Synthesis of picryl chloride
A total of six pilot-scale batches of picryl chloride were made. These included three 5-kg batches and three 10-kg batches. The three 5-kg batches were made to investigate the problems encountered with actual production and materials handling. The three 10-kg batches were made to study the process parameters and the yield problems originally encountered with the 5-kg batches. The yields on the 5-kg batches ranged from 40 to 60% of approximately 50% purity. The yields on the 10-kg batches were 80, 86 and 91% in chronological order. The purities were 95, 99+ and 99+% respectively.
- Research Organization:
- Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (United States)
- Sponsoring Organization:
- USDOE, Washington, DC (United States)
- DOE Contract Number:
- AC04-91AL65030
- OSTI ID:
- 532469
- Report Number(s):
- MHSMP--70-16; ON: DE97008918
- Country of Publication:
- United States
- Language:
- English
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