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Title: Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples

Abstract

A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.

Inventors:
; ; ; ; ;
Issue Date:
Research Org.:
Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1257229
Patent Number(s):
9366736
Application Number:
14/106,441
Assignee:
BATTELLE MEMORIAL INSTITUTE (Richland, WA)
Patent Classifications (CPCs):
G - PHYSICS G01 - MEASURING G01N - INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
DOE Contract Number:  
AC05-76RL01830
Resource Type:
Patent
Resource Relation:
Patent File Date: 2013 Dec 13
Country of Publication:
United States
Language:
English
Subject:
36 MATERIALS SCIENCE; 47 OTHER INSTRUMENTATION

Citation Formats

Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States: N. p., 2016. Web.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., & Ewing, James R. Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples. United States.
Cho, Herman M., Washton, Nancy M., Mueller, Karl T., Sears, Jr., Jesse A., Townsend, Mark R., and Ewing, James R. Tue . "Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples". United States. https://www.osti.gov/servlets/purl/1257229.
@article{osti_1257229,
title = {Sealed magic angle spinning nuclear magnetic resonance probe and process for spectroscopy of hazardous samples},
author = {Cho, Herman M. and Washton, Nancy M. and Mueller, Karl T. and Sears, Jr., Jesse A. and Townsend, Mark R. and Ewing, James R.},
abstractNote = {A magic-angle-spinning (MAS) nuclear magnetic resonance (NMR) probe is described that includes double containment enclosures configured to seal and contain hazardous samples for analysis. The probe is of a modular design that ensures containment of hazardous samples during sample analysis while preserving spin speeds for superior NMR performance and convenience of operation.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue Jun 14 00:00:00 EDT 2016},
month = {Tue Jun 14 00:00:00 EDT 2016}
}

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