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Dehydrochlorination of waste 1,1,2-trichloroethane

Journal Article · · Industrial and Engineering Chemistry Research
; ;  [1]
  1. Technical Univ. of Szczecin (Poland). Dept. of Organic Technology

The best results of the waste 1,1,2-trichloroethane dehydrochlorination by 10 wt% NaOH are obtained in temperature 70--80 C at NaOH/112-TCE molar ratio 1.1:1 and flow rate 270 g/(dm{sup 3} h). In these conditions 98.3 wt% vinylidene chloride and aqueous layer (13 wt% NaCl + 0.07 wt % NaOH) are obtained. Vinylidene chloride yield is 97.5 mol%.

Sponsoring Organization:
USDOE
OSTI ID:
178380
Journal Information:
Industrial and Engineering Chemistry Research, Journal Name: Industrial and Engineering Chemistry Research Journal Issue: 6 Vol. 34; ISSN 0888-5885; ISSN IECRED
Country of Publication:
United States
Language:
English

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