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Title: Nanoindentation study of bulk zirconium hydrides at elevated temperatures

Here, the mechanical properties of zirconium hydrides was studied using nano-indentation technique at a temperature range of 25 – 400 °C. Temperature dependency of reduced elastic modulus and hardness of δ- and ε-zirconium hydrides were obtained by conducting nanoindentation experiments on the bulk hydride samples with independently heating capability of indenter and heating stage. The reduced elastic modulus of δ-zirconium hydride (H/Zr ratio =1.61) decreased from ~113 GPa to ~109 GPa while temperature increased from room temperature to 400°C. For ε-zirconium hydrides (H/Zr ratio=1.79), the reduced elastic modulus decreased from 61 GPa to 54 GPa as temperature increased from room temperature to 300 °C. Whereas, hardness of δ-zirconium hydride significantly decreased from 4.1 GPa to 2.41 GPa when temperature increased from room temperature to 400 °C. Similarly, hardness of ε-zirconium hydride decreased from 3.06 GPa to 2.19 GPa with temperature increase from room temperature to 300°C.
Authors:
ORCiD logo [1] ;  [2] ; ORCiD logo [1] ;  [3] ; ORCiD logo [1]
  1. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
  2. Univ. of California, Berkeley, CA (United States)
  3. Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States); Michigan State Univ., East Lansing, MI (United States)
Publication Date:
Grant/Contract Number:
AC05-00OR22725
Type:
Accepted Manuscript
Journal Name:
Journal of Alloys and Compounds
Additional Journal Information:
Journal Volume: 726; Journal Issue: C; Journal ID: ISSN 0925-8388
Publisher:
Elsevier
Research Org:
Oak Ridge National Lab. (ORNL), Oak Ridge, TN (United States)
Sponsoring Org:
USDOE Office of Nuclear Energy (NE)
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; Zirconium hydrides; Bulk hydride; Nanoindentation; Temperature dependent elastic modulus; δ hydrides; Reduced elastic modulus
OSTI Identifier:
1400216

Cinbiz, Mahmut Nedim, Balooch, Mehdi, Hu, Xunxiang, Amroussia, Aida, and Terrani, Kurt A. Nanoindentation study of bulk zirconium hydrides at elevated temperatures. United States: N. p., Web. doi:10.1016/j.jallcom.2017.07.319.
Cinbiz, Mahmut Nedim, Balooch, Mehdi, Hu, Xunxiang, Amroussia, Aida, & Terrani, Kurt A. Nanoindentation study of bulk zirconium hydrides at elevated temperatures. United States. doi:10.1016/j.jallcom.2017.07.319.
Cinbiz, Mahmut Nedim, Balooch, Mehdi, Hu, Xunxiang, Amroussia, Aida, and Terrani, Kurt A. 2017. "Nanoindentation study of bulk zirconium hydrides at elevated temperatures". United States. doi:10.1016/j.jallcom.2017.07.319. https://www.osti.gov/servlets/purl/1400216.
@article{osti_1400216,
title = {Nanoindentation study of bulk zirconium hydrides at elevated temperatures},
author = {Cinbiz, Mahmut Nedim and Balooch, Mehdi and Hu, Xunxiang and Amroussia, Aida and Terrani, Kurt A.},
abstractNote = {Here, the mechanical properties of zirconium hydrides was studied using nano-indentation technique at a temperature range of 25 – 400 °C. Temperature dependency of reduced elastic modulus and hardness of δ- and ε-zirconium hydrides were obtained by conducting nanoindentation experiments on the bulk hydride samples with independently heating capability of indenter and heating stage. The reduced elastic modulus of δ-zirconium hydride (H/Zr ratio =1.61) decreased from ~113 GPa to ~109 GPa while temperature increased from room temperature to 400°C. For ε-zirconium hydrides (H/Zr ratio=1.79), the reduced elastic modulus decreased from 61 GPa to 54 GPa as temperature increased from room temperature to 300 °C. Whereas, hardness of δ-zirconium hydride significantly decreased from 4.1 GPa to 2.41 GPa when temperature increased from room temperature to 400 °C. Similarly, hardness of ε-zirconium hydride decreased from 3.06 GPa to 2.19 GPa with temperature increase from room temperature to 300°C.},
doi = {10.1016/j.jallcom.2017.07.319},
journal = {Journal of Alloys and Compounds},
number = C,
volume = 726,
place = {United States},
year = {2017},
month = {8}
}