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Production Of Fullerenic Soot In Flames

Patent ·
OSTI ID:879589

A method for the production of fullerenic nanostructures is described in which unsaturated hydrocarbon fuel and oxygen are combusted in a burner chamber at a sub-atmospheric pressure, thereby establishing a flame. The condensibles of the flame are collected at a post-flame location. The condensibles contain fullerenic nanostructures, such as single and nested nanotubes, single and nested nanoparticles and giant fullerenes. The method of producing fullerenic soot from flames is also described.

Research Organization:
MASSACHUSETTS INST OF TECH
DOE Contract Number:
FG02-84ER13282
Assignee:
Massachusetts Institute of Technology (Cambridge, MA)
Patent Number(s):
US 6162411
Application Number:
09/292068
OSTI ID:
879589
Country of Publication:
United States
Language:
English

References (49)

Surface Properties of Carbon journal May 1971
Packing of C60 molecules and related fullerenes in crystals: a direct view journal July 1991
Structure and energetics of single and multilayer fullerene cages journal May 1993
Fullerenes C60 and C70 in flames journal July 1991
Structure and reactivity of carbons: From carbon black to carbon composites journal January 1982
Progressive Oxidation of Selected Particles of Carbon Black: Further Evidence for a New Microstructural Model journal March 1966
Formation of carbon nanofibers journal August 1992
Down the straight and narrow journal July 1992
Reactivity of large carbon clusters: spheroidal carbon shells and their possible relevance to the formation and morphology of soot journal February 1986
Micromorphology of carbon black journal January 1992
High-yield synthesis, separation, and mass-spectrometric characterization of fullerenes C60 to C266 journal September 1991
Structure and formation process of carbon blacks formed by decomposing SiC powder using a conically converging shock-wave technique journal January 1989
Large-scale synthesis of carbon nanotubes journal July 1992
Carbon blacks produced in a detonation wave from propylene journal January 1980
Vapor-Condensation Generation and STM Analysis of Fullerene Tubes journal April 1993
Soot formation journal January 1981
Dispersal of carbon blacks to individual crystallites journal May 1967
Microstructure of Carbon Black journal November 1964
Direct observation of the tetrahedral bonding in graphitized carbon black by high resolution electron microscopy journal November 1980
Fullerenes journal October 1991
Microstructure and Morphology of Carbon Blacks book June 1976
Comment on the proposed role of spheroidal carbon clusters in soot formation journal January 1988
Fullerene ions and their relation to PAH and soot in low-pressure hydrocarbon flames journal July 1992
Thinning and opening of carbon nanotubes by oxidation using carbon dioxide journal April 1993
The 60-carbon cluster has been revealed journal June 1987
Extraction and STM Imaging of Spherical Giant Fullerenes journal March 1992
Carbon Black Morphology: I. Particle Microstructure. II. Automated EM Analysis of Aggregate Size and Shape journal September 1969
Buckytubes and Derivatives: Their Growth and Implications for Buckyball Formation journal March 1993
Effect of processing conditions on the morphology and yield of carbon nanotubes journal January 1993
Production of C60 and C70 fullerenes in benzene-oxygen flames journal August 1992
Opening carbon nanotubes with oxygen and implications for filling journal April 1993
Spectroscopic and chemical characterisation of “fullerene black” journal June 1992
Helical microtubules of graphitic carbon journal November 1991
Is Soot Composed Predominantly of Carbon Clusters? journal March 1990
Fullerenes synthesis in combustion journal January 1992
Morphology and yield of carbon clusters in arc-discharge deposits journal January 1993
Fullerene molecular weight distributions in graphite soot extractions measured by laser desorption Fourier transform mass spectrometry journal February 1993
The behavior of polycyclic aromatic hydrocarbons during the early stages of soot formation journal January 1989
Carbon onions introduce new flavour to fullerene studies journal October 1992
The formation of quasi-icosahedral spiral shell carbon particles journal January 1988
Quantitative micrography of carbon black microstructure journal December 1971
Specific Shape Characterization of Carbon Black Primary Units journal March 1973
The interrelationship of C60, soot and combustion journal January 1993
Simulated transmission electron microscope images and characterisation of concentric shell and icospiral graphitic microparticles journal January 1992
Curling and closure of graphitic networks under electron-beam irradiation journal October 1992
Extraction of giant fullerene molecules, and their subsequent solvation in low boiling point solvents journal January 1992
Pentagons, heptagons and negative curvature in graphite microtubule growth journal April 1992
Structure and Properties of Carbon Black - Changes Induced by Heat Treatment journal August 1953
Fullerenes formation in flames journal January 1992

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