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Structural, magnetic, and crystalline electric-field effects in single crystals of Y{sub 1{minus}{ital x}}Pr{sub {ital x}}Ba{sub 2}Cu{sub 3}O{sub 7{minus}{delta}}

Journal Article · · Physical Review, B: Condensed Matter
; ; ; ;  [1]; ; ; ;  [2]
  1. Department of Physics, Indian Institute of Technology, Madras 600036 (India)
  2. Department of Physics, University of Oxford, Clarendon Laboratory, Oxford, 0X13PU (England)

We report here structural and directional magnetic susceptibility measurements on single crystals of Y{sub 1{minus}{ital x}}Pr{sub {ital x}}Ba{sub 2}Cu{sub 3}O{sub 7{minus}{delta}} ({ital x}=1.0, {delta}=1, 0.11; {ital x}=0.7, {delta}=0; and {ital x}=0.42, {delta}=0.22). The space group of PrBa{sub 2}Cu{sub 3}O{sub 6} (Pr-O6) and Y{sub 0.58}Pr{sub 0.42}Ba{sub 2}Cu{sub 3}O{sub 6.78} (Pr 0.42-O7) were found to be {ital P}4/{ital mmm} and that of PrBa{sub 2}Cu{sub 3}O{sub 6.89} (Pr-O7) was found to be {ital Pmmm}. Also, Pr-O7 was found to be weakly orthorhombic. Directional, magnetic susceptibility measurements in the temperature range 2{endash}300 K revealed a clear peaking in the paramagnetic anisotropy of Pr-O7 around 17 K, and {chi}{sub {ital c}}{approx_gt}{chi}{sub {ital a},{ital b}} at all temperatures. However for Y{sub 0.3}Pr{sub 0.7}Ba{sub 2}Cu{sub 3}O{sub 7} (Pr0.7-O7) and Pr0.42-O7, {chi}{sub {ital c}}{approx_gt}{chi}{sub {ital a},{ital b}} at room temperature and {chi}{sub {ital c}}{lt}{chi}{sub {ital a},{ital b}} for temperatures below 110 and 60 K, respectively. The magnetic susceptibilities have been analyzed in the light of crystalline electric-field effects considering {ital J} mixing of all the thirteen multiplets. Intermediate coupled wave functions have also been used in the calculations. Crystal-field interaction is found to be stronger in the case of Pr-O7 compared to Pr-O6 which is also evident from a shorter Pr-O bond length in the case of Pr-O7 than in Pr-O6. A best set of eigenvalues and eigenfunctions has been determined and these are discussed and compared with inelastic neutron scattering data. {copyright} {ital 1996 The American Physical Society.}

OSTI ID:
282041
Journal Information:
Physical Review, B: Condensed Matter, Journal Name: Physical Review, B: Condensed Matter Journal Issue: 10 Vol. 53; ISSN 0163-1829; ISSN PRBMDO
Country of Publication:
United States
Language:
English