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Near-field microwave microscopy of high-κ oxides grown on graphene with an organic seeding layer

Journal Article · · Applied Physics Letters
DOI:https://doi.org/10.1063/1.4847675· OSTI ID:22253813
;  [1]; ; ;  [2]; ;  [2]
  1. Oak Ridge National Laboratory, Center for Nanophase Materials Sciences, Oak Ridge, Tennessee 37831 (United States)
  2. Department of Materials Science and Engineering, Northwestern University, Evanston, Illinois 60208 (United States)

Near-field scanning microwave microscopy (SMM) is used for non-destructive nanoscale characterization of Al{sub 2}O{sub 3} and HfO{sub 2} films grown on epitaxial graphene on SiC by atomic layer deposition using a self-assembled perylene-3,4,9,10-tetracarboxylic dianhydride seeding layer. SMM allows imaging of buried inhomogeneities in the dielectric layer with a spatial resolution close to 100 nm. The results indicate that, while topographic features on the substrate surface cannot be eliminated as possible sites of defect nucleation, the use of a vertically heterogeneous Al{sub 2}O{sub 3}/HfO{sub 2} stack suppresses formation of large outgrowth defects in the oxide film, ultimately improving lateral uniformity of the dielectric film.

OSTI ID:
22253813
Journal Information:
Applied Physics Letters, Journal Name: Applied Physics Letters Journal Issue: 24 Vol. 103; ISSN APPLAB; ISSN 0003-6951
Country of Publication:
United States
Language:
English

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