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Electron paramagnetic resonance spectrum of Pr{sup 4+} in BaCeO{sub 3}

Journal Article · · Journal of Solid State Chemistry
 [1];  [2]
  1. Japan Atomic Energy Research Inst., Ibaraki (Japan)
  2. Lawrence Berkeley Lab., CA (United States)

The electron paramagnetic resonance spectrum of a powder of Pr{sup 4+} in BaCeO{sub 3} was measured at 8.5 K. A very large hyperfine interaction with the {sup 141}Pr nucleus was observed. In addition to the allowed hyperfine transitions, forbidden hyperfine interaction with the {sup 141}Pr nucleus was observed. In addition to the allowed hyperfine transitions, forbidden hyperfine transitions were observed. The results were analyzed based on the weak field approximation, i.e., Breit-Rabi formula, and the g value, {vert_bar}g{vert_bar} = 0.745(1) and the hyperfine coupling constant, {vert_bar}A{vert_bar} = 0.0606(2) cm{sup {minus}1}, were obtained. From the measured g value, the {Gamma}{sub 7} {r_arrow} {Gamma}{sub 8} crystal field transition for BaPrO{sub 3} obtained form an earlier inelastic neutron scattering experiment, and setting the spin-orbit coupling constant to its free ion value {zeta} = 865 cm{sup {minus}1}, the energy levels of Pr{sup 4+} in BaCeO{sub 3} were calculated. The measured magnetic susceptibility of BaPrO{sub 3} was compared to the values calculated with the above model.

OSTI ID:
518199
Journal Information:
Journal of Solid State Chemistry, Journal Name: Journal of Solid State Chemistry Journal Issue: 1 Vol. 112; ISSN 0022-4596; ISSN JSSCBI
Country of Publication:
United States
Language:
English

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