Nuclear magnetic resonance probe head design for precision strain control

Kissikov, T.; Sarkar, R.; Bush, B. T.; Lawson, M.; Canfield, P. C.; Curro, N. J.

doi:10.1063/1.5002631

Title: Nuclear magnetic resonance probe head design for precision strain control

Abstract

We present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on the order of 0.3% with a precision of 0.001%. 75As NMR in BaFe2As2 reveals large changes to the electric field gradient and indicates that the strain is homogeneous to within 16% over the volume of the NMR coil.

Authors:

Kissikov, T. ^[1]; Sarkar, R. ^[2]; Bush, B. T. ^[1]; Lawson, M. ^[1]; Canfield, P. C. ^[3];

^[1]

Univ. of California, Davis, CA (United States). Dept. of Physics
TU Dresden, Dresden (Germany). Inst. for Solid State Physics
Ames Lab. and Iowa State Univ., Ames, IA (United States). Dept. of Physics and Astronomy

Publication Date:: Tue Oct 03 00:00:00 EDT 2017

Research Org.:: Ames Lab., Ames, IA (United States)

Sponsoring Org.:: USDOE National Nuclear Security Administration (NNSA); USDOE Office of Science (SC), Basic Energy Sciences (BES) (SC-22). Materials Sciences & Engineering Division; National Science Foundation (NSF); German Research Foundation (DFG)

OSTI Identifier:: 1409367

Alternate Identifier(s):: OSTI ID: 1396312; OSTI ID: 1464758

Report Number(s):: IS-J-9498
Journal ID: ISSN 0034-6748; TRN: US1703196

Grant/Contract Number:: AC02-07CH11358; DMR-1506961; NA0002908; 1143

Resource Type:: Accepted Manuscript

Journal Name:: Review of Scientific Instruments

Additional Journal Information:: Journal Volume: 88; Journal Issue: 10; Journal ID: ISSN 0034-6748

Publisher:: American Institute of Physics (AIP)

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; NMR; strain; piezoelectricity; transition metals; programming languages; thermal effects; connectors; materials analysis; amorphous metals; sensors; magnetic resonance imaging; cryogenics

Citation Formats


                    Kissikov, T., Sarkar, R., Bush, B. T., Lawson, M., Canfield, P. C., and Curro, N. J. Nuclear magnetic resonance probe head design for precision strain control.  United States: N. p., 2017. 
Web.  doi:10.1063/1.5002631.

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                    Kissikov, T., Sarkar, R., Bush, B. T., Lawson, M., Canfield, P. C., & Curro, N. J. Nuclear magnetic resonance probe head design for precision strain control.  United States.  https://doi.org/10.1063/1.5002631

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                    Kissikov, T., Sarkar, R., Bush, B. T., Lawson, M., Canfield, P. C., and Curro, N. J. Tue .  
"Nuclear magnetic resonance probe head design for precision strain control".  United States.  https://doi.org/10.1063/1.5002631.  https://www.osti.gov/servlets/purl/1409367.

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@article{osti_1409367,

  title        = {Nuclear magnetic resonance probe head design for precision strain control},

  author       = {Kissikov, T. and Sarkar, R. and Bush, B. T. and Lawson, M. and Canfield, P. C. and Curro, N. J.},

  abstractNote = {We present the design and construction of an NMR probe to investigate single crystals under strain at cryogenic temperatures. The probe head incorporates a piezoelectric-based apparatus from Razorbill Instruments that enables both compressive and tensile strain tuning up to strain values on the order of 0.3% with a precision of 0.001%. 75As NMR in BaFe2As2 reveals large changes to the electric field gradient and indicates that the strain is homogeneous to within 16% over the volume of the NMR coil.},

  doi          = {10.1063/1.5002631},

  journal      = {Review of Scientific Instruments},

  number       = 10,

  volume       = 88,

  place        = {United States},

  year         = {Tue Oct 03 00:00:00 EDT 2017},

  month        = {Tue Oct 03 00:00:00 EDT 2017}

}

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Works referenced in this record:

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Piezoelectric-based apparatus for strain tuning
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Carrier-Concentration Dependence of the Pseudogap Ground State of Superconducting ${Bi}_{2} {Sr}_{2 - x} {La}_{x} {CuO}_{6 + δ}$ Revealed by ${}^{63, 65}{Cu}$ -Nuclear Magnetic Resonance in Very High Magnetic Fields
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Works referencing / citing this record:

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors
journal, February 2019

Barber, Mark E.; Steppke, Alexander; Mackenzie, Andrew P.
Review of Scientific Instruments, Vol. 90, Issue 2
DOI: 10.1063/1.5075485

Modal learning displacement–strain transformation
journal, July 2019

Deng, Huaxia; Zhang, Haicong; Wang, Jun
Review of Scientific Instruments, Vol. 90, Issue 7
DOI: 10.1063/1.5100905

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors
preprint, January 2018

Barber, Mark E.; Steppke, Alexander; Mackenzie, Andrew P.
arXiv
DOI: 10.48550/arxiv.1810.09573

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Title: Nuclear magnetic resonance probe head design for precision strain control

Abstract

Citation Formats

Surface-dominated conduction up to 240 K in the Kondo insulator SmB6 under strain journal, April 2017

Nonlinear effect of uniaxial pressure on superconductivity in CeCoIn 5 journal, April 2011

NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped Ba ( Fe 1 − x Co x ) 2 As 2 journal, October 2016

Temperature versus doping phase diagrams for Ba ( Fe 1 − x TM x ) 2 As 2 ( TM = Ni , Cu , Cu / Co ) single crystals journal, July 2010

Magnetization studies of the nuclear spin ordered phases of solid 3He in silver sinters journal, August 2005

NMR signal averaging in 62T pulsed fields journal, May 2011

Magnetic properties of URu 2 Si 2 under uniaxial stress by neutron scattering journal, November 2011

Commensurate Itinerant Antiferromagnetism in BaFe 2 As 2 : 75 As-NMR Studies on a Self-Flux Grown Single Crystal journal, November 2008

Strong Increase of Tc of Sr2RuO4 Under Both Tensile and Compressive Strain journal, April 2014

High-temperature silicon-29 NMR investigation of solid and molten silicates journal, January 1990

A device for the application of uniaxial strain to single crystal samples for use in synchrotron radiation experiments journal, October 2015

Piezoelectric-based apparatus for strain tuning journal, June 2014

Carrier-Concentration Dependence of the Pseudogap Ground State of Superconducting Bi 2 Sr 2 − x La x CuO 6 + δ Revealed by Cu 63 , 65 -Nuclear Magnetic Resonance in Very High Magnetic Fields journal, September 2010

Thermal expansion under uniaxial pressure in URu 2 Si 2 journal, March 2013

High-sensitivity NMR beyond 200,000 atmospheres of pressure journal, August 2015

Effect of Biaxial Strain on the Phase Transitions of Ca ( Fe 1 − x Co x ) 2 As 2 journal, March 2017

Commensurate Itinerant Antiferromagnetism in BaFe2As2: 75As-NMR Studies on a Self-Flux Grown Single Crystal text, January 2008

Non-linear effect of uniaxial pressure on superconductivity in CeCoIn5 text, January 2010

Piezoelectric-based apparatus for strain tuning text, January 2014

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors journal, February 2019

Modal learning displacement–strain transformation journal, July 2019

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors preprint, January 2018

Surface-dominated conduction up to 240 K in the Kondo insulator SmB6 under strain
journal, April 2017

Nonlinear effect of uniaxial pressure on superconductivity in CeCoIn $_{5}$
journal, April 2011

NMR study of nematic spin fluctuations in a detwinned single crystal of underdoped $Ba {({Fe}_{1 - x} {Co}_{x})}_{2} {As}_{2}$
journal, October 2016

Temperature versus doping phase diagrams for $Ba {({Fe}_{1 - x} {TM}_{x})}_{2} {As}_{2} (TM = Ni, Cu, Cu / Co)$ single crystals
journal, July 2010

Magnetization studies of the nuclear spin ordered phases of solid 3He in silver sinters
journal, August 2005

NMR signal averaging in 62T pulsed fields
journal, May 2011

Magnetic properties of URu $_{2}$ Si $_{2}$ under uniaxial stress by neutron scattering
journal, November 2011

Commensurate Itinerant Antiferromagnetism in BaFe ₂ As ₂ : ⁷⁵ As-NMR Studies on a Self-Flux Grown Single Crystal
journal, November 2008

Strong Increase of Tc of Sr2RuO4 Under Both Tensile and Compressive Strain
journal, April 2014

High-temperature silicon-29 NMR investigation of solid and molten silicates
journal, January 1990

A device for the application of uniaxial strain to single crystal samples for use in synchrotron radiation experiments
journal, October 2015

Piezoelectric-based apparatus for strain tuning
journal, June 2014

Carrier-Concentration Dependence of the Pseudogap Ground State of Superconducting ${Bi}_{2} {Sr}_{2 - x} {La}_{x} {CuO}_{6 + δ}$ Revealed by ${}^{63, 65}{Cu}$ -Nuclear Magnetic Resonance in Very High Magnetic Fields
journal, September 2010

Thermal expansion under uniaxial pressure in URu $_{2}$ Si $_{2}$
journal, March 2013

High-sensitivity NMR beyond 200,000 atmospheres of pressure
journal, August 2015

Effect of Biaxial Strain on the Phase Transitions of $Ca ({Fe}_{1 - x} {Co}_{x})_{2} {As}_{2}$
journal, March 2017

Commensurate Itinerant Antiferromagnetism in BaFe2As2: 75As-NMR Studies on a Self-Flux Grown Single Crystal
text, January 2008

Non-linear effect of uniaxial pressure on superconductivity in CeCoIn5
text, January 2010

Piezoelectric-based apparatus for strain tuning
text, January 2014

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors
journal, February 2019

Modal learning displacement–strain transformation
journal, July 2019

Piezoelectric-based uniaxial pressure cell with integrated force and displacement sensors
preprint, January 2018