Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Walter, Eric D.; Sears, Jesse A.; Mehta, Hardeep S.; Hoyt, David W.

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Title: Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Abstract

Snap-in bushings are disclosed that enable sealing of sample chambers in MAS-NMR rotors for high pressure and/or high temperature operation that enhance pressure limits up to about 400 bar and temperature limits up to at least about 250° C.

Inventors:: Walter, Eric D.; Sears, Jr., Jesse A.; Mehta, Hardeep S.; Hoyt, David W.

Issue Date:: Tue Feb 04 00:00:00 EST 2020

Research Org.:: Pacific Northwest National Laboratory (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1632518

Patent Number(s):: 10550889

Application Number:: 15/225,688

Assignee:: Battelle Memorial Institute (Richland, WA)

Patent Classifications (CPCs):: F - MECHANICAL ENGINEERING F16 - ENGINEERING ELEMENTS AND UNITS F16C - SHAFTS

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES

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F - MECHANICAL ENGINEERING F16 - ENGINEERING ELEMENTS AND UNITS F16C - SHAFTS
F16C33/74 - of sliding-contact bearings
F16C35/02 - in the case of sliding-contact bearings

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/30 - Sample handling arrangements, e.g. sample cells, spinning mechanisms
G01R33/305 - {specially adapted for high-pressure applications}
G01R33/307 - {specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer}

Show less

DOE Contract Number:: AC05-76RL01830

Resource Type:: Patent

Resource Relation:: Patent File Date: 08/01/2016

Country of Publication:: United States

Language:: English

Subject:: 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats


                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., and Hoyt, David W. Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy.  United States: N. p., 2020. 
        Web.

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                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., & Hoyt, David W. Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy.  United States.

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                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., and Hoyt, David W. Tue .  
        "Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy".  United States.  https://www.osti.gov/servlets/purl/1632518.

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@article{osti_1632518,

  title        = {Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy},

  author       = {Walter, Eric D. and Sears, Jr., Jesse A. and Mehta, Hardeep S. and Hoyt, David W.},

  abstractNote = {Snap-in bushings are disclosed that enable sealing of sample chambers in MAS-NMR rotors for high pressure and/or high temperature operation that enhance pressure limits up to about 400 bar and temperature limits up to at least about 250° C.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {Tue Feb 04 00:00:00 EST 2020},

  month        = {Tue Feb 04 00:00:00 EST 2020}

}

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Works referenced in this record:

High-Pressure, High Temperature Magic Angle Spinning Nuclear Magnetic Resonance Devices and Processes for Making and Using Same
patent-application, February 2014

Hu, JIan Zhi; Hu, Mary Y.; Townsend, Mark R.
US Patent Application 13/961,012; 2014/0044598 Al
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140044598

Devices and Process for High-Pressure Magic Angle Spinning Nuclear Magnetic Resonance
patent-application, June 2012

Hoyt, David W.; Sears, Jr., Jesse A.; Turcu, Romulus V. F.
US Patent Application 13/193172; 20120146636
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20120146636

Rack Bush and Rack Pinion Type Steering Apparatus Having Rack Bush for Vehicle
patent-application, October 2010

Kim, Heung-Ju; Heo, Sung-Moo; Choi, Byung-Yun
US Patent Application 12/753338; 20100251839
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100251839

Sample Holder and Method
patent-application, February 2016

Turcu, Romulus Valeriu Flaviu; Simon, Simion
US Patent Application 14/457919; 20160047867
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20160047867

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
patent, April 2014

Hoyt, David W.; Sears, Jr., Jesse A.; Turcu, Romulus V. F.
US Patent Document 8,692,548
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/8692548

Endoscopic Overtube
patent-application, May 2010

Rosemurgy, Alexander S.; Ross, Sharona B.
US Patent Application 12/695655; 20100130821
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20100130821

NMR MAS sealing sample cells and methods
patent, April 2000

Doty, F. David
US Patent Document 6,054,857
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6054857

Tilting o-ring check valve
patent, June 1998

Gregoire, Roger J.
US Patent Document 5,762,103
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/5762103

Processes for Delivery of Viscous Drug Therapies
patent-application, October 2014

Scribben, Eric C.; Risser, Steven M.; Heintz, Amy M.
US Patent Application 14/356859; 20140324022
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/20140324022

Two-way check valve
patent, October 2001

LeVey, Kenneth; Nowak, David R.
US Patent Document 6,298,873
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6298873

The use of supercritical fluids as solvents for NMR spectroscopy
journal, October 2005

Yonker, Clement R.; Linehan, John C.
Progress in Nuclear Magnetic Resonance Spectroscopy, Vol. 47, Issue 1-2, p. 95-109
https://doi.org/10.1016/j.pnmrs.2005.08.002

Split tube flexure
patent, July 2003

Goldfarb, Michael; Speich, John E.
US Patent Document 6,585,445
URL: https://image-ppubs.uspto.gov/dirsearch-public/print/downloadPdf/6585445

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Similar Records

Title: Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Abstract

Citation Formats

High-Pressure, High Temperature Magic Angle Spinning Nuclear Magnetic Resonance Devices and Processes for Making and Using Same patent-application, February 2014

Devices and Process for High-Pressure Magic Angle Spinning Nuclear Magnetic Resonance patent-application, June 2012

Rack Bush and Rack Pinion Type Steering Apparatus Having Rack Bush for Vehicle patent-application, October 2010

Sample Holder and Method patent-application, February 2016

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance patent, April 2014

Endoscopic Overtube patent-application, May 2010

NMR MAS sealing sample cells and methods patent, April 2000

Tilting o-ring check valve patent, June 1998

Processes for Delivery of Viscous Drug Therapies patent-application, October 2014

Two-way check valve patent, October 2001

The use of supercritical fluids as solvents for NMR spectroscopy journal, October 2005

Split tube flexure patent, July 2003

High-Pressure, High Temperature Magic Angle Spinning Nuclear Magnetic Resonance Devices and Processes for Making and Using Same
patent-application, February 2014

Devices and Process for High-Pressure Magic Angle Spinning Nuclear Magnetic Resonance
patent-application, June 2012

Rack Bush and Rack Pinion Type Steering Apparatus Having Rack Bush for Vehicle
patent-application, October 2010

Sample Holder and Method
patent-application, February 2016

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
patent, April 2014

Endoscopic Overtube
patent-application, May 2010

NMR MAS sealing sample cells and methods
patent, April 2000

Tilting o-ring check valve
patent, June 1998

Processes for Delivery of Viscous Drug Therapies
patent-application, October 2014

Two-way check valve
patent, October 2001

The use of supercritical fluids as solvents for NMR spectroscopy
journal, October 2005

Split tube flexure
patent, July 2003