Influence of specimen thickness in quantitative electron-energy-loss spectroscopy: II
Conference
·
OSTI ID:6094785
Homogenous specimens of boron nitride (BN), nickel oxide (NiO), and aluminium oxide (Al/sub 2/O/sub 3/) were analyzed as a function of thickness (0.25 < t/lambda < 2.5) for scattering angles of 2.6, 5.7, and 14.7 mr at an incident beam energy of 100 keV using a Philips EM400 TEM. EELS measurements were made with both a Gatan 607 EELS and a ..pi../2 magnetic sector analyzer designed by the author. EELS spectra were recorded at energy resolutions approx. 3 eV over the range 0 to 3 keV, on a EDAX PV9100 MCA. Deconvolution of multiple scattering was accomplished using the method described by Leapman and Swyt.
- Research Organization:
- Argonne National Lab., IL (USA)
- DOE Contract Number:
- W-31109-ENG-38
- OSTI ID:
- 6094785
- Report Number(s):
- CONF-830815-6; ON: DE83010739
- Country of Publication:
- United States
- Language:
- English
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Related Subjects
37 INORGANIC, ORGANIC, PHYSICAL, AND ANALYTICAL CHEMISTRY
400103* -- Radiometric & Radiochemical Procedures-- (-1987)
ALUMINIUM COMPOUNDS
ALUMINIUM OXIDES
BORON COMPOUNDS
BORON NITRIDES
CHALCOGENIDES
DIMENSIONS
ELECTRON SPECTROSCOPY
ENERGY-LOSS SPECTROSCOPY
MULTIPLE SCATTERING
NICKEL COMPOUNDS
NICKEL OXIDES
NITRIDES
NITROGEN COMPOUNDS
OXIDES
OXYGEN COMPOUNDS
PNICTIDES
SCATTERING
SPECTROSCOPY
THICKNESS
TRANSITION ELEMENT COMPOUNDS
400103* -- Radiometric & Radiochemical Procedures-- (-1987)
ALUMINIUM COMPOUNDS
ALUMINIUM OXIDES
BORON COMPOUNDS
BORON NITRIDES
CHALCOGENIDES
DIMENSIONS
ELECTRON SPECTROSCOPY
ENERGY-LOSS SPECTROSCOPY
MULTIPLE SCATTERING
NICKEL COMPOUNDS
NICKEL OXIDES
NITRIDES
NITROGEN COMPOUNDS
OXIDES
OXYGEN COMPOUNDS
PNICTIDES
SCATTERING
SPECTROSCOPY
THICKNESS
TRANSITION ELEMENT COMPOUNDS