Control of polymer architectures by living ring-opening metathesis copolymerization

Grubbs, Robert H.; Lin, Tzu-Pin; Chang, Alice; Chen, Hsiang-Yun; Bates, Christopher M.

Title: Control of polymer architectures by living ring-opening metathesis copolymerization

Patent · Tue Jul 06 00:00:00 EDT 2021

OSTI ID:1840227

Grubbs, Robert H.; Lin, Tzu-Pin; Chang, Alice; Chen, Hsiang-Yun; Bates, Christopher M.

In an aspect, a method of synthesizing a graft copolymer comprises the steps of: copolymerizing a first macromonomer and a first reactive diluent; wherein said first macromonomer comprises a first backbone precursor directly or indirectly covalently linked to a first polymer side chain group; wherein said reactive diluent is provided in the presence of the first macromonomer at an amount selected so as to result in formation said graft copolymer having a first backbone incorporating said diluent and said first macromonomer in a first polymer block characterized by a preselected first graft density or a preselected first graft distribution of said first macromonomer. In some embodiments of this aspect, said preselected first graft density is any value selected from the range of 0.05 to 0.75. In some methods, the composition and amount of said diluent is selected to provide both a first preselected first graft density and a first preselected first graft distribution.

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Research Organization:: California Institute of Technology (CalTech), Pasadena, CA (United States)

Sponsoring Organization:: USDOE; National Science Foundation (NSF)

DOE Contract Number:: AR0000683; CHE1502616

Assignee:: California Institute of Technology (Pasadena, CA)

Patent Number(s):: 11,053,356

Application Number:: 15/914,762

OSTI ID:: 1840227

Resource Relation:: Patent File Date: 03/07/2018

Country of Publication:: United States

Language:: English

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