Visualization of dynamic fiber-matrix interfacial shear debonding
Abstract
To visualize the debonding event in real time for the study of dynamic crack initiation and propagation at the fiber–matrix interface, a modified tension Kolsky bar was integrated with a high-speed synchrotron X-ray phase-contrast imaging setup. In the gage section, the pull-out configuration was utilized to understand the behavior of interfacial debonding between SC-15 epoxy matrix and S-2 glass fiber, tungsten wire, steel wire, and carbon fiber composite Z-pin at pull-out velocities of 2.5 and 5.0 m s–1. The load history and images of the debonding progression were simultaneously recorded. Both S-2 glass fiber and Z-pin experienced catastrophic interfacial debonding whereas tungsten and steel wire experienced both catastrophic debonding and stick–slip behavior. Even though S-2 glass fiber and Z-pin samples exhibited a slight increase and tungsten and steel wire samples exhibited a slight decrease in average peak force and average interfacial shear stress as the pull-out velocities were increased, no statistical difference was found for most properties when the velocity was increased. Furthermore, the debonding behavior for each fiber material is similar with increasing pull-out velocity. Thus, the debonding mechanism, peak force, and interfacial shear stress were rate insensitive as the pull-out velocity doubled from 2.5 to 5.0 m s–1.more »
- Authors:
-
[1];
- Purdue Univ., West Lafayette, IN (United States)
- Argonne National Lab. (ANL), Lemont, IL (United States)
- U.S. Army Research Lab., Adelphi, MD (United States)
- Publication Date:
- Research Org.:
- Argonne National Lab. (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- U.S. Army Research Laboratory, U.S. Army Research Office (ARO); USDOE
- OSTI Identifier:
- 1460090
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Journal of Materials Science
- Additional Journal Information:
- Journal Volume: 53; Journal Issue: 8; Journal ID: ISSN 0022-2461
- Publisher:
- Springer
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 36 MATERIALS SCIENCE; Kolsky bar; high-speed synchrotron x-ray; interfacial shear stress; phase contrast imaging; pull-out technique
Citation Formats
Chu, Jou -Mei, Claus, Benjamin, Parab, Niranjan, O’Brien, Daniel, Sun, Tao, Fezzaa, Kamel, and Chen, Wayne. Visualization of dynamic fiber-matrix interfacial shear debonding. United States: N. p., 2017.
Web. doi:10.1007/s10853-017-1759-1.
Chu, Jou -Mei, Claus, Benjamin, Parab, Niranjan, O’Brien, Daniel, Sun, Tao, Fezzaa, Kamel, & Chen, Wayne. Visualization of dynamic fiber-matrix interfacial shear debonding. United States. https://doi.org/10.1007/s10853-017-1759-1
Chu, Jou -Mei, Claus, Benjamin, Parab, Niranjan, O’Brien, Daniel, Sun, Tao, Fezzaa, Kamel, and Chen, Wayne. Tue .
"Visualization of dynamic fiber-matrix interfacial shear debonding". United States. https://doi.org/10.1007/s10853-017-1759-1. https://www.osti.gov/servlets/purl/1460090.
@article{osti_1460090,
title = {Visualization of dynamic fiber-matrix interfacial shear debonding},
author = {Chu, Jou -Mei and Claus, Benjamin and Parab, Niranjan and O’Brien, Daniel and Sun, Tao and Fezzaa, Kamel and Chen, Wayne},
abstractNote = {To visualize the debonding event in real time for the study of dynamic crack initiation and propagation at the fiber–matrix interface, a modified tension Kolsky bar was integrated with a high-speed synchrotron X-ray phase-contrast imaging setup. In the gage section, the pull-out configuration was utilized to understand the behavior of interfacial debonding between SC-15 epoxy matrix and S-2 glass fiber, tungsten wire, steel wire, and carbon fiber composite Z-pin at pull-out velocities of 2.5 and 5.0 m s–1. The load history and images of the debonding progression were simultaneously recorded. Both S-2 glass fiber and Z-pin experienced catastrophic interfacial debonding whereas tungsten and steel wire experienced both catastrophic debonding and stick–slip behavior. Even though S-2 glass fiber and Z-pin samples exhibited a slight increase and tungsten and steel wire samples exhibited a slight decrease in average peak force and average interfacial shear stress as the pull-out velocities were increased, no statistical difference was found for most properties when the velocity was increased. Furthermore, the debonding behavior for each fiber material is similar with increasing pull-out velocity. Thus, the debonding mechanism, peak force, and interfacial shear stress were rate insensitive as the pull-out velocity doubled from 2.5 to 5.0 m s–1. In conclusion, scanning electron microscope imaging of recovered epoxy beads revealed a snap-back behavior around the meniscus region of the bead for S-2 glass, tungsten, and steel fiber materials at 5.0 m s–1 whereas those at 2.5 m s–1 exhibited no snap-back behavior.},
doi = {10.1007/s10853-017-1759-1},
journal = {Journal of Materials Science},
number = 8,
volume = 53,
place = {United States},
year = {Tue Oct 31 00:00:00 EDT 2017},
month = {Tue Oct 31 00:00:00 EDT 2017}
}
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Works referenced in this record:
In Situ Visual Observation of Fracture Processes in Several High-Performance Fibers
journal, February 2015
- Hudspeth, Matthew; Claus, Ben; Parab, Niranjan
- Journal of Dynamic Behavior of Materials, Vol. 1, Issue 1
A microbond method for determination of the shear strength of a fiber/resin interface
journal, January 1987
- Miller, Bernard; Muri, Pierre; Rebenfeld, Ludwig
- Composites Science and Technology, Vol. 28, Issue 1
Equilibrium conformations of liquid drops on thin cylinders under forces of capillarity. A theory for the roll-up process
journal, March 1986
- Carroll, B. J.
- Langmuir, Vol. 2, Issue 2
Observation of Crack Propagation in Glass Using X-ray Phase Contrast Imaging
journal, October 2014
- Parab, Niranjan D.; Black, John T.; Claus, Benjamin
- International Journal of Applied Glass Science, Vol. 5, Issue 4
Interface strength in glass fibre–polypropylene measured using the fibre pull-out and microbond methods
journal, September 2010
- Yang, L.; Thomason, J. L.
- Composites Part A: Applied Science and Manufacturing, Vol. 41, Issue 9
Improving the delamination resistance of CFRP by stitching—a review
journal, January 1994
- Dransfield, Kimberley; Baillie, Caroline; Mai, Yiu-Wing
- Composites Science and Technology, Vol. 50, Issue 3
Development of a single fiber fragmentation test for high strain rates
journal, January 2000
- Greenfield, M. J.; Pedicini, A.; Penn, L. S.
- International Journal of Adhesion and Adhesives, Vol. 20, Issue 5
Experimental assessment of fracture of individual sand particles at different loading rates
journal, June 2014
- Parab, Niranjan D.; Claus, Benjamin; Hudspeth, Matthew C.
- International Journal of Impact Engineering, Vol. 68
Micromechanics analysis of Kevlar-29 aramid fiber and epoxy resin microdroplet composite by Micro-Raman spectroscopy
journal, September 2006
- Cen, Hao; Kang, Yilan; Lei, Zhenkun
- Composite Structures, Vol. 75, Issue 1-4
The effects of glass-fiber sizings on the strength and energy absorption of the fiber/matrix interphase under high loading rates
journal, February 2001
- Tanoglu, M.; McKnight, S. H.; Palmese, G. R.
- Composites Science and Technology, Vol. 61, Issue 2
High speed synchrotron x-ray phase contrast imaging of dynamic material response to split Hopkinson bar loading
journal, February 2013
- Hudspeth, M.; Claus, B.; Dubelman, S.
- Review of Scientific Instruments, Vol. 84, Issue 2
Microbond method for determination of the shear strength of a fiber/resin interface: Evaluation of experimental parameters
journal, January 1989
- Gaur, Umesh; Miller, Bernard
- Composites Science and Technology, Vol. 34, Issue 1
Comparison of methods for the measurement of fibre/matrix adhesion in composites
journal, January 1992
- Herrera-Franco, P. J.; Drzal, L. T.
- Composites, Vol. 23, Issue 1
A new technique to characterize the fiber/matrix interphase properties under high strain rates
journal, October 2000
- Tanoglu, M.; McKnight, S. H.; Palmese, G. R.
- Composites Part A: Applied Science and Manufacturing, Vol. 31, Issue 10
Dynamic Transverse Debonding of a Single Fiber
journal, October 2016
- Levine, S.; Nie, Y.; Chen, W.
- Journal of Dynamic Behavior of Materials, Vol. 2, Issue 4
NIH Image to ImageJ: 25 years of image analysis
journal, June 2012
- Schneider, Caroline A.; Rasband, Wayne S.; Eliceiri, Kevin W.
- Nature Methods, Vol. 9, Issue 7
In situ observation of fracture processes in high-strength concretes and limestone using high-speed X-ray phase-contrast imaging
journal, January 2017
- Parab, Niranjan D.; Guo, Zherui; Hudspeth, Matthew
- Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences, Vol. 375, Issue 2085
Influence of microbond test parameters on interfacial shear strength of fiber reinforced polymer-matrix composites
journal, September 2017
- Zhi, Chao; Long, Hairu; Miao, Menghe
- Composites Part A: Applied Science and Manufacturing, Vol. 100
High speed X-ray phase contrast imaging of energetic composites under dynamic compression
journal, September 2016
- Parab, Niranjan D.; Roberts, Zane A.; Harr, Michael H.
- Applied Physics Letters, Vol. 109, Issue 13
Measurement and mechanical aspects of the microbond pull-out technique for obtaining fiber/resin interfacial shear strength
journal, January 1991
- Miller, B.; Gaur, U.; Hirt, D.
- Composites Science and Technology, Vol. 42, Issue 1-3
High rate test method for fiber-matrix interface characterization
journal, July 2016
- Tamrakar, Sandeep; (Gama) Haque, Bazle Z.; Gillespie, John W.
- Polymer Testing, Vol. 52
Tensile properties of fibre-reinforced metals: Copper/tungsten and copper/molybdenum
journal, December 1965
- Kelly, A.; Tyson, W. R.
- Journal of the Mechanics and Physics of Solids, Vol. 13, Issue 6
The effect of interfacial radial and shear stress on fibre pull-out in composite materials
journal, November 1973
- Takaku, A.; Arridge, R. G. C.
- Journal of Physics D: Applied Physics, Vol. 6, Issue 17
Works referencing / citing this record:
Understanding mechanical behavior of interfaces in materials
journal, January 2018
- Dongare, Avinash M.; Rajendran, Arunachalam M.; Namburu, Raju
- Journal of Materials Science, Vol. 53, Issue 8
In-Situ Visualization of Tensile Failure in Additively Manufactured 316 L Stainless Steel
journal, July 2019
- Kirk, C. D.; Parab, N. D.; Kedir, N.
- Experimental Mechanics, Vol. 59, Issue 6
Rate effects on fiber–matrix interfacial transverse debonding behavior
journal, October 2019
- Chu, Jou-Mei; Claus, Benjamin; Lim, Boon Him
- Journal of Composite Materials, Vol. 54, Issue 4