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U.S. Department of Energy
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Amino acid analysis by gas chromatography

Book ·
OSTI ID:5941690

The partial content of this set of 3 volumes include the following: sample preparation and protein hydrolysis; comparison of short-time, high-temperature hydrolysis with conventional 6 N HCl hydrolysis; development of the N-TFA n-butyl ester method; derivatization, separation and applications of the N-heptafluorobutyryl isobutyl derivatives; measurement of amino acids in fishery products; gas chromatography of the N-TFA amyl and methyl esters; electron capture, alkali flame, and flame ionization detection of the N-HFB isobutyl derivatives in blood plasma and other biological samples; screening for potential inborn errors of metabolism using the N-TFA n-propyl derivatives; the role of gas chromatography in the study of cosmochemistry; the chiral diamide phases for resolution of amino acid enantiomers, the influence of structural features of the diamides, mechanism of resolution of enantiomers, and enantiomeric analyses; analysis of amino acid racemization, the separation of amino acid enantiomers; the comparison of the resolution of various D,L-amino acid derivatives on optically active columns and age dating of sediments by determination of the extent of racemization of amino acids in fossil shells.

OSTI ID:
5941690
Country of Publication:
United States
Language:
English