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Reactions of adducts of phosphorus pentachloride and oxa-containing nucleophiles with arsenic trifluoride

Journal Article · · J. Gen. Chem. USSR (Engl. Transl.); (United States)
OSTI ID:7005357
; ;

Results are given on the synthesis of phosphonofluoridates by the reactions of arsenic trifluoride with adducts of phosphorus pentachloride with oxa-containing nucleophiles. The nucleophiles used were saturated ethers, dioxolanes, and vinyl ethers. Reaction products were identified by means of NMR spectroscopy using H 1, P 31, and C 13. A full analysis of chemical shift and spin-spin coupling constant behavior as well as the spectral structure is conducted.

Research Organization:
S. M. Kirov Kazan' Institute of Chemical Technology (USSR)
OSTI ID:
7005357
Journal Information:
J. Gen. Chem. USSR (Engl. Transl.); (United States), Journal Name: J. Gen. Chem. USSR (Engl. Transl.); (United States) Vol. 57:7; ISSN JGCHA
Country of Publication:
United States
Language:
English

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Related Subjects

37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400201* -- Chemical & Physicochemical Properties
640302 -- Atomic
Molecular & Chemical Physics-- Atomic & Molecular Properties & Theory
74 ATOMIC AND MOLECULAR PHYSICS
ACTIVATION ENERGY
ADDUCTS
ARSENIC COMPOUNDS
ARSENIC FLUORIDES
CARBON 13
CARBON ISOTOPES
CHEMICAL REACTION KINETICS
CHEMICAL REACTION YIELD
CHEMICAL SHIFT
CHLORIDES
CHLORINE COMPOUNDS
COUPLING
COUPLING CONSTANTS
DIENES
ENERGY
ETHERS
EVEN-ODD NUCLEI
FLUORIDES
FLUORINE COMPOUNDS
HALIDES
HALOGEN COMPOUNDS
HYDROCARBONS
HYDROGEN 1
HYDROGEN ISOTOPES
INTERMEDIATE COUPLING
ISOTOPES
J-J COUPLING
KINETICS
LIGHT NUCLEI
NMR SPECTRA
NUCLEI
ODD-EVEN NUCLEI
ORGANIC COMPOUNDS
ORGANIC FLUORINE COMPOUNDS
ORGANIC HALOGEN COMPOUNDS
ORGANIC OXYGEN COMPOUNDS
ORGANIC PHOSPHORUS COMPOUNDS
PHOSPHORUS 31
PHOSPHORUS CHLORIDES
PHOSPHORUS COMPOUNDS
PHOSPHORUS ISOTOPES
POLYENES
REACTION KINETICS
SPECTRA
STABLE ISOTOPES
STRUCTURAL CHEMICAL ANALYSIS
SYNTHESIS
YIELDS