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1,2-bis-difluoroamino-4-methylpentane: heats of combustion, formation, and vaporization; vapor pressure; and N--F thermochemical bond energy

Journal Article · · J. Phys. Chem.; (United States)
DOI:https://doi.org/10.1021/j100800a037· OSTI ID:7305430

The heat of combustion of 1,2-bis-difluoroamino-4-methylpentane was measured by rotating-bomb calorimetry, and the vapor pressure was measured between -20 and +20/sup 0/ with an inclined-piston gage. Experimental techniques suitable for studying compounds of this class were developed. The results were used to calculate the following thermochemical data in kcal. mole/sup -1/ at 298.15/sup 0/K: standard heat of formation of the liquid, -60.09; heat of vaporization, 10.51; and standard heat of formation of the gas, -49.58. The N--F thermochemical bond energy in this compound was found to be 67 kcal. mole/sup -1/, about the same as the N--F thermochemical bond energy in NF/sub 3/ and N/sub 2/F/sub 4/ but significantly less than that in perfluoropiperidine.

Research Organization:
Bureau of Mines, Bartlesville, OK
OSTI ID:
7305430
Journal Information:
J. Phys. Chem.; (United States), Journal Name: J. Phys. Chem.; (United States) Vol. 67; ISSN JPCHA
Country of Publication:
United States
Language:
English