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Title: WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Sediment FTICR-MS, Dissolved Organic Carbon, Aerobic Respiration, Elemental Composition, Grain Size, Total Nitrogen and Organic Carbon Content, Bacterial Abundance, and Stable Isotopes (v9)

Abstract

The WHONDRS Summer 2019 Sampling (S19S) Campaign collected samples in 97 globally distributed river corridor systems between July and September 2019. Surficial streambed sediments were collected at three locations within each site (upstream, midstream, and downstream). Surface water was collected at the downstream site. This dataset includes a portion of the data types produced from the sediment samples and does not include any results from the surface water. Surface water data can be found at https://data.ess-dive.lbl.gov/view/doi:10.15485/1603775. The S19S campaign was designed with the science community to ask questions associated with links among core/transient metabolomes, microbial metabolism, biogeochemical function, and physical properties of watershed and river corridor systems. This data package was originally published in December 2020. It was updated in April 2021 (v2; modified files), May 2022 (v3; new and modified files), November 2022 (v4; new and modified files), January 2023 (v5 and v6; new and modified files), February 2023 (v7; new and modified files), August 2023 (v8; new and modified files), and July 2025 (new and modified files). See the change history section in the readme for details. This dataset contains (1) high resolution characterization of dissolved organic matter from sediment via 12 Tesla Fourier transform ion cyclotron resonancemore » mass spectrometry (FTICR-MS) through the Environmental Molecular Sciences Laboratory (EMSL; https://www.pnnl.gov/environmental-molecular-sciences-laboratory); (2) dissolved organic carbon (DOC, measured as non-purgeable organic carbon, NPOC); (3) respiration rates and normalized respiration rates calculated from laboratory sediment incubations; (4) X-ray fluorescence (XRF) elemental composition; (5) grain size distribution from the < 2 millimeter fraction of sediment; (6) total organic carbon and total nitrogen content; (7) bacterial abundance flow cytometry data; (8) sediment stable isotopes (C and N); (9) site photos; (10) field and laboratory methods metadata, including international generic sample number (IGSN) mapping file; (11) file-level metadata (flmd); (12) data dictionary (dd); and (13) water and sediment mass and volume used in incubations. The FTICR-MS files are .xml, and the data package includes instructions for using Formularity (https://omics.pnl.gov/software/formularity) and an R script to process the data based on the user’s specific needs. The XRF data includes .msa, .txt, and .spx files. All other data files are .csv, .pdf, .txt, .jpg, or .jpeg. CORRECTION: Carbon and nitrogen content are reported as percentages. The current column headers "01395_C_percent_per_mg" and "01397_N_percent_per_mg" are incorrect. These should read "01395_C_percent" and "01397_N_percent" and will be corrected in the next version of this data package.« less

Authors:
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  1. Pacific Northwest National Laboratory
  2. Ben Gurion University of the Negev
  3. Colorado State University
  4. University of Arizona/Pacific Northwest National Laboratory
  5. Oregon State University
Publication Date:
DOE Contract Number:  
AC02-05CH11231
Research Org.:
River Corridor and Watershed Biogeochemistry SFA
Sponsoring Org.:
ESS-DIVE; U.S. DOE > Office of Science > Biological and Environmental Research (BER)
Subject:
13C; 15N; 54 ENVIRONMENTAL SCIENCES; Aerobic respiration rate; Bacterial abundance; Biogeochemistry; Carbon; Catchment; EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > SURFACE WATER; EARTH SCIENCE > TERRESTRIAL HYDROSPHERE > WATER QUALITY/WATER CHEMISTRY > ISOTOPES > STABLE ISOTOPES; ESS-DIVE CSV File Formatting Guidelines Reporting Format; ESS-DIVE File Level Metadata Reporting Format; ESS-DIVE Sample ID and Metadata Reporting Format; Elemental abundance; FTICR; FTICR-MS; Flow cytometry; Freshwater; Grain size; Hydrologic exchange; Hydrology; Hyporheic zone; Mass spectrometry; Metabolite; Metabolomics; NPOC; Non-purgeable organic carbon; Respiration; River; River corridor; Stream; WHONDRS; Watershed; related identifiers
OSTI Identifier:
1729719
DOI:
https://doi.org/10.15485/1729719

Citation Formats

Goldman, Amy E, Arnon, Shai, Bar-Zeev, Edo, Chu, Rosalie K, Danczak, Robert E, Daly, Rebecca A, Delgado, Dillman, Fansler, Sarah, Forbes, Brieanne, Garayburu-Caruso, Vanessa A, Graham, Emily B, Laan, Maggi, McCall, Marcy L, McKever, Sophia, Patel, Kaizad F, Ren, Huiying, Renteria, Lupita, Resch, Charles T, Rod, Kenton A, Tfaily, Malak, Tolic, Nikola, Torgeson, Joshua M, Toyoda, Jason G, Wells, Jacqueline, Wrighton, Kelly C, Stegen, James C, and WHONDRS Consortium, The. WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Sediment FTICR-MS, Dissolved Organic Carbon, Aerobic Respiration, Elemental Composition, Grain Size, Total Nitrogen and Organic Carbon Content, Bacterial Abundance, and Stable Isotopes (v9). United States: N. p., 2020. Web. doi:10.15485/1729719.
Goldman, Amy E, Arnon, Shai, Bar-Zeev, Edo, Chu, Rosalie K, Danczak, Robert E, Daly, Rebecca A, Delgado, Dillman, Fansler, Sarah, Forbes, Brieanne, Garayburu-Caruso, Vanessa A, Graham, Emily B, Laan, Maggi, McCall, Marcy L, McKever, Sophia, Patel, Kaizad F, Ren, Huiying, Renteria, Lupita, Resch, Charles T, Rod, Kenton A, Tfaily, Malak, Tolic, Nikola, Torgeson, Joshua M, Toyoda, Jason G, Wells, Jacqueline, Wrighton, Kelly C, Stegen, James C, & WHONDRS Consortium, The. WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Sediment FTICR-MS, Dissolved Organic Carbon, Aerobic Respiration, Elemental Composition, Grain Size, Total Nitrogen and Organic Carbon Content, Bacterial Abundance, and Stable Isotopes (v9). United States. doi:https://doi.org/10.15485/1729719
Goldman, Amy E, Arnon, Shai, Bar-Zeev, Edo, Chu, Rosalie K, Danczak, Robert E, Daly, Rebecca A, Delgado, Dillman, Fansler, Sarah, Forbes, Brieanne, Garayburu-Caruso, Vanessa A, Graham, Emily B, Laan, Maggi, McCall, Marcy L, McKever, Sophia, Patel, Kaizad F, Ren, Huiying, Renteria, Lupita, Resch, Charles T, Rod, Kenton A, Tfaily, Malak, Tolic, Nikola, Torgeson, Joshua M, Toyoda, Jason G, Wells, Jacqueline, Wrighton, Kelly C, Stegen, James C, and WHONDRS Consortium, The. 2020. "WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Sediment FTICR-MS, Dissolved Organic Carbon, Aerobic Respiration, Elemental Composition, Grain Size, Total Nitrogen and Organic Carbon Content, Bacterial Abundance, and Stable Isotopes (v9)". United States. doi:https://doi.org/10.15485/1729719. https://www.osti.gov/servlets/purl/1729719. Pub date:Wed Jan 01 00:00:00 UTC 2020
@article{osti_1729719,
title = {WHONDRS Summer 2019 Sampling Campaign: Global River Corridor Sediment FTICR-MS, Dissolved Organic Carbon, Aerobic Respiration, Elemental Composition, Grain Size, Total Nitrogen and Organic Carbon Content, Bacterial Abundance, and Stable Isotopes (v9)},
author = {Goldman, Amy E and Arnon, Shai and Bar-Zeev, Edo and Chu, Rosalie K and Danczak, Robert E and Daly, Rebecca A and Delgado, Dillman and Fansler, Sarah and Forbes, Brieanne and Garayburu-Caruso, Vanessa A and Graham, Emily B and Laan, Maggi and McCall, Marcy L and McKever, Sophia and Patel, Kaizad F and Ren, Huiying and Renteria, Lupita and Resch, Charles T and Rod, Kenton A and Tfaily, Malak and Tolic, Nikola and Torgeson, Joshua M and Toyoda, Jason G and Wells, Jacqueline and Wrighton, Kelly C and Stegen, James C and WHONDRS Consortium, The},
abstractNote = {The WHONDRS Summer 2019 Sampling (S19S) Campaign collected samples in 97 globally distributed river corridor systems between July and September 2019. Surficial streambed sediments were collected at three locations within each site (upstream, midstream, and downstream). Surface water was collected at the downstream site. This dataset includes a portion of the data types produced from the sediment samples and does not include any results from the surface water. Surface water data can be found at https://data.ess-dive.lbl.gov/view/doi:10.15485/1603775. The S19S campaign was designed with the science community to ask questions associated with links among core/transient metabolomes, microbial metabolism, biogeochemical function, and physical properties of watershed and river corridor systems. This data package was originally published in December 2020. It was updated in April 2021 (v2; modified files), May 2022 (v3; new and modified files), November 2022 (v4; new and modified files), January 2023 (v5 and v6; new and modified files), February 2023 (v7; new and modified files), August 2023 (v8; new and modified files), and July 2025 (new and modified files). See the change history section in the readme for details. This dataset contains (1) high resolution characterization of dissolved organic matter from sediment via 12 Tesla Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) through the Environmental Molecular Sciences Laboratory (EMSL; https://www.pnnl.gov/environmental-molecular-sciences-laboratory); (2) dissolved organic carbon (DOC, measured as non-purgeable organic carbon, NPOC); (3) respiration rates and normalized respiration rates calculated from laboratory sediment incubations; (4) X-ray fluorescence (XRF) elemental composition; (5) grain size distribution from the < 2 millimeter fraction of sediment; (6) total organic carbon and total nitrogen content; (7) bacterial abundance flow cytometry data; (8) sediment stable isotopes (C and N); (9) site photos; (10) field and laboratory methods metadata, including international generic sample number (IGSN) mapping file; (11) file-level metadata (flmd); (12) data dictionary (dd); and (13) water and sediment mass and volume used in incubations. The FTICR-MS files are .xml, and the data package includes instructions for using Formularity (https://omics.pnl.gov/software/formularity) and an R script to process the data based on the user’s specific needs. The XRF data includes .msa, .txt, and .spx files. All other data files are .csv, .pdf, .txt, .jpg, or .jpeg. CORRECTION: Carbon and nitrogen content are reported as percentages. The current column headers "01395_C_percent_per_mg" and "01397_N_percent_per_mg" are incorrect. These should read "01395_C_percent" and "01397_N_percent" and will be corrected in the next version of this data package.},
doi = {10.15485/1729719},
journal = {},
number = ,
volume = ,
place = {United States},
year = {Wed Jan 01 00:00:00 UTC 2020},
month = {Wed Jan 01 00:00:00 UTC 2020}
}