Tritium-labeled compounds IV. D-glucose-6-t, d-xylose-5-t, and d-mannitol-1-t
Journal Article
·
· Journal of Research of the National Bureau of Standards, Section A: Physics and Chemistry
BS>Methods are presented for the preparation of D-glucose6-t. D-xylose- 5-t. and D-mannitol-1-t by the reduction of suitable compounds with lithium borohydride-t in anhydrous tetrahydrofuran. followed by hydrolysis of the products. The starting materials for the reductions are. respectively, 1,2-O- isopropylidene-D-glucurono-6.3-lactone. 5-aldo1.2-O-isopropylidene-D-xylo- pentofuranose. and 2.3: 5.6di-C-isopropylidene-D-mannofuranose. The apparatus and procedure for carrying out the reductions in a closed systems are described.
- Research Organization:
- Originating Research Org. not identified
- Sponsoring Organization:
- USDOE
- NSA Number:
- NSA-14-021377
- OSTI ID:
- 4179319
- Journal Information:
- Journal of Research of the National Bureau of Standards, Section A: Physics and Chemistry, Journal Name: Journal of Research of the National Bureau of Standards, Section A: Physics and Chemistry Journal Issue: 4 Vol. 64A; ISSN 0022-4332
- Country of Publication:
- Country unknown/Code not available
- Language:
- English
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