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Synthesis of benzotrifuroxane. Quarterly report, July--September, 1971

Technical Report ·
DOI:https://doi.org/10.2172/532475· OSTI ID:532475
;
This work is to find an improved method for the synthesis of benzotrifuroxane which could be conveniently scaled up. Three batches were made; the first following the LLL procedure, the second with modifications in the initial addition step, and the third with changes in fluid system and handling procedures going from the intermediate to the final product.
Research Organization:
Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (United States)
Sponsoring Organization:
USDOE, Washington, DC (United States)
DOE Contract Number:
AC04-91AL65030
OSTI ID:
532475
Report Number(s):
MHSMP--71-88G; SANL--900-007; ON: DE97009030
Country of Publication:
United States
Language:
English

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Related Subjects

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
CHEMICAL EXPLOSIVES
CHEMICAL PREPARATION
CHEMICAL REACTIONS
POLYCYCLIC NITRO COMPOUNDS
PRECURSOR
XYLENES