Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides
Abstract
Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.
- Inventors:
- Issue Date:
- Research Org.:
- Sandia National Laboratories (SNL), Albuquerque, NM, and Livermore, CA (United States)
- Sponsoring Org.:
- USDOE
- OSTI Identifier:
- 1455058
- Patent Number(s):
- 9981893
- Application Number:
- 15/010,899
- Assignee:
- National Technology & Engineering Solutions of Sandia, LLC (Albuquerque, NM)
- Patent Classifications (CPCs):
-
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01F - COMPOUNDS OF THE METALS BERYLLIUM, MAGNESIUM, ALUMINIUM, CALCIUM, STRONTIUM, BARIUM, RADIUM, THORIUM, OR OF THE RARE-EARTH METALS
C - CHEMISTRY C01 - INORGANIC CHEMISTRY C01P - INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- DOE Contract Number:
- AC04-94AL85000
- Resource Type:
- Patent
- Resource Relation:
- Patent File Date: 2016 Jan 29
- Country of Publication:
- United States
- Language:
- English
- Subject:
- 37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
Citation Formats
Boyle, Timothy J. Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides. United States: N. p., 2018.
Web.
Boyle, Timothy J. Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides. United States.
Boyle, Timothy J. Tue .
"Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides". United States. https://www.osti.gov/servlets/purl/1455058.
@article{osti_1455058,
title = {Method to synthesize lanthanide fluoride materials from lanthanide fluorinated alkoxides},
author = {Boyle, Timothy J.},
abstractNote = {Lanthanide fluorinated alkoxide derivatives can be synthesized from the alcoholysis reaction of the lanthanide bis-trimethylsilyl amide and an excess amount of hexafluoro iso-propanol. Nanoparticles can be formed from the lanthanide fluorinated alkoxide derivatives by a solvothermal or solution precipitation process.},
doi = {},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Tue May 29 00:00:00 EDT 2018},
month = {Tue May 29 00:00:00 EDT 2018}
}
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