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Title: Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides

Abstract

Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.

Inventors:
Issue Date:
Research Org.:
Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
Sponsoring Org.:
USDOE
OSTI Identifier:
1455058
Patent Number(s):
9981893
Application Number:
15/010,899
Assignee:
National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)
Patent Classifications (CPCs):
C - CHEMISTRY C07 - ORGANIC CHEMISTRY C07C - ACYCLIC OR CARBOCYCLIC COMPOUNDS
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
DOE Contract Number:  
AC04-94AL85000
Resource Type:
Patent
Resource Relation:
Patent File Date: 2016 Jan 29
Country of Publication:
United States
Language:
English
Subject:
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY

Citation Formats

Boyle, Timothy J. Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides. United States: N. p., 2018. Web.
Boyle, Timothy J. Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides. United States.
Boyle, Timothy J. Tue . "Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides". United States. https://www.osti.gov/servlets/purl/1455058.
@article{osti_1455058,
title = {Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides},
author = {Boyle, Timothy J.},
abstractNote = {Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {2018},
month = {5}
}

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Works referenced in this record:

Synthesizing Biofunctionalized Nanoparticles to Image Cell Signaling Pathways
journal, December 2006


Advances in Structurally Characterized Lanthanide Alkoxide, Aryloxide, and Silyloxide Compounds
journal, June 2008


Nonstoichiometric fluorides—Solid electrolytes for electrochemical devices: A review
journal, September 2007


Fluoride electrode with LaF3-membrane and simple disjoining solid-state internal contact
journal, September 2001