Control of polymer architectures by living ring-opening metathesis copolymerization

Grubbs, Robert H.; Lin, Tzu-Pin; Chang, Alice; Chen, Hsiang-Yun; Bates, Christopher M.

Control of polymer architectures by living ring-opening metathesis copolymerization

Patent · Tue Jul 06 00:00:00 EDT 2021

OSTI ID:1840227

Grubbs, Robert H.; Lin, Tzu-Pin; Chang, Alice; Chen, Hsiang-Yun; Bates, Christopher M.

In an aspect, a method of synthesizing a graft copolymer comprises the steps of: copolymerizing a first macromonomer and a first reactive diluent; wherein said first macromonomer comprises a first backbone precursor directly or indirectly covalently linked to a first polymer side chain group; wherein said reactive diluent is provided in the presence of the first macromonomer at an amount selected so as to result in formation said graft copolymer having a first backbone incorporating said diluent and said first macromonomer in a first polymer block characterized by a preselected first graft density or a preselected first graft distribution of said first macromonomer. In some embodiments of this aspect, said preselected first graft density is any value selected from the range of 0.05 to 0.75. In some methods, the composition and amount of said diluent is selected to provide both a first preselected first graft density and a first preselected first graft distribution.

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Research Organization:: California Inst. of Technology (CalTech), Pasadena, CA (United States)

Sponsoring Organization:: USDOE; National Science Foundation (NSF)

DOE Contract Number:: AR0000683

Assignee:: California Institute of Technology (Pasadena, CA)

Patent Number(s):: 11,053,356

Application Number:: 15/914,762

OSTI ID:: 1840227

Country of Publication:: United States

Language:: English

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Computer Simulations of Bottle Brushes: From Melts to Soft Networks Cao, Zhen; Carrillo, Jan-Michael Y.; Sheiko, Sergei S. Macromolecules, Vol. 48, Issue 14 https://doi.org/10.1021/acs.macromol.5b00682	journal	July 2015
Well-Defined Polyethylene-Based Random, Block, and Bilayered Molecular Cobrushes Zhang, Hefeng; Zhang, Zhen; Gnanou, Yves Macromolecules, Vol. 48, Issue 11 https://doi.org/10.1021/acs.macromol.5b00713	journal	May 2015
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Rheological Influence of Short-Chain Branching for Polymeric Materials under Shear with Variable Branch Density and Branching Architecture Jeong, Seung Heum; Kim, Jun Mo; Baig, Chunggi Macromolecules, Vol. 50, Issue 11 https://doi.org/10.1021/acs.macromol.7b00544	journal	May 2017
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Synthesis of Fluorine-18 Functionalized Nanoparticles for use as in vivo Molecular Imaging Agents Matson, John B.; Grubbs, Robert H. Journal of the American Chemical Society, Vol. 130, Issue 21 https://doi.org/10.1021/ja802010d	journal	May 2008
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Full Color Stop Bands in Hybrid Organic/Inorganic Block Copolymer Photonic Gels by Swelling−Freezing Kang, Changjoon; Kim, Eunjoo; Baek, Heeyoel Journal of the American Chemical Society, Vol. 131, Issue 22 https://doi.org/10.1021/ja9021478	journal	June 2009
Alternating Ring-Opening Metathesis Copolymerization of Amino Acid Derived Norbornene Monomers Carrying Nonprotected Carboxy and Amino Groups Based on Acid−Base Interaction Sutthasupa, Sutthira; Shiotsuki, Masashi; Masuda, Toshio Journal of the American Chemical Society, Vol. 131, Issue 30 https://doi.org/10.1021/ja903248c	journal	July 2009
One-Pot Synthesis of Brush-Like Polymers via Integrated Ring-Opening Metathesis Polymerization and Polymerization of Amino Acid N -Carboxyanhydrides Lu, Hua; Wang, Jing; Lin, Yao Journal of the American Chemical Society, Vol. 131, Issue 38 https://doi.org/10.1021/ja903425x	journal	September 2009
Efficient Synthesis of Narrowly Dispersed Brush Copolymers and Study of Their Assemblies: The Importance of Side Chain Arrangement Xia, Yan; Olsen, Bradley D.; Kornfield, Julia A. Journal of the American Chemical Society, Vol. 131, Issue 51, p. 18525-18532 https://doi.org/10.1021/ja908379q	journal	December 2009
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