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Isotope effects in proton-transfer reactions. An ion cyclotron resonance determination of the equilibrium deuterium isotope effect in the bichloride ion

Journal Article · · J. Phys. Chem.; (United States)
DOI:https://doi.org/10.1021/j100287a013· OSTI ID:6949221

The equilibrium constant for the gas-phase chloride exchange reaction ClHCl/sup -/ + DCl in equilibrium ClDCl/sup -/ + HCl has been measured by using ion cyclotron resonance spectroscopic trapped-ion techniques. The value obtained of 0.60 can be shown by statistical thermodynamic calculations to be principally due to rotational partition function ratios rather than due to differences in zero-point energies. The equilibrium data have been used to calculate a gas-phase deuterium fractionation factor of 0.28, inferring that the bichloride ion should have a double-minimum potential energy well with the lowest allowed energy level at or near the height of the central barrier. Implications for kinetic isotope effects are also discussed.

Research Organization:
Univ. of Waterloo, Ontario
OSTI ID:
6949221
Journal Information:
J. Phys. Chem.; (United States), Journal Name: J. Phys. Chem.; (United States) Vol. 91:3; ISSN JPCHA
Country of Publication:
United States
Language:
English