Fluids and Electrolytes under Confinement in Single-Digit Nanopores

Aluru, Narayana R.; Aydin, Fikret; Bazant, Martin Z.; Blankschtein, Daniel; Brozena, Alexandra H.; de Souza, J. Pedro; Elimelech, Menachem; Faucher, Samuel; Fourkas, John T.; Koman, Volodymyr B.; Kuehne, Matthias; Kulik, Heather J.; Li, Hao-Kun; Li, Yuhao; Li, Zhongwu; Majumdar, Arun; Martis, Joel; Misra, Rahul Prasanna; Noy, Aleksandr; Pham, Tuan Anh; Qu, Haoran; Rayabharam, Archith; Reed, Mark A.; Ritt, Cody L.; Schwegler, Eric; Siwy, Zuzanna; Strano, Michael S.; Wang, YuHuang; Yao, Yun-Chiao; Zhan, Cheng; Zhang, Ze

doi:10.1021/acs.chemrev.2c00155

Title: Fluids and Electrolytes under Confinement in Single-Digit Nanopores

Abstract

Confined fluids and electrolyte solutions in nanopores exhibit rich and surprising physics and chemistry that impact the mass transport and energy efficiency in many important natural systems and industrial applications. Existing theories often fail to predict the exotic effects observed in the narrowest of such pores, called single-digit nanopores (SDNs), which have diameters or conduit widths of less than 10 nm, and have only recently become accessible for experimental measurements. What SDNs reveal has been surprising, including a rapidly increasing number of examples such as extraordinarily fast water transport, distorted fluid-phase boundaries, strong ion-correlation and quantum effects, and dielectric anomalies that are not observed in larger pores. Exploiting these effects presents myriad opportunities in both basic and applied research that stand to impact a host of new technologies at the water–energy nexus, from new membranes for precise separations and water purification to new gas permeable materials for water electrolyzers and energy-storage devices. SDNs also present unique opportunities to achieve ultrasensitive and selective chemical sensing at the single-ion and single-molecule limit. In this review article, we summarize the progress on nanofluidics of SDNs, with a focus on the confinement effects that arise in these extremely narrow nanopores. The recent development ofmore »« less

Authors:

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Oden Institute for Computational Engineering and Sciences, Walker Department of Mechanical Engineering, The University of Texas at Austin, Austin, 78712TexasUnited States
Materials Science Division, Physical and Life Science Directorate, Lawrence Livermore National Laboratory, Livermore, California94550, United States
Department of Chemical Engineering, Massachusetts Institute of Technology, Cambridge, Massachusetts02139, United States, Department of Mathematics, Massachusetts Institute of Technology, Cambridge, Massachusetts02139, United States
Department of Chemical Engineering, Massachusetts Institute of Technology, Cambridge, Massachusetts02139, United States
Department of Chemistry and Biochemistry, University of Maryland, College Park, Maryland20742, United States
Department of Chemical and Environmental Engineering, Yale University, New Haven, Connecticut06520-8286, United States
Department of Chemistry and Biochemistry, University of Maryland, College Park, Maryland20742, United States, Institute for Physical Science and Technology, University of Maryland, College Park, Maryland20742, United States, Maryland NanoCenter, University of Maryland, College Park, Maryland20742, United States
Department of Mechanical Engineering, Stanford University, Stanford, California94305, United States
Materials Science Division, Physical and Life Science Directorate, Lawrence Livermore National Laboratory, Livermore, California94550, United States, School of Natural Sciences, University of California Merced, Merced, California95344, United States
Department of Electrical Engineering, Yale University, 15 Prospect Street, New Haven, Connecticut06520, United States
Department of Physics and Astronomy, Department of Chemistry, Department of Biomedical Engineering, University of California, Irvine, Irvine92697, United States
Department of Chemistry and Biochemistry, University of Maryland, College Park, Maryland20742, United States, Maryland NanoCenter, University of Maryland, College Park, Maryland20742, United States

Publication Date:: Fri Mar 10 00:00:00 EST 2023

Research Org.:: Massachusetts Inst. of Technology (MIT), Cambridge, MA (United States); Lawrence Livermore National Laboratory (LLNL), Livermore, CA (United States)

Sponsoring Org.:: USDOE Office of Science (SC), Basic Energy Sciences (BES); USDOE National Nuclear Security Administration (NNSA); National Science Foundation (NSF)

OSTI Identifier:: 1962916

Alternate Identifier(s):: OSTI ID: 1962748; OSTI ID: 2204955

Report Number(s):: LLNL-JRNL-856109
Journal ID: ISSN 0009-2665

Grant/Contract Number:: SC0019112; AC52-07NA27344; 1122374

Resource Type:: Published Article

Journal Name:: Chemical Reviews

Additional Journal Information:: Journal Name: Chemical Reviews Journal Volume: 123 Journal Issue: 6; Journal ID: ISSN 0009-2665

Publisher:: American Chemical Society

Country of Publication:: United States

Language:: English

Subject:: 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY; 36 MATERIALS SCIENCE; Carbon nanotubes; Membranes; Nanofluidics; Nanopores; Nanoporous materials

Citation Formats


                    Aluru, Narayana R., Aydin, Fikret, Bazant, Martin Z., Blankschtein, Daniel, Brozena, Alexandra H., de Souza, J. Pedro, Elimelech, Menachem, Faucher, Samuel, Fourkas, John T., Koman, Volodymyr B., Kuehne, Matthias, Kulik, Heather J., Li, Hao-Kun, Li, Yuhao, Li, Zhongwu, Majumdar, Arun, Martis, Joel, Misra, Rahul Prasanna, Noy, Aleksandr, Pham, Tuan Anh, Qu, Haoran, Rayabharam, Archith, Reed, Mark A., Ritt, Cody L., Schwegler, Eric, Siwy, Zuzanna, Strano, Michael S., Wang, YuHuang, Yao, Yun-Chiao, Zhan, Cheng, and Zhang, Ze. Fluids and Electrolytes under Confinement in Single-Digit Nanopores.  United States: N. p., 2023. 
Web.  doi:10.1021/acs.chemrev.2c00155.

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                    Aluru, Narayana R., Aydin, Fikret, Bazant, Martin Z., Blankschtein, Daniel, Brozena, Alexandra H., de Souza, J. Pedro, Elimelech, Menachem, Faucher, Samuel, Fourkas, John T., Koman, Volodymyr B., Kuehne, Matthias, Kulik, Heather J., Li, Hao-Kun, Li, Yuhao, Li, Zhongwu, Majumdar, Arun, Martis, Joel, Misra, Rahul Prasanna, Noy, Aleksandr, Pham, Tuan Anh, Qu, Haoran, Rayabharam, Archith, Reed, Mark A., Ritt, Cody L., Schwegler, Eric, Siwy, Zuzanna, Strano, Michael S., Wang, YuHuang, Yao, Yun-Chiao, Zhan, Cheng, & Zhang, Ze. Fluids and Electrolytes under Confinement in Single-Digit Nanopores.  United States.  https://doi.org/10.1021/acs.chemrev.2c00155

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                    Aluru, Narayana R., Aydin, Fikret, Bazant, Martin Z., Blankschtein, Daniel, Brozena, Alexandra H., de Souza, J. Pedro, Elimelech, Menachem, Faucher, Samuel, Fourkas, John T., Koman, Volodymyr B., Kuehne, Matthias, Kulik, Heather J., Li, Hao-Kun, Li, Yuhao, Li, Zhongwu, Majumdar, Arun, Martis, Joel, Misra, Rahul Prasanna, Noy, Aleksandr, Pham, Tuan Anh, Qu, Haoran, Rayabharam, Archith, Reed, Mark A., Ritt, Cody L., Schwegler, Eric, Siwy, Zuzanna, Strano, Michael S., Wang, YuHuang, Yao, Yun-Chiao, Zhan, Cheng, and Zhang, Ze. Fri .  
"Fluids and Electrolytes under Confinement in Single-Digit Nanopores".  United States.  https://doi.org/10.1021/acs.chemrev.2c00155.

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@article{osti_1962916,

  title        = {Fluids and Electrolytes under Confinement in Single-Digit Nanopores},

  author       = {Aluru, Narayana R. and Aydin, Fikret and Bazant, Martin Z. and Blankschtein, Daniel and Brozena, Alexandra H. and de Souza, J. Pedro and Elimelech, Menachem and Faucher, Samuel and Fourkas, John T. and Koman, Volodymyr B. and Kuehne, Matthias and Kulik, Heather J. and Li, Hao-Kun and Li, Yuhao and Li, Zhongwu and Majumdar, Arun and Martis, Joel and Misra, Rahul Prasanna and Noy, Aleksandr and Pham, Tuan Anh and Qu, Haoran and Rayabharam, Archith and Reed, Mark A. and Ritt, Cody L. and Schwegler, Eric and Siwy, Zuzanna and Strano, Michael S. and Wang, YuHuang and Yao, Yun-Chiao and Zhan, Cheng and Zhang, Ze},

  abstractNote = {Confined fluids and electrolyte solutions in nanopores exhibit rich and surprising physics and chemistry that impact the mass transport and energy efficiency in many important natural systems and industrial applications. Existing theories often fail to predict the exotic effects observed in the narrowest of such pores, called single-digit nanopores (SDNs), which have diameters or conduit widths of less than 10 nm, and have only recently become accessible for experimental measurements. What SDNs reveal has been surprising, including a rapidly increasing number of examples such as extraordinarily fast water transport, distorted fluid-phase boundaries, strong ion-correlation and quantum effects, and dielectric anomalies that are not observed in larger pores. Exploiting these effects presents myriad opportunities in both basic and applied research that stand to impact a host of new technologies at the water–energy nexus, from new membranes for precise separations and water purification to new gas permeable materials for water electrolyzers and energy-storage devices. SDNs also present unique opportunities to achieve ultrasensitive and selective chemical sensing at the single-ion and single-molecule limit. In this review article, we summarize the progress on nanofluidics of SDNs, with a focus on the confinement effects that arise in these extremely narrow nanopores. The recent development of precision model systems, transformative experimental tools, and multiscale theories that have played enabling roles in advancing this frontier are reviewed. Furthermore, we also identify new knowledge gaps in our understanding of nanofluidic transport and provide an outlook for the future challenges and opportunities at this rapidly advancing frontier.},

  doi          = {10.1021/acs.chemrev.2c00155},

  journal      = {Chemical Reviews},

  number       = 6,

  volume       = 123,

  place        = {United States},

  year         = {Fri Mar 10 00:00:00 EST 2023},

  month        = {Fri Mar 10 00:00:00 EST 2023}

}

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Title: Fluids and Electrolytes under Confinement in Single-Digit Nanopores

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Confinement of Dyes inside Boron Nitride Nanotubes: Photostable and Shifted Fluorescence down to the Near Infrared
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Fabrication of solid-state nanopores with single-nanometre precision
journal, July 2003

Equilibrium ion partitioning between aqueous salt solutions and inhomogeneous ion exchange membranes
journal, November 2018

Solvatochromic shifts of single-walled carbon nanotubes in nonpolar microenvironments
journal, January 2010

Raman spectroscopy of carbon nanotubes
journal, March 2005

Comparison of the Orientational Dynamics of Water Confined in Hydrophobic and Hydrophilic Nanopores
journal, October 2002

Formation of ordered ice nanotubes inside carbon nanotubes
journal, August 2001

Molecular layer-by-layer deposition of highly crosslinked polyamide films
journal, November 2011

Barriers to Superfast Water Transport in Carbon Nanotube Membranes
journal, April 2013

Dielectric dispersion and dielectric friction in electrolyte solutions. I.
journal, December 1977

Probing the Structure of Salt Water under Confinement with First-Principles Molecular Dynamics and Theoretical X-ray Absorption Spectroscopy
journal, September 2012

Solvent–Solvent Correlations across Graphene: The Effect of Image Charges
journal, June 2020

Noise in solid-state nanopores
journal, January 2008

Phase transitions in confined water nanofilms
journal, July 2010

Nanoscale Heterogeneity of Polyamide Membranes Formed by Interfacial Polymerization
journal, May 2003

Enhancing single-wall carbon nanotube properties through controlled endohedral filling
journal, January 2016

Remote Joule heating by a carbon nanotube
journal, April 2012

Langevin-Poisson-EQT: A dipolar solvent based quasi-continuum approach for electric double layers
journal, January 2017

Streaming potential/current measurement system for investigation of liquids confined in extended-nanospace
journal, January 2010

The role of graphene for electrochemical energy storage
journal, December 2014

Encapsulation and Polymerization of White Phosphorus Inside Single-Wall Carbon Nanotubes
journal, June 2017

Anomalously Soft Dynamics of Water in a Nanotube: A Revelation of Nanoscale Confinement
journal, July 2004

Ultrathin graphene-based membrane with precise molecular sieving and ultrafast solvent permeation
journal, November 2017

Ion transport through nanoslits dominated by the effective surface charge
journal, June 2005

Self-assembly of a sulphur-terminated graphene nanoribbon within a single-walled carbon nanotube
journal, August 2011

Generalized Neural-Network Representation of High-Dimensional Potential-Energy Surfaces
journal, April 2007

Luminescence Properties of Individual Empty and Water-Filled Single-Walled Carbon Nanotubes
journal, February 2012

Temperature-dependent gas transport performance of vertically aligned carbon nanotube/parylene composite membranes
journal, January 2014

Single-Molecule Analysis with Solid-State Nanopores
journal, June 2019

Fundamental water and salt transport properties of polymeric materials
journal, January 2014

Acyclic Cucurbit[n]uril Molecular Containers Selectively Solubilize Single-Walled Carbon Nanotubes in Water
journal, April 2012

Properties of metal–water interfaces studied from first principles
journal, December 2009

Fundamental mechanisms of interfacial friction. 1. Relation between adhesion and friction
journal, April 1993

Rectification properties of conically shaped nanopores: consequences of miniaturization
journal, January 2013

Mechanically activated ionic transport across single-digit carbon nanotubes
journal, July 2020

In situ multiphase fluid experiments in hydrothermal carbon nanotubes
journal, August 2001

pH-Regulated Ionic Conductance in a Nanochannel with Overlapped Electric Double Layers
journal, April 2015

Time dependent wettability of graphite upon ambient exposure: The role of water adsorption
journal, August 2014

Uncovering a Universal Molecular Mechanism of Salt Ion Adsorption at Solid/Water Interfaces
journal, January 2021

Confined nanobubbles shape the surface roughness structures of thin film composite polyamide desalination membranes
journal, July 2019

Dehydration as a Universal Mechanism for Ion Selectivity in Graphene and Other Atomically Thin Pores
journal, July 2017

Electrolytic Transport in Modified Carbon Nanotubes
journal, October 2003

Nanoporous Membranes Derived from Block Copolymers: From Drug Delivery to Water Filtration
journal, June 2010

Temperature-dependent Raman spectra of bamboo-like boron nitride nanotubes
journal, January 2014

Scaling Behavior for Ionic Transport and its Fluctuations in Individual Carbon Nanotubes
journal, April 2016

Water in Carbon Nanotubes: Pronounced Anisotropy in Dielectric Dispersion and Its Microscopic Origin
journal, September 2019

Electrical recognition of the twenty proteinogenic amino acids using an aerolysin nanopore
journal, December 2019

Spatial Diffusion of Water in Carbon Nanotubes: From Fickian to Ballistic Motion
journal, October 2011

Ionic transport through sub-10 nm diameter hydrophobic high-aspect ratio nanopores: experiment, theory and simulation
journal, June 2015

Carbon Materials for Chemical Capacitive Energy Storage
journal, September 2011

Four billion people facing severe water scarcity
journal, February 2016

Nanopore Fabrication by Controlled Dielectric Breakdown
journal, March 2014

Fabrication and practical applications of molybdenum disulfide nanopores
journal, March 2019

A biosensing expedition of nanopore: A review
journal, April 2019

Testing the Core/Shell Model of Nanoconfined Water in Reverse Micelles Using Linear and Nonlinear IR Spectroscopy
journal, April 2006

Reticular synthesis and the design of new materials
journal, June 2003

Zeta potential in intact carbonates at reservoir conditions and its impact on oil recovery during controlled salinity waterflooding
journal, April 2020

Two dimensional anisotropic etching in tracked glass
journal, January 2009

Nanofluidic technology for biomolecule applications: a critical review
journal, January 2010

A new family of mesoporous molecular sieves prepared with liquid crystal templates
journal, December 1992

Large scale, selective dispersion of long single-walled carbon nanotubes with high photoluminescence quantum yield by shear force mixing
journal, August 2016

Monolithic nanofluid sieving structures for DNA manipulation
journal, November 1998

CHARMM general force field: A force field for drug-like molecules compatible with the CHARMM all-atom additive biological force fields
journal, January 2009

Nanopores: A journey towards DNA sequencing
journal, June 2012