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Plasma oxidation of CF/sub 4/ in a tubular-alumina fast-flow reactor

Journal Article · · J. Appl. Phys.; (United States)
DOI:https://doi.org/10.1063/1.325576· OSTI ID:6145538

Mass-spectrometric analyses were made of the plasma reactions of 50-W CF/sub 4/ and CF/sub 4/-O/sub 2/ discharges as functions of pressure (0.15--0.6 Torr), flow rate (2--80 cm/sup 3//min) or the O/sub 2/ level in the feed. Discharges were investigated both in the presence and absence of single-crystal Si. The products from CF/sub 4/ alone were F, F/sub 2/, and C/sub 2/F/sub 6/; in the presence of Si the products were SiF/sub 4/, C/sub 2/F/sub 6/, and small amounts of F. The products from CF/sub 4/-O/sub 2/ were F, F/sub 2/, COF/sub 2/, CO/sub 2/, and CO; in the presence of Si the products were SiF/sub 4/, F, F/sub 2/, COF/sub 2/, CO/sub 2/, and CO. The conversion of CF/sub 4/ to products increased monotonically with residence time in the discharge and the O/sub 2/ concentration in the feed. It appears that F/sub 2/ was produced in the plasma zone and that the SiF/sub x/ (x<4) species reacted with F/sub 2/ to give SiF/sub 4/.

Research Organization:
Bell Laboratories, Murray Hill, New Jersey 07974
OSTI ID:
6145538
Journal Information:
J. Appl. Phys.; (United States), Journal Name: J. Appl. Phys.; (United States) Vol. 50:7; ISSN JAPIA
Country of Publication:
United States
Language:
English