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The Synthesis of Biphenyl-3, 3’, 5, 5’-d4 and Biphenyl-d10

Technical Report ·
DOI:https://doi.org/10.2172/4292317· OSTI ID:4292317
 [1]
  1. North American Aviation, Inc., Canoga Park, CA (United States). Atomics International Div.
Biphenyl-3, 3', 5, 5'-d4 has been prepared from aniline hydrobromide by a 4-step synthesis. Biphenyl-d10 has been prepared from benzene by a 3-step synthesis. The two deuterated biphenyls were 98.0 and 95.1 mole percent pure, respectively; the impurities consisted of biphenyls with a lower deuterium content.
Research Organization:
North American Aviation, Inc., Canoga Park, CA (United States). Atomics International Div.
Sponsoring Organization:
US Atomic Energy Commission (AEC)
DOE Contract Number:
AT(11-1)-GEN-8
NSA Number:
NSA-13-002726
OSTI ID:
4292317
Report Number(s):
NAA-SR--3043
Country of Publication:
United States
Language:
English