He synthesis. Quarterly report, October--December, 1971

Technical Report · Sun Dec 31 04:00:00 EST 1972

DOI:https://doi.org/10.2172/537252· OSTI ID:537252

Hayes, D V; Honea, F I

Existing supplies of bis-trinitroanisole and picryl hydrazine were used to make 2 kg of bis-hexanitrohydrazobenzene. Development of the HNAB recrystallization process was temporarily stopped due to the need to produce a supply of the intermediate products (picryl chloride and HNHB). Purchase orders for DINOL and DNPIA required for synthesis of AFNOL were awarded.

• Research Organization: Mason and Hanger-Silas Mason Co., Inc., Amarillo, TX (United States)
• Sponsoring Organization: USDOE, Washington, DC (United States)
• DOE Contract Number: AC04-91AL65030
• OSTI ID: 537252
• Report Number(s): MHSMP--72-28N; ON: DE97008924
• Country of Publication: United States
• Language: English

Related Subjects

45 MILITARY TECHNOLOGY, WEAPONRY, AND NATIONAL DEFENSE
CHEMICAL EXPLOSIVES
CHEMICAL REACTION YIELD
MOLECULAR STRUCTURE
NITRO COMPOUNDS
RECRYSTALLIZATION
SYNTHESIS