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U.S. Department of Energy
Office of Scientific and Technical Information

PROCESS FOR THE SEPARATION OF THORIUM AND URANIUM SALTS

Patent ·
OSTI ID:4131787

A process is proposed for separation of Th from U in organic solutions in which both metals are present as nitrates. To the organic solution is added an aqueous solution of an agent that selectively precipitates the Th as a crystalline compound insoluble in, but transferred to, the aqueous phase. Free oxalic and sulfuric acid solutions are preferred as precipitating agents, but watersoluble salts of the acids may be used. Preferred concentrations of sulfuric acid and water-soluble sulfates are between about 1.5 and 2.5 M. For oxalic acid and water-soluble oxalate solutions, a concentration of between about 0.8 and 1.2 M is preferred. Recovery of Th with cocentraction of less than 1% of U present in the starting solution is possible. The process may be carried out continuously or batch-wise. (A.G.W.)

Research Organization:
Originating Research Org. not identified
NSA Number:
NSA-18-005436
Assignee:
DTIE; NSA-18-005436
Patent Number(s):
US 3104940
OSTI ID:
4131787
Country of Publication:
United States
Language:
English