications demonstrated in the literature and the patent space. NC has multiple forms depending on the starting cellulose source and the specific process used to produce it. Its high degree of surface reactivity makes it an ideal support structure for a wide variety of functional groups, leading to the ability to engineer materials for very specific applications. However, removing water from an NC suspension, e.g., dewatering and drying, while retaining the nanoscale properties of the NC remains a significant challenge to successful commercialization of NC materials. Processes for dewatering and drying of NC are desirable because of the high transport costs of shipping dilute aqueous suspensions, as well as end-use application requirements. Therefore, the development of nondestructive, cost-effective, scalable, and environmentally friendly dewatering and drying processes is important for commercial deployment of NC applications. This review addresses the current state of published knowledge on NC dewatering and drying and identifies research gaps that could be further explored in a precompetitive context to accelerate commercialization.

Authors:

Sinquefield, Scott ^[1];

^[2];

^[3]; Gardner, Douglas J. ^[4];

^[5]

Georgia Inst. of Technology, Atlanta, GA (United States). Renewable Bioproducts Inst.
National Renewable Energy Lab. (NREL), Golden, CO (United States). Biosciences Center
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Univ. of Maine, Orono, ME (United States)
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Univ. of Tennessee, Knoxville, TN (United States)

Publication Date:: Mon Jun 08 00:00:00 EDT 2020

Research Org.:: Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); National Renewable Energy Lab. (NREL), Golden, CO (United States)

Sponsoring Org.:: USDOE Office of Energy Efficiency and Renewable Energy (EERE), Sustainable Transportation Office. Bioenergy Technologies Office

OSTI Identifier:: 1649340

Alternate Identifier(s):: OSTI ID: 1659860

Report Number(s):: NREL/JA-2700-76238
Journal ID: ISSN 2168-0485

Grant/Contract Number:: AC05-00OR22725; AC36-08GO28308

Resource Type:: Accepted Manuscript

Journal Name:: ACS Sustainable Chemistry & Engineering

Additional Journal Information:: Journal Volume: 8; Journal Issue: 26; Journal ID: ISSN 2168-0485

Publisher:: American Chemical Society (ACS)

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; Nanocellulose; dewatering; drying; cellulose nanofibrils; cellulose nanocrystals; 29 EE - Bioenergy Technologies Office (EE-3B); nanocellulose

Citation Formats


                    Sinquefield, Scott, Ciesielski, Peter N., Li, Kai, Gardner, Douglas J., and Ozcan, Soydan. Nanocellulose Dewatering and Drying: Current State and Future Perspectives.  United States: N. p., 2020. 
Web.  doi:10.1021/acssuschemeng.0c01797.

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                    Sinquefield, Scott, Ciesielski, Peter N., Li, Kai, Gardner, Douglas J., & Ozcan, Soydan. Nanocellulose Dewatering and Drying: Current State and Future Perspectives.  United States.  https://doi.org/10.1021/acssuschemeng.0c01797

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                    Sinquefield, Scott, Ciesielski, Peter N., Li, Kai, Gardner, Douglas J., and Ozcan, Soydan. Mon .  
"Nanocellulose Dewatering and Drying: Current State and Future Perspectives".  United States.  https://doi.org/10.1021/acssuschemeng.0c01797.  https://www.osti.gov/servlets/purl/1649340.

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@article{osti_1649340,

  title        = {Nanocellulose Dewatering and Drying: Current State and Future Perspectives},

  author       = {Sinquefield, Scott and Ciesielski, Peter N. and Li, Kai and Gardner, Douglas J. and Ozcan, Soydan},

  abstractNote = {The knowledge base for nanocellulose (NC) has grown exponentially over the past two decades and continues to expand with the increasing number of potential applications demonstrated in the literature and the patent space. NC has multiple forms depending on the starting cellulose source and the specific process used to produce it. Its high degree of surface reactivity makes it an ideal support structure for a wide variety of functional groups, leading to the ability to engineer materials for very specific applications. However, removing water from an NC suspension, e.g., dewatering and drying, while retaining the nanoscale properties of the NC remains a significant challenge to successful commercialization of NC materials. Processes for dewatering and drying of NC are desirable because of the high transport costs of shipping dilute aqueous suspensions, as well as end-use application requirements. Therefore, the development of nondestructive, cost-effective, scalable, and environmentally friendly dewatering and drying processes is important for commercial deployment of NC applications. This review addresses the current state of published knowledge on NC dewatering and drying and identifies research gaps that could be further explored in a precompetitive context to accelerate commercialization.},

  doi          = {10.1021/acssuschemeng.0c01797},

  journal      = {ACS Sustainable Chemistry & Engineering},

  number       = 26,

  volume       = 8,

  place        = {United States},

  year         = {Mon Jun 08 00:00:00 EDT 2020},

  month        = {Mon Jun 08 00:00:00 EDT 2020}

}

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Eyholzer, Ch.; Bordeanu, N.; Lopez-Suevos, F.
Cellulose, Vol. 17, Issue 1
DOI: 10.1007/s10570-009-9372-3

Drying of a cellulose II gel: effect of physical modification and redispersibility in water
journal, January 2017

Beaumont, Marco; König, Jakob; Opietnik, Martina
Cellulose, Vol. 24, Issue 3
DOI: 10.1007/s10570-016-1166-9

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Title: Nanocellulose Dewatering and Drying: Current State and Future Perspectives

Abstract

Citation Formats

In Vivo Evaluation of the Pulmonary Toxicity of Cellulose Nanocrystals: A Renewable and Sustainable Nanomaterial of the Future journal, May 2014

Importance of Agricultural and Industrial Waste in the Field of Nanocellulose and Recent Industrial Developments of Wood Based Nanocellulose: A Review journal, February 2018

Review of nanocellulose for sustainable future materials journal, April 2015

Cellulose nanomaterials: promising sustainable nanomaterials for application in water/wastewater treatment processes journal, January 2018

A review on nanocellulosic fibres as new material for sustainable packaging: Process and applications journal, October 2016

Review of Hydrogels and Aerogels Containing Nanocellulose journal, April 2017

Cellulose nanocrystals and related nanocomposites: Review of some properties and challenges journal, April 2014

Current characterization methods for cellulose nanomaterials journal, January 2018

Preparation, properties and applications of nanocellulosic materials journal, May 2017

Overview of Cellulose Nanomaterials, Their Capabilities and Applications journal, July 2016

Production of cellulose nanofibrils: A review of recent advances journal, December 2016

Review of Nanocellulose Polymer Composite Characteristics and Challenges journal, December 2016

A review of cellulose nanocrystals and nanocomposites journal, May 2011

A cellulose nanocrystal-based composite electrolyte with superior dimensional stability for alkaline fuel cell membranes journal, January 2015

Green nanomaterials: On track for a sustainable future journal, August 2015

Nanocellulose, a Versatile Green Platform: From Biosources to Materials and Their Applications journal, November 2018

High modulus biocomposites via additive manufacturing: Cellulose nanofibril networks as “microsponges” journal, September 2019

Advanced Materials through Assembly of Nanocelluloses journal, March 2018

Nanocellulose, a tiny fiber with huge applications journal, June 2016

Market projections of cellulose nanomaterial-enabled products ? Part 1: Applications journal, June 2014

Market projections of cellulose nanomaterial-enabled products - Part 2: Volume estimates journal, July 2014

Studies on Bound Water of Cellulose by Differential Scanning Calorimetry journal, September 1981

Quantification of water in different states of interaction with wood pulp fibres journal, December 1996

Crystal Structure and Hydrogen-Bonding System in Cellulose Iβ from Synchrotron X-ray and Neutron Fiber Diffraction journal, August 2002

Crystal Structure and Hydrogen Bonding System in Cellulose I α from Synchrotron X-ray and Neutron Fiber Diffraction journal, November 2003

Hydrophilicity and Lipophilicity of Cellulose Crystal Surfaces journal, October 2001

Diffraction from nonperiodic models of cellulose crystals journal, January 2012

Water Structuring over the Hydrophobic Surface of Cellulose journal, November 2014

Nanocellulose–surfactant interactions journal, May 2017

Key advances in the chemical modification of nanocelluloses journal, January 2014

Nanofibrillated Cellulose Surface Modification: A Review journal, May 2013

Production of nanocrystalline cellulose from lignocellulosic biomass: Technology and applications journal, April 2013

Effect of Reaction Conditions on the Properties and Behavior of Wood Cellulose Nanocrystal Suspensions journal, March 2005

Single-Step Method for the Isolation and Surface Functionalization of Cellulosic Nanowhiskers journal, February 2009

Cellulose Nanocrystals: Chemistry, Self-Assembly, and Applications journal, June 2010

Multifunctional Cellulolytic Enzymes Outperform Processive Fungal Cellulases for Coproduction of Nanocellulose and Biofuels journal, February 2017

Electrokinetic properties of processed cellulose fibers journal, September 1998

Wettability of cotton fabric by aqueous solutions of surfactants with different structures journal, January 2007

Interaction of the Anionic Surfactant SDS with a Cellulose Thin Film and the Role of Electrolyte and Poyelectrolyte. 2 Hydrophilic Cellulose journal, June 2012

TEMPO-oxidized cellulose nanofibers journal, January 2011

Reduction of water wettability of nanofibrillated cellulose by adsorption of cationic surfactants journal, December 2010

Hydrophobic cellulose nanocrystals modified with quaternary ammonium salts journal, January 2012

Dewatering Behavior of a Wood-Cellulose Nanofibril Particulate System journal, October 2019

Sonication-assisted surface modification method to expedite the water removal from cellulose nanofibers for use in nanopapers and paper making journal, October 2018

The Influence of Ionic Strength on the Electroassisted Filtration of Microcrystalline Cellulose journal, October 2017

Electroosmotic dewatering of cellulose nanocrystals journal, March 2018

Flocculation behavior of cellulose nanofibrils under different salt conditions and its impact on network strength and dewatering ability journal, October 2015

The influence of shear on the dewatering of high consistency nanofibrillated cellulose furnishes journal, June 2013

Micro nanofibrillated cellulose (MNFC) gel dewatering induced at ultralow-shear in presence of added colloidally-unstable particles journal, January 2017

Effect of fibril length, aspect ratio and surface charge on ultralow shear-induced structuring in micro and nanofibrillated cellulose aqueous suspensions journal, November 2017

The role of MFC/NFC swelling in the rheological behavior and dewatering of high consistency furnishes journal, October 2013

Acid dissociation of surface bound water on cellulose nanofibrils in aqueous micro nanofibrillated cellulose (MNFC) gel revealed by adsorption of calcium carbonate nanoparticles under the application of ultralow shear journal, June 2017

Consolidation and dewatering of a microfibrillated cellulose fiber composite paper in wet pressing journal, July 2015

Dewatering of Biomaterials by Mechanical Thermal Expression journal, August 2006

WtF-Nano: One-Pot Dewatering and Water-Free Topochemical Modification of Nanocellulose in Ionic Liquids or γ-Valerolactone journal, November 2017

Ionic liquids for sustainable processes: Liquid metal catalysis journal, June 2018

Charge reversal system with cationized cellulose nanocrystals to promote dewatering of a cellulosic fiber suspension journal, September 2017

Drying techniques applied to cellulose nanofibers journal, February 2016

Drying cellulose nanofibrils: in search of a suitable method journal, December 2011

Production and modification of nanofibrillated cellulose using various mechanical processes: A review journal, January 2014

Strong and Tough Cellulose Nanofibrils Composite Films: Mechanism of Synergetic Effect of Hydrogen Bonds and Ionic Interactions journal, August 2019

Influence of drying restraint on physical and mechanical properties of nanofibrillated cellulose films journal, January 2014

Purification and drying of bromelain journal, January 2009

Influence of drying method on the material properties of nanocellulose I: thermostability and crystallinity journal, August 2013

Building dry powder formulations using supercritical CO 2 spray drying journal, June 2017

In-situ modification of cellulose nanofibrils by organosilanes during spray drying journal, December 2016

Maleic anhydride polypropylene modified cellulose nanofibril polypropylene nanocomposites with enhanced impact strength journal, September 2014

Aerogels from nanofibrillated cellulose with tunable oleophobicity journal, January 2010

Nanocellulose-based foams and aerogels: processing, properties, and applications journal, January 2017

Self-Assembling Behavior of Cellulose Nanoparticles during Freeze-Drying: Effect of Suspension Concentration, Particle Size, Crystal Structure, and Surface Charge journal, April 2013

Freeze-Casting of Porous Biomaterials: Structure, Properties and Opportunities journal, March 2010

The effect of drying technique of nanocellulose dispersions on properties of dried materials journal, February 2012

Spray-freeze-drying: A novel process for the drying of foods and bioproducts journal, February 2015

Spray freezing into liquid versus spray-freeze drying: Influence of atomization on protein aggregation and biological activity journal, January 2006

Effect of drying conditions on cellulose nanocrystal (CNC) agglomerate porosity and dispersibility in polymer nanocomposites journal, July 2014

Fabrication and characterization of nano-cellulose aerogels via supercritical CO2 drying technology journal, November 2016

Butanol-mediated oven-drying of nanocellulose with enhanced dehydration rate and aqueous re-dispersion journal, October 2017

In Vivo Evaluation of the Pulmonary Toxicity of Cellulose Nanocrystals: A Renewable and Sustainable Nanomaterial of the Future
journal, May 2014

Importance of Agricultural and Industrial Waste in the Field of Nanocellulose and Recent Industrial Developments of Wood Based Nanocellulose: A Review
journal, February 2018

Review of nanocellulose for sustainable future materials
journal, April 2015

Cellulose nanomaterials: promising sustainable nanomaterials for application in water/wastewater treatment processes
journal, January 2018

A review on nanocellulosic fibres as new material for sustainable packaging: Process and applications
journal, October 2016

Review of Hydrogels and Aerogels Containing Nanocellulose
journal, April 2017

Cellulose nanocrystals and related nanocomposites: Review of some properties and challenges
journal, April 2014

Current characterization methods for cellulose nanomaterials
journal, January 2018

Preparation, properties and applications of nanocellulosic materials
journal, May 2017

Overview of Cellulose Nanomaterials, Their Capabilities and Applications
journal, July 2016

Production of cellulose nanofibrils: A review of recent advances
journal, December 2016

Review of Nanocellulose Polymer Composite Characteristics and Challenges
journal, December 2016

A review of cellulose nanocrystals and nanocomposites
journal, May 2011

A cellulose nanocrystal-based composite electrolyte with superior dimensional stability for alkaline fuel cell membranes
journal, January 2015

Green nanomaterials: On track for a sustainable future
journal, August 2015

Nanocellulose, a Versatile Green Platform: From Biosources to Materials and Their Applications
journal, November 2018

High modulus biocomposites via additive manufacturing: Cellulose nanofibril networks as “microsponges”
journal, September 2019

Advanced Materials through Assembly of Nanocelluloses
journal, March 2018

Nanocellulose, a tiny fiber with huge applications
journal, June 2016

Market projections of cellulose nanomaterial-enabled products ? Part 1: Applications
journal, June 2014

Market projections of cellulose nanomaterial-enabled products - Part 2: Volume estimates
journal, July 2014

Studies on Bound Water of Cellulose by Differential Scanning Calorimetry
journal, September 1981

Quantification of water in different states of interaction with wood pulp fibres
journal, December 1996

Crystal Structure and Hydrogen-Bonding System in Cellulose Iβ from Synchrotron X-ray and Neutron Fiber Diffraction
journal, August 2002

Crystal Structure and Hydrogen Bonding System in Cellulose I _α from Synchrotron X-ray and Neutron Fiber Diffraction
journal, November 2003

Hydrophilicity and Lipophilicity of Cellulose Crystal Surfaces
journal, October 2001

Diffraction from nonperiodic models of cellulose crystals
journal, January 2012

Water Structuring over the Hydrophobic Surface of Cellulose
journal, November 2014

Nanocellulose–surfactant interactions
journal, May 2017

Key advances in the chemical modification of nanocelluloses
journal, January 2014

Nanofibrillated Cellulose Surface Modification: A Review
journal, May 2013

Production of nanocrystalline cellulose from lignocellulosic biomass: Technology and applications
journal, April 2013

Effect of Reaction Conditions on the Properties and Behavior of Wood Cellulose Nanocrystal Suspensions
journal, March 2005

Single-Step Method for the Isolation and Surface Functionalization of Cellulosic Nanowhiskers
journal, February 2009

Cellulose Nanocrystals: Chemistry, Self-Assembly, and Applications
journal, June 2010

Multifunctional Cellulolytic Enzymes Outperform Processive Fungal Cellulases for Coproduction of Nanocellulose and Biofuels
journal, February 2017

Electrokinetic properties of processed cellulose fibers
journal, September 1998

Wettability of cotton fabric by aqueous solutions of surfactants with different structures
journal, January 2007

Interaction of the Anionic Surfactant SDS with a Cellulose Thin Film and the Role of Electrolyte and Poyelectrolyte. 2 Hydrophilic Cellulose
journal, June 2012

TEMPO-oxidized cellulose nanofibers
journal, January 2011

Reduction of water wettability of nanofibrillated cellulose by adsorption of cationic surfactants
journal, December 2010

Hydrophobic cellulose nanocrystals modified with quaternary ammonium salts
journal, January 2012

Dewatering Behavior of a Wood-Cellulose Nanofibril Particulate System
journal, October 2019

Sonication-assisted surface modification method to expedite the water removal from cellulose nanofibers for use in nanopapers and paper making
journal, October 2018

The Influence of Ionic Strength on the Electroassisted Filtration of Microcrystalline Cellulose
journal, October 2017

Electroosmotic dewatering of cellulose nanocrystals
journal, March 2018

Flocculation behavior of cellulose nanofibrils under different salt conditions and its impact on network strength and dewatering ability
journal, October 2015

The influence of shear on the dewatering of high consistency nanofibrillated cellulose furnishes
journal, June 2013

Micro nanofibrillated cellulose (MNFC) gel dewatering induced at ultralow-shear in presence of added colloidally-unstable particles
journal, January 2017

Effect of fibril length, aspect ratio and surface charge on ultralow shear-induced structuring in micro and nanofibrillated cellulose aqueous suspensions
journal, November 2017

The role of MFC/NFC swelling in the rheological behavior and dewatering of high consistency furnishes
journal, October 2013

Acid dissociation of surface bound water on cellulose nanofibrils in aqueous micro nanofibrillated cellulose (MNFC) gel revealed by adsorption of calcium carbonate nanoparticles under the application of ultralow shear
journal, June 2017

Consolidation and dewatering of a microfibrillated cellulose fiber composite paper in wet pressing
journal, July 2015

Dewatering of Biomaterials by Mechanical Thermal Expression
journal, August 2006

WtF-Nano: One-Pot Dewatering and Water-Free Topochemical Modification of Nanocellulose in Ionic Liquids or γ-Valerolactone
journal, November 2017

Ionic liquids for sustainable processes: Liquid metal catalysis
journal, June 2018

Charge reversal system with cationized cellulose nanocrystals to promote dewatering of a cellulosic fiber suspension
journal, September 2017

Drying techniques applied to cellulose nanofibers
journal, February 2016

Drying cellulose nanofibrils: in search of a suitable method
journal, December 2011

Production and modification of nanofibrillated cellulose using various mechanical processes: A review
journal, January 2014

Strong and Tough Cellulose Nanofibrils Composite Films: Mechanism of Synergetic Effect of Hydrogen Bonds and Ionic Interactions
journal, August 2019

Influence of drying restraint on physical and mechanical properties of nanofibrillated cellulose films
journal, January 2014

Purification and drying of bromelain
journal, January 2009

Influence of drying method on the material properties of nanocellulose I: thermostability and crystallinity
journal, August 2013

Building dry powder formulations using supercritical CO 2 spray drying
journal, June 2017

In-situ modification of cellulose nanofibrils by organosilanes during spray drying
journal, December 2016

Maleic anhydride polypropylene modified cellulose nanofibril polypropylene nanocomposites with enhanced impact strength
journal, September 2014

Aerogels from nanofibrillated cellulose with tunable oleophobicity
journal, January 2010

Nanocellulose-based foams and aerogels: processing, properties, and applications
journal, January 2017

Self-Assembling Behavior of Cellulose Nanoparticles during Freeze-Drying: Effect of Suspension Concentration, Particle Size, Crystal Structure, and Surface Charge
journal, April 2013

Freeze-Casting of Porous Biomaterials: Structure, Properties and Opportunities
journal, March 2010

The effect of drying technique of nanocellulose dispersions on properties of dried materials
journal, February 2012

Spray-freeze-drying: A novel process for the drying of foods and bioproducts
journal, February 2015

Spray freezing into liquid versus spray-freeze drying: Influence of atomization on protein aggregation and biological activity
journal, January 2006

Effect of drying conditions on cellulose nanocrystal (CNC) agglomerate porosity and dispersibility in polymer nanocomposites
journal, July 2014

Fabrication and characterization of nano-cellulose aerogels via supercritical CO2 drying technology
journal, November 2016

Butanol-mediated oven-drying of nanocellulose with enhanced dehydration rate and aqueous re-dispersion
journal, October 2017

Assembling and Redispersibility of Rice Straw Nanocellulose: Effect of tert -Butanol
journal, October 2014

Water Redispersible Dried Nanofibrillated Cellulose by Adding Sodium Chloride
journal, November 2012

Poly (vinyl alcohol) as a capping agent in oven dried cellulose nanofibrils
journal, January 2018