Structure-dependent performance of TiO2/C as anode material for Na-ion batteries
Abstract
The performance of energy storage materials is highly dependent on their nanostructures. Herein, hierarchical rod-in-tube TiO2 with a uniform carbon coating is synthesized as the anode material for sodium-ion batteries by a facile solvothermal method. This unique structure consists of a tunable nanorod core, interstitial hollow spaces, and a functional nanotube shell assembled from two-dimensional nanosheets. By adjusting the types of solvents used and reaction time, the morphologies of TiO2/C composites can be tuned to nanoparticles, microrods, rod-in-tube structures, or microtubes. Among these materials, rod-in-tube TiO2 with a uniform carbon coating shows the highest electronic conductivity, specific surface area (336.4 m2 g-1), and porosity, and these factors lead to the best sodium storage capability. Benefiting from the unique structural features and improved electronic/ionic conductivity, the as-obtained rod-in-tube TiO2/C in coin cell tests exhibits a high discharge capacity of 277.5 and 153.9 mAh g-1 at 50 and 5000 mA g-1, respectively, and almost 100% capacity retention over 14,000 cycles at 5000 mA g-1. In operando high-energy X-ray diffraction further confirms the stable crystal structure of the rod-in-tube TiO2/C during Na+ insertion/extraction. Finally, this work highlights that nanostructure design is an effective strategy to achieve advanced energy storage materials.
- Authors:
-
- Central South Univ., Changsha (China). Hunan Provincial Key Lab. of Chemical Power Sources, College of Chemistry and Chemical Engineering
- Central South Univ., Changsha (China). Hunan Provincial Key Lab. of Chemical Power Sources, College of Chemistry and Chemical Engineering; Hong Kong Univ. of Science and Technology, Hong Kong (China). Dept. of Chemical and Biological Engineering
- Argonne National Lab. (ANL), Argonne, IL (United States). Chemical Sciences and Engineering Division
- Argonne National Lab. (ANL), Argonne, IL (United States). Advanced Photon Source (APS), X-ray Science Division
- Hong Kong Univ. of Science and Technology, Hong Kong (China). Dept. of Chemical and Biological Engineering
- Argonne National Lab. (ANL), Argonne, IL (United States). Chemical Sciences and Engineering Division; Stanford Univ., CA (United States). Materials Science and Engineering
- Hong Kong Univ. of Science and Technology, Hong Kong (China). Dept. of Chemical and Biological Engineering, and Energy Inst.
- Publication Date:
- Research Org.:
- Argonne National Laboratory (ANL), Argonne, IL (United States)
- Sponsoring Org.:
- National Natural Science Foundation of China (NSFC); USDOE Office of Energy Efficiency and Renewable Energy (EERE), Vehicle Technologies Office (EE-3V); USDOE
- OSTI Identifier:
- 1422570
- Alternate Identifier(s):
- OSTI ID: 1548948
- Grant/Contract Number:
- AC02-06CH11357
- Resource Type:
- Accepted Manuscript
- Journal Name:
- Nano Energy
- Additional Journal Information:
- Journal Volume: 44; Journal Issue: C; Journal ID: ISSN 2211-2855
- Publisher:
- Elsevier
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 25 ENERGY STORAGE; hierarchical rod-in-tube structure; morphology tuning; rate performance; sodium-ion battery; titanium dioxide
Citation Formats
He, Hanna, Gan, Qingmeng, Wang, Haiyan, Xu, Gui-Liang, Zhang, Xiaoyi, Huang, Dan, Fu, Fang, Tang, Yougen, Amine, Khalil, and Shao, Minhua. Structure-dependent performance of TiO2/C as anode material for Na-ion batteries. United States: N. p., 2017.
Web. doi:10.1016/j.nanoen.2017.11.077.
He, Hanna, Gan, Qingmeng, Wang, Haiyan, Xu, Gui-Liang, Zhang, Xiaoyi, Huang, Dan, Fu, Fang, Tang, Yougen, Amine, Khalil, & Shao, Minhua. Structure-dependent performance of TiO2/C as anode material for Na-ion batteries. United States. https://doi.org/10.1016/j.nanoen.2017.11.077
He, Hanna, Gan, Qingmeng, Wang, Haiyan, Xu, Gui-Liang, Zhang, Xiaoyi, Huang, Dan, Fu, Fang, Tang, Yougen, Amine, Khalil, and Shao, Minhua. Wed .
"Structure-dependent performance of TiO2/C as anode material for Na-ion batteries". United States. https://doi.org/10.1016/j.nanoen.2017.11.077. https://www.osti.gov/servlets/purl/1422570.
@article{osti_1422570,
title = {Structure-dependent performance of TiO2/C as anode material for Na-ion batteries},
author = {He, Hanna and Gan, Qingmeng and Wang, Haiyan and Xu, Gui-Liang and Zhang, Xiaoyi and Huang, Dan and Fu, Fang and Tang, Yougen and Amine, Khalil and Shao, Minhua},
abstractNote = {The performance of energy storage materials is highly dependent on their nanostructures. Herein, hierarchical rod-in-tube TiO2 with a uniform carbon coating is synthesized as the anode material for sodium-ion batteries by a facile solvothermal method. This unique structure consists of a tunable nanorod core, interstitial hollow spaces, and a functional nanotube shell assembled from two-dimensional nanosheets. By adjusting the types of solvents used and reaction time, the morphologies of TiO2/C composites can be tuned to nanoparticles, microrods, rod-in-tube structures, or microtubes. Among these materials, rod-in-tube TiO2 with a uniform carbon coating shows the highest electronic conductivity, specific surface area (336.4 m2 g-1), and porosity, and these factors lead to the best sodium storage capability. Benefiting from the unique structural features and improved electronic/ionic conductivity, the as-obtained rod-in-tube TiO2/C in coin cell tests exhibits a high discharge capacity of 277.5 and 153.9 mAh g-1 at 50 and 5000 mA g-1, respectively, and almost 100% capacity retention over 14,000 cycles at 5000 mA g-1. In operando high-energy X-ray diffraction further confirms the stable crystal structure of the rod-in-tube TiO2/C during Na+ insertion/extraction. Finally, this work highlights that nanostructure design is an effective strategy to achieve advanced energy storage materials.},
doi = {10.1016/j.nanoen.2017.11.077},
journal = {Nano Energy},
number = C,
volume = 44,
place = {United States},
year = {Wed Dec 06 00:00:00 EST 2017},
month = {Wed Dec 06 00:00:00 EST 2017}
}
Web of Science
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