Skip to main content
U.S. Department of Energy
Office of Scientific and Technical Information

Organometallic chemistry on a metallathiaborane cluster: Reactions of [8,8-(PPh{sub 3}){sub 2}-nido-8,7-RhSB{sub 9}H{sub 10}] with bidentate phosphine ligands

Journal Article · · Organometallics
DOI:https://doi.org/10.1021/om9901168· OSTI ID:696627
; ;  [1]
  1. Univ. of Missouri, St. Louis, MO (United States). Dept. of Chemistry

Reactions of the unsaturated cluster [8,8-(PPh{sub 3}){sub 2}-nido-8,7-RhSB{sub 9}H{sub 10}] (1) with the bidentate 1,n-bis(diphenylphosphino)alkanes (CH{sub 2}){sub n}(PPh{sub 2}){sub 2}, where n = 1--3 (abbreviated as dppm, dppe, and dppp, respectively), have been studied. The species have been characterized by NMR and mass spectrometry, and crystal structure determinations are described.

Sponsoring Organization:
National Science Foundation, Washington, DC (United States); USDOE, Washington, DC (United States); National Insts. of Health, Bethesda, MD (United States)
DOE Contract Number:
FG02-92CH10499
OSTI ID:
696627
Journal Information:
Organometallics, Journal Name: Organometallics Journal Issue: 18 Vol. 18; ISSN ORGND7; ISSN 0276-7333
Country of Publication:
United States
Language:
English

Similar Records

Organometallic chemistry on a metallathiaborane cluster: Reactions of [8,8-(PPh[sub 3])[sub 2]-nido-8,7-RhSB[sub 9]H[sub 10]] with bidentate phosphine ligands
Journal Article · Mon Aug 30 00:00:00 EDT 1999 · Organometallics · OSTI ID:5937113

Phosphine-based platinum(II) hydroxo and oxo complexes
Journal Article · Tue Jan 30 23:00:00 EST 1996 · Inorganic Chemistry · OSTI ID:255638

Calorimetric studies of the heats of protonation of the metal in cis-M(CO)[sub 2](bidentate phosphine)[sub 2] complexes of chromium, molybdenum, and tungsten
Journal Article · Wed Apr 15 00:00:00 EDT 1992 · Inorganic Chemistry; (United States) · OSTI ID:7016995