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U.S. Department of Energy
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Mechanical properties of silicon nitride-silicon nitride joints. [Glass-filled, sintered silicon nitride joints]

Conference ·
OSTI ID:6910914
Oxynitride glasses in the Y--Si--Al--O--N system were used to join sintered and hot pressed silicon nitrides. Joint flexural strengths were dependent upon the joining temperature, joining glass composition, silicon nitride type, and joint morphology. Joint flexural strengths comparable to that of as-received silicon nitride were observed to test temperatures as high as 1100/degree/C, and were dependent upon joint morphology. Non-brittle behavior was observed in /open quotes/fast fracture/close quotes/ of glass-filled joints at temperatures of 1025/degree/C. However, slow crack growth was observed in the temperature range of 900 to 1025/degrees/C. Slow crack growth was found to be strongly temperature dependent /endash/ long joint lifetimes occur below 900/degree/C. Initial experiments indicated that thermal cycling did not degrade the flexural strength of glass-filled joints. 10 refs., 6 figs.
Research Organization:
EG and G Idaho, Inc., Idaho Falls (USA)
DOE Contract Number:
AC07-76ID01570
OSTI ID:
6910914
Report Number(s):
EGG-M-31987; CONF-880504-7; ON: DE88015095
Country of Publication:
United States
Language:
English