Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Walter, Eric D.; Sears, Jesse A.; Mehta, Hardeep S.; Hoyt, David W.

Title: Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Abstract

Snap-in bushings are disclosed that enable sealing of sample chambers in MAS-NMR rotors for high pressure and/or high temperature operation that enhance pressure limits up to about 400 bar and temperature limits up to at least about 250° C.

Inventors:: Walter, Eric D.; Sears, Jr., Jesse A.; Mehta, Hardeep S.; Hoyt, David W.

Issue Date:: 2020-02-04

Research Org.:: Pacific Northwest National Lab. (PNNL), Richland, WA (United States)

Sponsoring Org.:: USDOE

OSTI Identifier:: 1632518

Patent Number(s):: 10550889

Application Number:: 15/225,688

Assignee:: Battelle Memorial Institute (Richland, WA)

Patent Classifications (CPCs):: F - MECHANICAL ENGINEERING F16 - ENGINEERING ELEMENTS AND UNITS F16C - SHAFTS

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES

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F - MECHANICAL ENGINEERING F16 - ENGINEERING ELEMENTS AND UNITS F16C - SHAFTS
F16C33/74 - of sliding-contact bearings

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/305 - {specially adapted for high-pressure applications}
G01R33/307 - {specially adapted for moving the sample relative to the MR system, e.g. spinning mechanisms, flow cells or means for positioning the sample inside a spectrometer}

F - MECHANICAL ENGINEERING F16 - ENGINEERING ELEMENTS AND UNITS F16C - SHAFTS
F16C35/02 - in the case of sliding-contact bearings

G - PHYSICS G01 - MEASURING G01R - MEASURING ELECTRIC VARIABLES
G01R33/30 - Sample handling arrangements, e.g. sample cells, spinning mechanisms

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DOE Contract Number:: AC05-76RL01830

Resource Type:: Patent

Resource Relation:: Patent File Date: 08/01/2016

Country of Publication:: United States

Language:: English

Subject:: 46 INSTRUMENTATION RELATED TO NUCLEAR SCIENCE AND TECHNOLOGY

Citation Formats


                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., and Hoyt, David W. Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy.  United States: N. p., 2020. 
        Web.

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                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., & Hoyt, David W. Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy.  United States.

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                    Walter, Eric D., Sears, Jr., Jesse A., Mehta, Hardeep S., and Hoyt, David W. Tue .  
        "Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy".  United States.  https://www.osti.gov/servlets/purl/1632518.

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@article{osti_1632518,

  title        = {Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy},

  author       = {Walter, Eric D. and Sears, Jr., Jesse A. and Mehta, Hardeep S. and Hoyt, David W.},

  abstractNote = {Snap-in bushings are disclosed that enable sealing of sample chambers in MAS-NMR rotors for high pressure and/or high temperature operation that enhance pressure limits up to about 400 bar and temperature limits up to at least about 250° C.},

  doi          = {},

  journal      = {},
number       = ,

  volume       = ,

  place        = {United States},

  year         = {2020},

  month        = {2}

}

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Works referenced in this record:

NMR MAS sealing sample cells and methods
patent, April 2000

Doty, F. David
US Patent Document 6,054,857
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=6054857

Tilting o-ring check valve
patent, June 1998

Gregoire, Roger J.
US Patent Document 5,762,103
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=5762103

Two-way check valve
patent, October 2001

Levey, Kenneth R.; Nowak, David R.
US Patent Document 6,298,873
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=6298873

Split tube flexure
patent, July 2003

Goldfarb, Michael; Speich, John E.
US Patent Document 6,585,445
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=6585445

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
patent, April 2014

Hoyt, David W.; Sears, Jr., Jesse A.; Turcu, Romulus V. F.
US Patent Document 8,692,548
URL: http://patft.uspto.gov/netacgi/nph-Parser?patentnumber=8692548

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Title: Snap-in bushings and process for high-pressure and/or high temperature magic angle spinning nuclear magnetic resonance spectroscopy

Abstract

Citation Formats

NMR MAS sealing sample cells and methods patent, April 2000

Tilting o-ring check valve patent, June 1998

Two-way check valve patent, October 2001

Split tube flexure patent, July 2003

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance patent, April 2014

NMR MAS sealing sample cells and methods
patent, April 2000

Tilting o-ring check valve
patent, June 1998

Two-way check valve
patent, October 2001

Split tube flexure
patent, July 2003

Devices and process for high-pressure magic angle spinning nuclear magnetic resonance
patent, April 2014